KR20080107812A - Method of manufacturing coal using herbal remnants - Google Patents

Method of manufacturing coal using herbal remnants Download PDF

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KR20080107812A
KR20080107812A KR1020070056072A KR20070056072A KR20080107812A KR 20080107812 A KR20080107812 A KR 20080107812A KR 1020070056072 A KR1020070056072 A KR 1020070056072A KR 20070056072 A KR20070056072 A KR 20070056072A KR 20080107812 A KR20080107812 A KR 20080107812A
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weight
carbonized
residue
mixing
herbal
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Korean (ko)
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송두경
김상돈
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송두경
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/30—Active carbon
    • C01B32/312—Preparation
    • C01B32/318—Preparation characterised by the starting materials
    • C01B32/324—Preparation characterised by the starting materials from waste materials, e.g. tyres or spent sulfite pulp liquor
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/30—Active carbon
    • C01B32/312—Preparation
    • C01B32/342—Preparation characterised by non-gaseous activating agents
    • C01B32/348—Metallic compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines

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  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Materials Engineering (AREA)
  • Solid Fuels And Fuel-Associated Substances (AREA)

Abstract

A manufacturing method of activated charcoal using residue of herb medicine is provided to be molded by mixing a sticky mixture having an adhesive property and manufactured by mixing water, solubilized starch and sodium hydroxide, a residue of smashed and carbonized herb medicine and an illite and to be useful to human body by adding no harmful components such as nitrate etc. A manufacturing method of activated charcoal using residue of herb medicine comprises steps of: supplying the residue of herb medicine to a carbonizing machine(1) and being carbonized while being put in fire for 10~15 hours at 900~1000‹C indirectly; transferring and shattering the residue of carbonized herb medicine by a crusher(2); mixing water 68~72 of weight%, solubilized starch of 27.9~31.9 weight% and sodium hydroxide of 0.05~0.15 weight% in a first mixer(3) and manufacturing a sticky mixture having an adhesive property; mixing residue of carbonized and smashed herb medicine of 88.5~96,5 weight %, a sticky mixture of 3~10 weight % and an illite of 0.1~2 weight % in a second mixer(4) and manufacturing a semi-product on which a component gets; putting the mixed semi-product into a molder(5) and being molded to the coal of a cylinder of which a center is opened by a hole, a hexagonal pillar and an octagonal pillar; and being slowly cooled in a room temperature after putting the molded coal into a drying furnace(6) and drying the molded coal.

Description

한약 찌꺼기를 이용한 활성탄의 제조방법{omitted}Method of manufacturing activated carbon using herbal remnants {omitted}

도 1은 본 발명의 활성탄을 제조하는 상태를 나타낸 개략도.1 is a schematic view showing a state of producing the activated carbon of the present invention.

* 도면의 주요 부분에 대한 부호의 설명 *Explanation of symbols on the main parts of the drawings

1 : 탄화장치 2 : 파쇄기1: carbonization device 2: shredder

3, 4 : 교반기 5 : 성형기3, 4: agitator 5: molding machine

6 : 건조로6: drying furnace

본 발명은 한약 찌꺼기를 이용한 활성탄의 제조방법에 관한 것으로, 상세하게는 물, 가용성 전분 및 가성소다를 혼합하여 제조한 접착성이 있는 끈적끈적한 혼합물과, 탄화시켜 파쇄한 한약 찌꺼기 및 일라이트를 혼합하여 성형하도록 함으로써 음식점탄, 야외용탄, 번개탄을 제조하면서 발화성 물질인 질산염 등의 유해한 성분을 첨가하지 않으면서 인체에 유익하도록 하여 고기를 구울 때 육즙이 살아있고 골고루 익어 맛이 살아있도록 한 한약 찌꺼기를 이용한 활성탄의 제조방법에 관한 것이다.The present invention relates to a method for producing activated carbon using herbal remnants, and more specifically, to an adhesive sticky mixture prepared by mixing water, soluble starch and caustic soda, and to mixing carbonized and broken Chinese herbal remnants and illite. The Chinese medicine dregs are used to make restaurant charcoal, outdoor charcoal, and lightning charcoal, and to be beneficial to the human body without adding harmful ingredients such as ignitable substance such as pyrophoric substances. It relates to a method for producing activated carbon used.

일반적으로 숯불구이용으로 이용되는 고체연료의 경우 참나무 숯을 이용한 참숯이 가장 좋은 것으로 평가되고 있으나 가격이 비싸다는 큰 단점이 있다.In general, in the case of solid fuel used for charcoal roasting, the charcoal using oak charcoal is evaluated as the best, but the price is expensive.

따라서 현재 대량으로 이용되고 있는 대부분의 업소에서는 목분을 탄화하여 압축시킨 수입성형목탄과 목분에 화공약품인 질산바륨, 질산소다 등을 첨가시켜 착화성과 휴대성을 높인 순간착화 열탄이 일반적으로 가장 널리 사용되고 있다.Therefore, in most of the businesses that are currently used in large quantities, imported molded charcoal, which is carbonized and compressed with wood powder, and instantaneous ignited hot coal, which has high ignition and portability by adding chemicals such as barium nitrate and sodium nitrate, are generally used most widely. have.

지금까지의 숯불구이용 고체연료에 대한 개발 경향을 살펴보면 고형연료(특 10-0278791), 휴대용 고체연료(특 20-0220385호), 고체연료(특 1985-0001738), 2차적 성형목탄형 고체연료(특 1990-0004939호), 고체연료(특 1995-0005691호), 고체연료조성물(특 0144698호) 등과, 그 외 등록되지 못한 많은 출원물들은 대부분 업소에서 열탄 사용시 외부에서 착화하여 실내로 옮겨오는 과정을 생략하여 편리성을 추구하기 위해 목분에 첨가되는 화공약품 조성물의 종류, 혼합량 및 혼합방법에 대한 내용으로 구성되어 있다.So far, the development trends of charcoal-fired solid fuels include solid fuels (special 10-0278791), portable solid fuels (special 20-0220385), solid fuels (special 1985-0001738), secondary shaping charcoal solid fuels ( Japanese Patent No. 1990-0004939), Solid Fuel (Special 1995-0005691), Solid Fuel Composition (Special No. 0144698), and many other unregistered applications, most of them have a process of ignition from the outside when they use hot coal. It is composed of the contents, the mixing amount, and the mixing method of the chemical composition added to wood flour in order to omit convenience.

그러나 순간착화 등의 편리성을 위해 다양한 화공약품의 첨가와 복잡한 제조공정의 순간착화식 열탄은 MBC(2000년 12월, 2001년 2월, 2002년 5월), KBS(2002년 5월), SBS(2001년 12월, 2002년 3월, 2002년 5월) 뉴스에서 보도된 바와 같이 직화 구이 시 바륨, 아연 등의 유해성분 검출과 벤조피렌 등의 발암물질에 의한 위해성의 문제와, 생산단가의 상승으로 실제 현장적용에는 문제점을 발생시킬 수 있다.However, for the convenience of instant ignition, the addition of various chemicals and the flash ignition type of the complex manufacturing process are shown in MBC (December 2000, February 2001, May 2002), KBS (May 2002), As reported in the news of SBS (December 2001, March 2002, May 2002), the detection of harmful substances such as barium and zinc, and the risk of carcinogens such as benzopyrene and the production cost The rise may cause problems in actual field application.

따라서 소량으로 이용되는 가정용, 야외용으로는 일부 개발, 판매되고 있으나, 현재 대부분의 숯불구이용 고체연료를 사용하는 업소들의 경우 편리성보다는 경제성에 중점을 두어 여전히 실외에서 착화하여 실내로 옮겨오는 목분을 탄화하여 압축시킨 일반적인 수입 열탄의 이용률이 훨씬 높은 실정이다.Therefore, some are developed and sold for home use and outdoor use, which are used in small quantities. However, most of the businesses that use solid fuel for charcoal roasting still carbonize the wood powder, which is ignited outdoors and transferred to the indoors, focusing on economy rather than convenience. The utilization rate of the imported imported coal is compressed much higher.

그러나 대부분 업소에서 이용되고 있는 숯불구이용 열탄은 생산에 있어 원료 수급문제와 제조단가 등의 경제적인 문제에 의해 수입에 의존하고 있으며 사용시 재비산과 연소지속성에 문제가 있다.However, charcoal grilled hot coal, which is mostly used in businesses, is dependent on imports due to economic problems such as supply and demand for raw materials and manufacturing cost, and has problems with re-spreading and combustion sustainability.

한편, 석탄의 경우 연소시 이산화황이 발생되는 문제와 석탄의 특성상 착화 후에는 연소지속성이 좋지만 착화가 어려워 숯불구이용 연료로 활용하기에는 여러 가지 어려움이 많아 질산바륨 등의 화학물질을 첨가한 개량 열탄 및 그 제조방법(출원번호 1994-0004923호)과, 고체연료 조성물 및 고체연료의 제조방법(특허 0153137호)으로 등록된 바와 같이 목탄 등을 주성분으로 하여 소량의 석탄(무연탄 또는 코크스)을 연소속도 조절제로 첨가하는 방안에 대해서는 연구되고 있으나, 발화성 물질인 질산염 등의 유해한 성분을 첨가한 상태로 인하여 연소시 유해한 가스가 발생하게 되는 등의 단점이 있었다.On the other hand, in the case of coal, sulfur dioxide is generated during combustion and, due to the characteristics of coal, combustion persistence is good after ignition, but it is difficult to ignite, and thus it is difficult to be used as a fuel for charcoal roasting. As registered in the manufacturing method (Application No. 1994-0004923) and the manufacturing method of the solid fuel composition and the solid fuel (Patent 0153137), a small amount of coal (anthracite or coke) is used as a burn rate control agent based on charcoal and the like. Although the method of adding is being studied, there is a disadvantage in that harmful gas is generated during combustion due to the addition of harmful components such as nitrate, which is a flammable substance.

이에 따라 패각을 탈황제로 활용하고 석탄을 주원료로 이용하는 연구가 진행되어 2004년 2월 27일 특허출원 제10-2004-0013411호(환경친화적인 숯불구이용 고체연료 제조방법)가 제안되았는 바,As a result, research on the use of shells as a desulfurization agent and coal as a main raw material was conducted. On February 27, 2004, a patent application No. 10-2004-0013411 (a method for producing solid fuel for charcoal roasting) was proposed.

이는, 경제성에 의해 대부분의 업소용으로 여전히 이용되고 있는 일반적인 수입 열탄을 대체하고자 하여 구성물질과 혼합방법을 간소화하여 석탄, 탄화톱밥, 버려지는 패각과 농업부산물(볏짚 등), 점결제로 구성한 것으로서,It is composed of coal, carbon sawdust, discarded shells and agricultural by-products (straw straw, etc.) and caking additives by simplifying the composition and mixing method in order to replace the imported imported hot coal, which is still used for most businesses due to economic feasibility.

주원료인 석탄 40∼60％(w/w), 착화성 향상을 위한 탄화톱밥 20∼40％(w/w), 농업부산물인 왕겨, 볏짚 또는 톱밥 5∼20％(w/w) 그리고, binder로 당밀이나 밀가루 5∼20％(w/w)와 탈황제인 패각의 적량으로 구성하였다.Coal 40 ~ 60% (w / w) as main raw material, carbonized sawdust 20 ~ 40% (w / w) for improving flammability, rice hull, rice straw or sawdust 5 ~ 20% (w / w) as agricultural by-product, and binder Furnace was composed of an appropriate amount of molasses or wheat flour 5-20% (w / w) and the shell desulfurization agent.

그리고 이산화황 제어에 이용되는 패각의 분말입자크기는 90∼150㎛를 이용하고, 패각과 석탄의 Ca와 S의 함량을 고려하여 Ca/S 비율이 1.5∼3.0이 되게 첨가량을 결정하였다.The particle size of the shell used for sulfur dioxide control was 90 to 150 µm, and the amount of Ca / S was determined to be 1.5 to 3.0 in consideration of Ca and S contents of the shell and coal.

그러나 상기와 같은 종래의 환경친화적인 숯불구이용 고체연료 제조방법에 의하여서는 다양한 화학물질을 첨가하여 위해성에 문제는 있으나 순간착화 등의 편이성이 좋은 열탄에 비해 실외에서 착화하여 실내로 가지고 오는 불편이 있는 등의 단점이 있었다. However, the conventional environmentally friendly charcoal-fired solid fuel manufacturing method as described above has a problem in risk by adding various chemicals, but it is inconvenient to bring it to the room by ignition outdoors compared to hot coal, such as instant ignition. There was such a disadvantage.

이에 본 발명은 상기한 바와 같은 종래의 문제점을 해소시키기 위하여 안출된 것으로, 물, 가용성 전분 및 가성소다를 혼합하여 제조한 접착성이 있는 끈적끈적한 혼합물과, 탄화시켜 파쇄한 한약 찌꺼기 및 일라이트를 혼합하여 성형하도록 함으로써 음식점탄, 야외용탄, 번개탄을 제조하면서 발화성 물질인 질산염 등의 유해한 성분을 첨가하지 않으면서 인체에 유익하도록 하여 고기를 구울 때 육즙이 살아있고 골고루 익어 맛이 살아있도록 한 한약 찌꺼기를 이용한 활성탄의 제조방법을 제공하는 것을 그 목적으로 한다.Accordingly, the present invention has been made in order to solve the above-mentioned problems, the adhesive sticky mixture prepared by mixing water, soluble starch and caustic soda, and the Chinese herbal crushed and crushed by carbonization By mixing and molding, it is beneficial to the human body without adding harmful ingredients such as ignitables such as ignition flammables in the production of restaurant charcoal, outdoor charcoal, and lightning charcoal. It is an object of the present invention to provide a method for producing activated carbon.

상기 목적을 달성하기 위한 본 발명의 한약 찌꺼기를 이용한 활성탄의 제조방법은,Method for producing activated carbon using herbal remnants of the present invention for achieving the above object,

한약 찌꺼기, 가용성 전분, 가성소다 및 일라이트를 각각 호퍼에 저장하는 과정과,Storing medicinal dregs, soluble starch, caustic soda and illite in the hopper, respectively,

상기의 한약 찌꺼기를 탄화장치에 공급하여 900∼1000℃의 10∼15시간 동안 간접 연소시키는 중에 탄화되도록 하는 과정과,Supplying the herbal remnants to a carbonization apparatus to carbonize during indirect combustion at 900 to 1000 ° C. for 10 to 15 hours,

상기의 탄화시킨 한약 찌꺼기를 파쇄기로 이송하여 200∼300 메시의 고운 입자 상태로 파쇄시키는 과정과,Transferring the carbonized herbal remnants to a crusher and crushing them into fine particles of 200 to 300 mesh;

물 68∼72 중량％, 가용성 전분 27.9∼31.9 중량％ 및 가성소다 0.05∼0.15 중량％ 의 비율로 혼합하여 접착성이 있는 끈적끈적한 혼합물을 제조하는 과정과,Preparing a sticky sticky mixture by mixing 68 to 72% by weight of water, 27.9 to 31.9% by weight of soluble starch, and 0.05 to 0.15% by weight of caustic soda,

상기의 탄화시켜 파쇄한 한약 찌꺼기 88.5∼96,5 중량％와 끈적끈적한 혼합물 3∼10중량％ 및 일라이트 0.1∼2 중량％를 혼합하여 반제품을 제조하는 과정과,Preparing a semi-finished product by mixing 88.5 to 96,5% by weight of the carbonized and crushed herbal remnants, 3 to 10% by weight of the sticky mixture and 0.1 to 2% by weight of the illite;

상기의 혼합한 반제품을 성형기에 넣어 중앙에 구멍이 뚫린 원기둥, 육각 기둥, 팔각 기둥의 탄으로 성형하는 과정과,Putting the mixed semi-finished product into a molding machine and forming into a shot of a cylinder, hexagonal pillar, and octagonal pillar with a central hole,

상기의 성형한 탄을 건조로에 넣어 상기 탄화장치의 폐열을 이용하여 약 200∼300℃의 열풍으로 건조시킨 후 상온에서 천천히 식혀 완성하는 과정들로 구성됨을 특징으로 한다.The formed coal is dried in a drying furnace and dried using hot air of about 200 to 300 ° C. using waste heat of the carbonization apparatus, and then slowly cooled to room temperature to complete the process.

이하, 첨부된 도면을 참조하여 본 발명의 바람직한 실시예를 설명하면 다음과 같다.Hereinafter, exemplary embodiments of the present invention will be described with reference to the accompanying drawings.

본 발명에 따른 한약 찌꺼기를 이용한 활성탄의 제조방법은,Method for producing activated carbon using herbal remnants according to the present invention,

한약 찌꺼기, 가용성 전분, 가성소다 및 일라이트를 각각 저장하도록 하고,Store herbal remnants, soluble starch, caustic soda and illite, respectively,

상기의 한약 찌꺼기를 탄화장치(1)에 공급하여 900∼1000℃의 10∼15시간 동안 간접 연소시키는 중에 탄화되도록 하도록 하고,The herbal debris is supplied to the carbonization apparatus 1 so as to be carbonized during indirect combustion at 900 to 1000 ° C. for 10 to 15 hours,

상기의 탄화시킨 한약 찌꺼기를 파쇄기(2)로 이송하여 200∼300 메시의 고운 입자 상태로 파쇄시키도록 하고,The carbonized herbal debris is transferred to a crusher 2 to be crushed into fine particles of 200 to 300 mesh,

물 68∼72 중량％, 가용성 전분 27.9∼31.9 중량％ 및 가성소다 0.05∼0.15 중량％를 제1 교반기(3)에서 혼합하여 접착성이 있는 끈적끈적한 혼합물을 제조하도록 하고,68 to 72% by weight of water, 27.9 to 31.9% by weight of soluble starch and 0.05 to 0.15% by weight of caustic soda are mixed in the first stirrer 3 to prepare an adhesive sticky mixture,

상기의 탄화시켜 파쇄한 한약 찌꺼기 88.5∼96,5 중량％와 끈적끈적한 혼합물 3∼10중량％ 및 일라이트 0.1∼2 중량％를 제2 교반기(4)에서 혼합하여 탄 성분인 반제품을 제조하도록 하고,The carbonized and crushed Chinese herbal remnants 88.5 to 96,5% by weight, the sticky mixture 3-10% by weight and the illite 0.1-2% by weight are mixed in a second stirrer 4 to produce a burnt semi-finished product. ,

상기의 혼합한 탄 성분인 반제품을 성형기(5)에 넣어 중앙에 구멍이 뚫린 원기둥, 육각 기둥, 팔각 기둥의 탄으로 성형하도록 하고,The semi-finished product of the above-described mixed carbon component is put into the molding machine 5 so as to be molded into a cylinder having a central hole, a hexagonal column, and an octagonal column.

상기의 성형한 탄을 건조로(6)에 넣어 200∼300℃의 열풍으로 건조시킨 후 상온에서 천천히 식혀 활성탄을 완성하도록 한 것이다.The molded carbon is put in a drying furnace 6, dried with hot air at 200 to 300 ° C., and then cooled slowly at room temperature to complete activated carbon.

상기와 같은 본 발명은 한약 찌꺼기, 가용성 전분, 가성소다 및 일라이트의 재료로 구이에 좋은 활성탄의 제조방법에 그 특징이 있는 것으로서,As described above, the present invention is characterized by a method of producing activated carbon which is good for roasting with ingredients of herbal remnants, soluble starch, caustic soda and illite,

도면에 도시하지 않은 호퍼와 같은 저장용기에 한약 찌꺼기, 가용성 전분, 가성소다 및 일라이트를 각각 저장하는 과정과,Storing the herbal debris, soluble starch, caustic soda and illite in a storage container such as a hopper not shown in the drawing,

상기의 한약 찌꺼기를 탄화장치(1)에 공급하여 900∼1000℃의 10∼15시간 동안 간접 연소시키는 중에 탄화되도록 하는 과정과,Supplying the herbal debris to the carbonization apparatus 1 so as to carbonize it during indirect combustion at 900 to 1000 ° C. for 10 to 15 hours,

상기의 탄화시킨 한약 찌꺼기를 파쇄기(2)로 이송하여 200∼300 메시의 고운 입자 상태로 파쇄시키는 과정과,Transferring the carbonized herbal debris to the crusher 2 and crushing the finely divided grains into fine particles of 200 to 300 mesh;

물 68∼72 중량％, 가용성 전분 27.9∼31.9 중량％ 및 가성소다 0.05∼0.15 중량％를 제1 교반기(3)에서 혼합하여 접착성이 있는 끈적끈적한 혼합물을 제조하는 과정과,Mixing 68 to 72% by weight of water, 27.9 to 31.9% by weight of soluble starch, and 0.05 to 0.15% by weight of caustic soda in the first stirrer 3 to prepare an adhesive sticky mixture,

상기의 끈적끈적한 혼합물은 탄 성분을 성형한 후 임의로 분리되는 것을 방지하여 고체연료로의 제작이 가능하도록 함은 물론, 배합하는 비율에 의하여 연소 상태를 얼마간 조절할 수 있게 된다.The sticky mixture prevents the carbonaceous component from being separated after the molding of the burnt component, thereby making it possible to manufacture a solid fuel, and of course, the combustion state can be controlled by the mixing ratio.

상기의 탄화시켜 파쇄한 한약 찌꺼기 88.5∼96,5 중량％와 끈적끈적한 혼합물 3∼10중량％ 및 일라이트 0.1∼2 중량％를 제2 교반기(4)에서 혼합하여 탄 성분인 반제품을 제조하는 과정과,A process for producing a carbonaceous semi-finished product by mixing 88.5 to 96,5% by weight of the carbonized and crushed Chinese dregs and 3 to 10% by weight of the sticky mixture and 0.1 to 2% by weight of the illite in a second stirrer (4) and,

상기의 일라이트는 다량의 음이온과 원적외선 및 산소를 발산하는 점토질 광물로써 탄에 포함된 일라이트에서 발산되는 음이온과 원적외선에 의하여 인체에 유익한 효과를 가지게 된다.The illite is a clay mineral that emits a large amount of anions and far infrared rays and oxygen, and has an advantageous effect on the human body by the anion and far infrared rays emitted from the illite contained in the carbon.

상기의 혼합한 반제품을 성형기(5)에 넣어 중앙에 구멍이 뚫린 원기둥, 육각 기둥, 팔각 기둥의 탄으로 성형하는 과정과,Putting the mixed semi-finished product in the molding machine (5) and molding into a round cylinder, a hexagonal column, and an octagonal column with holes in the center;

상기의 성형한 탄을 건조로(6)에 넣어 상기 탄화장치의 폐열을 이용하여 약 200∼300℃의 열풍으로 건조시킨 후 상온에서 천천히 식혀 완성하는 과정들로 수행됨을 특징으로 한다.The molded coal is dried into a drying furnace 6, and dried using hot air of about 200 to 300 ° C. using waste heat of the carbonization apparatus, and then slowly cooled to room temperature to be completed.

상기와 같은 제조 과정에 의한 본 발명의 한약 찌꺼기를 이용한 활성탄의 제조방법은,Method for producing activated carbon using the herbal remnants of the present invention by the above manufacturing process,

한약 찌꺼기를 탄화장치(1)에 공급하여 900∼1000℃의 10∼15시간 동안 간접 연소시키는 중에 탄화시킨 후 파쇄기(2)로 200∼300 메시의 고운 입자 상태로 파쇄 시키도록 하고,The herbal remnants are fed to the carbonization apparatus 1 and carbonized during indirect combustion at 900 to 1000 ° C. for 10 to 15 hours, and then crushed into fine particles of 200 to 300 mesh by a crusher 2,

물 68∼72 중량％, 가용성 전분 27.9∼31.9 중량％ 및 가성소다 0.05∼0.15 중량％를 제1 교반기(3)에서 혼합하여 접착성이 있는 끈적끈적한 혼합물을 제조하고,68-72% by weight of water, 27.9-31.9% by weight of soluble starch and 0.05-0.15% by weight of caustic soda are mixed in the first stirrer 3 to prepare an adhesive sticky mixture,

상기의 탄화시켜 파쇄한 한약 찌꺼기 88.5∼96,5 중량％와 끈적끈적한 혼합물 3∼10중량％ 및 일라이트 0.1∼2 중량％를 제2 교반기(4)에서 혼합한 탄 성분인 반제품을 성형기(5)에 넣어 탄으로 성형하도록 하고,The carbonaceous semi-finished product which mixed 88.5-96,5 weight% of said carbonized and crushed Chinese dregs, 3-10 weight% of sticky mixtures, and 0.1-2 weight% of an illite in the 2nd stirrer 4 was used for the molding machine (5). ) Into a bullet,

상기의 성형한 탄을 건조로(6)에 넣어 200∼300℃의 열풍으로 건조시킨 후 상온에서 천천히 식혀 활성탄을 완성하여 음식점탄, 야외용탄, 번개탄을 제조하도록 함으로써 발화성 물질인 질산염의 유해한 성분을 첨가하지 않으면서 인체에 유익하도록 하여 고기를 구울 때 육즙이 살아있고 골고루 익어 맛이 살아있도록 한다.Put the molded coal into the drying furnace 6 and dry it with hot air at 200-300 ° C., and then slowly cool it at room temperature to complete the activated carbon to produce restaurant coal, outdoor coal, and lightning charcoal. It is beneficial to the human body without adding it so that the meat is alive and juicy evenly when grilled.

이상에서는 본 발명의 바람직한 실시예에 대하여 도시하고 또한 설명하였으나, 본 발명은 상기한 실시예에 한정되지 아니하며, 청구범위에서 청구하는 본 발명의 요지를 벗어남이 없이 당해 본 발명이 속하는 분야에서 통상의 지식을 가진 자라면 누구든지 다양한 변형 실시가 가능한 것은 물론이고, 그와 같은 변경은 기재된 청구범위 내에 있게 된다.Although the preferred embodiments of the present invention have been illustrated and described above, the present invention is not limited to the above-described embodiments, and the present invention is not limited to the above-described embodiments without departing from the spirit of the present invention as claimed in the claims. Various modifications can be made by those skilled in the art, and such modifications are intended to fall within the scope of the appended claims.

이상에서 상세히 설명한 바와 같이 본 발명에 따른 한약 찌꺼기를 이용한 활성탄의 제조방법에 의하여서는 한약 찌꺼기를 간접 연소시키면서 탄화하여 파쇄하 도록 하고,As described in detail above, according to the method for producing activated carbon using herbal remnants according to the present invention, the herbal remnants are carbonized while being indirectly burned and crushed,

물, 가용성 전분 및 가성소다를 혼합하여 접착성이 있는 끈적끈적한 혼합물을 제조하도록 하고,Mix water, soluble starch and caustic soda to produce a sticky sticky mixture,

상기의 탄화시켜 파쇄한 한약 찌꺼기와 접착성이 있는 끈적끈적한 혼합물 및 일라이트를 혼합하고 성형한 후 건조시키도록 함으로써 음식점탄, 야외용탄, 번개탄을 제조하면서 발화성 물질인 질산염 등의 유해한 성분을 첨가하지 않으면서 인체에 유익하도록 하여 고기를 구울 때 육즙이 살아있고 골고루 익어 맛이 살아있도록 하는 효과가 있다.By mixing, shaping, and drying the above carbonized and crushed Chinese herbal remnants and adhesive sticky mixtures and illite, it is possible to add harmful ingredients such as nitrate, which is a flammable substance, while preparing restaurant coal, outdoor coal, and lightning coal. It is beneficial to the human body without roasting the meat when the juice is alive and evenly cooked, the taste is alive.

Claims (1)

한약 찌꺼기, 가용성 전분, 가성소다 및 일라이트를 각각 저장하는 과정과,Storing the herbal residues, soluble starch, caustic soda and illite, respectively, 상기의 한약 찌꺼기를 탄화장치(1)에 공급하여 900∼1000℃의 10∼15시간 동안 간접 연소시키는 중에 탄화되도록 하는 과정과,Supplying the herbal debris to the carbonization apparatus 1 so as to carbonize it during indirect combustion at 900 to 1000 ° C. for 10 to 15 hours, 상기의 탄화시킨 한약 찌꺼기를 파쇄기(2)로 이송하여 200∼300 메시의 고운 입자 상태로 파쇄시키는 과정과,Transferring the carbonized herbal debris to the crusher 2 and crushing the finely divided grains into fine particles of 200 to 300 mesh; 물 68∼72 중량％, 가용성 전분 27.9∼31.9 중량％ 및 가성소다 0.05∼0.15 중량％를 제1 교반기(3)에서 혼합하여 접착성이 있는 끈적끈적한 혼합물을 제조하는 과정과,Mixing 68 to 72% by weight of water, 27.9 to 31.9% by weight of soluble starch, and 0.05 to 0.15% by weight of caustic soda in the first stirrer 3 to prepare an adhesive sticky mixture, 상기의 탄화시켜 파쇄한 한약 찌꺼기 88.5∼96,5 중량％와 끈적끈적한 혼합물 3∼10중량％ 및 일라이트 0.1∼2 중량％를 제2 교반기(4)에서 혼합하여 탄 성분인 반제품을 제조하는 과정과,A process for producing a carbonaceous semi-finished product by mixing 88.5 to 96,5% by weight of the carbonized and crushed Chinese dregs and 3 to 10% by weight of the sticky mixture and 0.1 to 2% by weight of the illite in a second stirrer (4) and, 상기의 혼합한 반제품을 성형기(5)에 넣어 중앙에 구멍이 뚫린 원기둥, 육각 기둥, 팔각 기둥의 탄으로 성형하는 과정과,Putting the mixed semi-finished product in the molding machine (5) and molding into a round cylinder, a hexagonal column, and an octagonal column with holes in the center; 상기의 성형한 탄을 건조로(6)에 넣어 상기 탄화장치의 폐열을 이용하여 약 200∼300℃의 열풍으로 건조시킨 후 상온에서 천천히 식혀 완성하는 과정들로 구성한 것을 특징으로 하는 한약 찌꺼기를 이용한 활성탄의 제조방법.Put the molded coal into the drying furnace (6) by using the waste heat of the carbonization apparatus dried by hot air of about 200 ~ 300 ℃ and then slowly cooled to room temperature and using the herbal residues, characterized in that consisting of Method for producing activated carbon.
KR1020070056072A 2007-06-08 2007-06-08 Method of manufacturing coal using herbal remnants KR20080107812A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100979391B1 (en) * 2010-06-15 2010-08-31 서원대 Grain rice hull charcoal and the producing method thereof
KR101593146B1 (en) * 2014-11-07 2016-02-12 (주)에코파낙스 A manufacturing method for smoked chips on charcoal roasting using red ginseng by-products
CN110467181A (en) * 2019-08-15 2019-11-19 石河子大学 A kind of classifying porous charcoal of liquorice dregs base and its preparation method and application
CN113479876A (en) * 2021-08-05 2021-10-08 河南中医药大学 Belladonna herb residue porous carbon and preparation method and application thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100979391B1 (en) * 2010-06-15 2010-08-31 서원대 Grain rice hull charcoal and the producing method thereof
KR101593146B1 (en) * 2014-11-07 2016-02-12 (주)에코파낙스 A manufacturing method for smoked chips on charcoal roasting using red ginseng by-products
CN110467181A (en) * 2019-08-15 2019-11-19 石河子大学 A kind of classifying porous charcoal of liquorice dregs base and its preparation method and application
CN113479876A (en) * 2021-08-05 2021-10-08 河南中医药大学 Belladonna herb residue porous carbon and preparation method and application thereof
CN113479876B (en) * 2021-08-05 2022-12-30 河南中医药大学 Belladonna herb residue porous carbon and preparation method and application thereof

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