KR20040070398A - Soap composition - Google Patents

Soap composition Download PDF

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KR20040070398A
KR20040070398A KR1020030006591A KR20030006591A KR20040070398A KR 20040070398 A KR20040070398 A KR 20040070398A KR 1020030006591 A KR1020030006591 A KR 1020030006591A KR 20030006591 A KR20030006591 A KR 20030006591A KR 20040070398 A KR20040070398 A KR 20040070398A
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soap
weight
parts
soap composition
skin
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KR1020030006591A
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Korean (ko)
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박홍양
권혁신
이재현
심우범
원성욱
오영민
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(주)지텍 바이오
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D47/00—Separating dispersed particles from gases, air or vapours by liquid as separating agent
    • B01D47/06—Spray cleaning
    • B01D47/063—Spray cleaning with two or more jets impinging against each other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/77—Liquid phase processes
    • B01D53/78—Liquid phase processes with gas-liquid contact
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/008—Control or steering systems not provided for elsewhere in subclass C02F
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/46—Treatment of water, waste water, or sewage by electrochemical methods
    • C02F1/461—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
    • C02F1/46104—Devices therefor; Their operating or servicing
    • C02F1/4618—Devices therefor; Their operating or servicing for producing "ionised" acidic or basic water

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Electrochemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

PURPOSE: A soap composition and a solid soap prepared by using the composition are provided, to improve an antibacterial effect and a moisturizing effect by using trichloric acid and benzalkonium chloride. CONSTITUTION: The soap composition comprises 0.01-5.0 parts by weight of trichloric acid and 0.01-5.0 parts by weight of benzalkonium chloride. Preferably the soap composition uses a mixture of a palm oil and a palm kernel oil in the ratio of 6:4 to 7:3 as a soap base. Preferably the soap composition comprises further a skin moisturizing agent, an emulsifier and a hard water softening agent.

Description

비누 조성물{Soap composition}Soap composition

본 발명은 비누 조성물에 관한 것이다.The present invention relates to a soap composition.

일반 비누는 통상 알카리성으로, 알카리성 비누로 자주 세정할 경우 피부 상피세포의 비정상적인 각화에 의해 모공이 막히고 피지가 피부 표면으로 배출이 되지 않으며 피지가 모공내에 뭉쳐있게 되고, 여드름의 원인이 되는 혐기성균 (proipionbacterium acne)이 침투하게 되면 염증이 생기고 피부가 붉어지게 된다. 또한, 피부 표면에 피지가 잘 배출 되더라도 세정후 시간이 흐르면 공기중의 미생물들이 피부 표면에 번식하여 피지를 산패시킴으로 피부의 냄새를 나쁘게 한다.Ordinary soaps are usually alkaline, and when frequently washed with alkaline soaps, pores are blocked by abnormal keratinization of skin epithelial cells, sebum is not discharged to the skin surface, sebum is stuck in the pores, and anaerobic bacteria that cause acne ( Infiltration of proipionbacterium acne causes inflammation and reddening of the skin. In addition, even if sebum is well discharged on the surface of the skin, after time passes, microorganisms in the air multiply on the surface of the skin to dissipate the sebum, which makes the skin smell bad.

일반적으로 비누에 항균효과를 주기 위해 트리클로산을 항균성분으로 사용하여 왔다.In general, triclosan has been used as an antibacterial ingredient to give an antibacterial effect to soap.

트리클로산(2,2',4'-trichloro-2'-hydroxy diphenylether; triclosan)은 그람양성균, 그람음성균, 곰팡이, 이스트 등 광밤위한 균류에 대하여 항균력을 나타내며, 특히 사람의 피부나 점막에 대하여 독성이 낮고, 자극성이 적어 비누나 샴푸, 세정제, 화장품, 연고 등에 사용할 수 있다. 그러나 이들 세제류에 트리클로산을 사용하는 경우 비누의 색을 변색시키거나 햇빛에 노출될 경우 비누를 갈변시키는 단점이 있어, 미국특허 제 4,282,110호에서는 이러한 비누의 변색을 방지하거나 지연시키기 위한 탈색 방지제를 함께 사용하여왔다.Triclosan (2,2 ', 4'-trichloro-2'-hydroxy diphenylether; triclosan) exhibits antimicrobial activity against broad-spectrum fungi such as gram-positive bacteria, gram-negative bacteria, molds and yeasts, and is particularly toxic to human skin or mucous membranes. It has a low irritation and can be used for soaps, shampoos, detergents, cosmetics and ointments. However, the use of triclosan in these detergents has the disadvantage of discoloring the color of the soap or browning the soap when exposed to sunlight, US Patent No. 4,282,110 used together with the anti-bleaching agent to prevent or delay the discoloration of the soap Has been.

또한 이러한 항균제를 포함하고 있는 비누는 주로 액상으로 물속에서 액체 상태로 있으므로, 살균효과를 감소시키는 단점이 있을 뿐 아니라, 피부 보습력이 떨어지는 것이 문제점으로 지적되어 왔다.In addition, since the soap containing the antimicrobial agent is mainly in the liquid state in the liquid state in the water, not only has a disadvantage in reducing the sterilization effect, it has been pointed out as a problem that the skin moisturizing power is poor.

이에 본 발명자들은 뛰어난 항균력을 보유하면서 동시에 피부 보습력도 우수한 비누를 개발함으로써 본 발명을 완성하였다.The present inventors have completed the present invention by developing a soap having excellent antibacterial activity and also excellent skin moisturizing power.

본 발명은 살균력과 보습력이 우수한 비누 조성물을 제공하고자 한다.The present invention is to provide a soap composition excellent in sterilization and moisturizing power.

본 발명은 트리클로산 및 벤잘코늄 클로라이드(benzalkonium chloride)를 함유하는 비누 조성물을 제공한다.The present invention provides a soap composition containing triclosan and benzalkonium chloride.

본 발명의 비누 조성물은 구체적으로 비누 기재, 트리클로산, 벤잘코늄 클로라이드, 피부 보습제, 유화제, 경수연화제를 포함한다.The soap composition of the present invention specifically includes a soap base, triclosan, benzalkonium chloride, a skin moisturizer, an emulsifier, a water softener.

본 발명의 비누 조성물은 비누 기재 80.0 ~ 99.0 중량부, 트리클로산 0.01 ~ 5.0 중량부, 벤잘코늄 클로라이드 0.01 ~ 5.0 중량부, 피부 보습제 0.01 ~ 5.0 중량부, 유화제 0.01 ~ 5.0 중량부, 경수연화제 0.01 ~ 2.0 중량부를 포함한다.Soap composition of the present invention is a soap base 80.0 ~ 99.0 parts by weight, triclosan 0.01 ~ 5.0 parts by weight, benzalkonium chloride 0.01 ~ 5.0 parts by weight, skin moisturizer 0.01 ~ 5.0 parts by weight, emulsifier 0.01 ~ 5.0 parts by weight, water softener 0.01 ~ 2.0 It includes parts by weight.

이하, 본 발명의 비누 조성물의 구성성분에 대해 상세히 설명한다.Hereinafter, the components of the soap composition of the present invention will be described in detail.

본 발명의 비누 조성물에서는 지방산을 비누기재로 사용하며, 이때 사용하는 지방산은 야자유, 팜유, 대두유, 파마자유, 올리브유, 팜핵류 등의 식물유와 우지,돈지, 양지, 어유 등의 동물유지 중에서 하나 이상을 선택하여 사용할 수 있다. 본 발명에서는 팜유/팜핵류를 6/4 또는 7/3의 비율로 혼합한 소지가 바람직하다. 비누 기재의 함량은 80.0 내지 99.0 중량부가 바람직하며, 90.0 내지 98.0 중량부가 더욱 바람직하다.In the soap composition of the present invention, a fatty acid is used as a soap base, wherein the fatty acid used is at least one of vegetable oils such as palm oil, palm oil, soybean oil, palm oil, olive oil, palm kernels, and animal oils such as tallow, pork, sun and fish oil. Can be selected and used. In the present invention, a mixture of palm oil / palm nucleus at a ratio of 6/4 or 7/3 is preferable. The content of the soap base is preferably 80.0 to 99.0 parts by weight, more preferably 90.0 to 98.0 parts by weight.

본 발명의 비누 조성물에서 트리클로산은 항균 작용을 하며, 0.01 내지 5.0 중량부를 포함하며, 0.05 내지 2.0 중량부가 바람직하다. 만일 트리클로산의 농도가 0.01 중량부 이하이면 살균력이 저하되고, 5.0 중량부 이상이면 살균력이 강해지나 독성이 증가한다.In the soap composition of the present invention, triclosan has an antibacterial effect, and includes 0.01 to 5.0 parts by weight, and preferably 0.05 to 2.0 parts by weight. If the concentration of triclosan is 0.01 parts by weight or less, the bactericidal power is lowered. If it is 5.0 parts by weight or more, the bactericidal power becomes stronger but the toxicity is increased.

본 발명의 비누 조성물에서 벤잘코늄 클로라이드는 양이온 계면활성제로 살균효과가 뛰어나며, 하나의 C8~18의 알칼리, 두개의 C1~4의 알칼리 및 벤질기를 포함한다. 벤잘코늄 클로라이드는 0.01 내지 5.0 중량부를 포함하며, 0.05 내지 2.0 중량부가 바람직하다. 만일 벤잘코늄 클로라이드의 농도가 0.01 중량부 이하이면 살균력이 저하되고, 5.0 중량부 이상이면 살균력이 강해지나 독성이 증가한다.Benzalkonium benzalkonium chloride in the soap compositions of the present invention comprises an alkali, the two alkaline and benzyl of C 1 ~ 4 of a C 8 ~ 18, an excellent sterilizing effect by the cationic surfactant. Benzalkonium chloride contains 0.01 to 5.0 parts by weight, with 0.05 to 2.0 parts by weight being preferred. If the concentration of benzalkonium chloride is 0.01 parts by weight or less, the bactericidal power is lowered. If it is 5.0 parts by weight or more, the bactericidal power becomes strong but the toxicity is increased.

본 발명의 비누 조성물에서 피부 보습제는 피부에 보습효과를 주기 위한 것으로, 글리세린, 에리트리톨, 폴리에틸렌글리콜, 프로필렌글리콜, 부틸렌글리콜, 펜틸렌글리콜, 헥실글리콜, 이소프로필미리스테이트, 실리콘 유도체, 알로에 베라, 솔비톨로 이루어진 군으로부터 선택된 1종 이상을 포함하며, 본 발명에서는 글리세린이 바람직하다. 피부 보습제는 0.01 내지 5.0 중량부 포함하며, 0.1 내지 2.0 중량부가 더욱 바람직하다. 만일 0.01 중량부 이하이면 피부 보습이 급격히 나빠지며, 5.0 중량부 이상일 경우 너무 끈적거려서 사용감이 나빠진다.Skin moisturizer in the soap composition of the present invention is to give a moisturizing effect to the skin, glycerin, erythritol, polyethylene glycol, propylene glycol, butylene glycol, pentylene glycol, hexyl glycol, isopropyl myristate, silicone derivatives, aloe vera , At least one selected from the group consisting of sorbitol, and glycerin is preferred in the present invention. The skin moisturizer contains 0.01 to 5.0 parts by weight, more preferably 0.1 to 2.0 parts by weight. If the amount is less than 0.01 parts by weight, the skin moisturizes rapidly, and if it is more than 5.0 parts by weight, it becomes too sticky and the feeling of use becomes worse.

본 발명의 비누 조성물에서 피부 유화제는 피부에 유연효과를 주기 위한 것으로, 천연오일, 왁스 지방알콜, 탄화수소류, 천연식물 추출물로 이루어진 군으로부터 선택된 1종 이상을 포함하며, 0.01 내지 5.0 중량부가 바람직하고, 0.1 내지 3.0 중량부가 더욱 바람직하다. 만일 0.01 중량부 이하이면 피부 유연상태가 급격히 나빠지며, 5.0 중량부 이상일 경우 너무 끈적거려서 사용감이 나빠진다.In the soap composition of the present invention, the skin emulsifier is used to give the skin a softening effect, and includes at least one selected from the group consisting of natural oils, wax fatty alcohols, hydrocarbons, and natural plant extracts, and preferably 0.01 to 5.0 parts by weight. , 0.1 to 3.0 parts by weight is more preferred. If the amount is less than 0.01 parts by weight, the softness of the skin is sharply worsened, and if it is more than 5.0 parts by weight, it is too sticky and the feeling of use becomes worse.

본 발명의 비누 조성물에서 경수연화제는 경수연화작용을 하는 것으로, 테트라소듐 이디티에이를 포함하며, 0.01 내지 2.0 중량부가 바람직하고, 0.05 내지 1.0 중량부가 더욱 바람직하다. 일반적으로 수돗물 및 지하수에는 중금속 및 각종 오염원이 되는 무기광물질이 함유되어 있어 비누를 사용하는 경우 물속의 금속 이온과 비누의 지방산이 결합하여 금속성 잔유물질이 피부에 남게 되기 때문에 피부를 거칠게 하는 동시에 세균번식 및 피부손상의 원인이 되는 문제점이 있는데, 이를 완화시켜주는 역할을 한다.In the soap composition of the present invention, the water softener has a water softening action, and includes tetrasodium idieti, preferably 0.01 to 2.0 parts by weight, more preferably 0.05 to 1.0 parts by weight. In general, tap water and groundwater contain heavy metals and inorganic minerals that can cause various pollutants. When soap is used, metal ions in the water and fatty acids of the soap are combined to leave metallic residues on the skin, making the skin rough and at the same time breeding bacteria. And there is a problem that causes skin damage, it serves to alleviate this.

또한, 항균제, 분산제, 거품억제제, 용매, 물때 방지제, 부식 방지제, 향료, 색소, 금속 이온봉쇄제, 산화방지제 및 방부제 등을 부가적으로 함유할 수 있다.In addition, antimicrobial agents, dispersants, antifoaming agents, solvents, scale inhibitors, corrosion inhibitors, fragrances, pigments, metal ion blocking agents, antioxidants and preservatives may be additionally contained.

본 발명의 비누 조성물은 공중위생시설, 학교, 단체급식시설, 식품제조공장, 일반가정 및 병원에서 유용하게 사용할 수 있다.Soap composition of the present invention can be usefully used in public health facilities, schools, group meal facilities, food manufacturing plants, homes and hospitals.

이하, 본 발명의 이해를 돕기 위하여 바람직한 실시예를 제시한다. 그러나 하기의 실시예는 본 발명을 보다 쉽게 이해하기 위하여 제공되는 것일 뿐, 실시예에 의해 본 발명의 내용이 한정되는 것은 아니다.Hereinafter, preferred examples are provided to aid in understanding the present invention. However, the following examples are merely provided to more easily understand the present invention, and the contents of the present invention are not limited by the examples.

실시예 : 비누의 제조 Example : Preparation of Soap

소지(팜유/팜핵류 : 6/4) 98.6 중량부, 트리클로산 3.0 중량부, 벤잘코늄 클로라이드(50%) 0.2 중량부, 키토산 0.3 중량부, 조조바 오일 0.2 중량부, 모노 소듐 코코일 글루타메이트 0.5 중량부, 글리세린 0.3 중량부, 테트라소듐 이디티에이 0.2 중량부를 혼합기에 혼합한 뒤, 일반 비누의 제조장치에 의해 성형 및 압출 공정을 거쳐 절단 및 형타하여 비누를 제조하였다.Soybean oil (Palm oil / Palm nucleus: 6/4) 98.6 parts by weight, 3.0 parts by weight of triclosan, 0.2 parts by weight of benzalkonium chloride (50%), 0.3 parts by weight of chitosan, 0.2 parts by weight of jojoba oil, 0.5 parts by weight of mono sodium cocoyl glutamate , 0.3 parts by weight of glycerin and 0.2 parts by weight of tetrasodium editie were mixed in a mixer, and then soap was manufactured by cutting and molding through a molding and extrusion process using a general soap manufacturing apparatus.

실험예 1 : 살균력 분석시험 Experimental Example 1 bactericidal power assay

비교예 1 및 2는 하기 표 1과 같은 성분으로 혼합하는 것을 제외하고는 실시예와 동일한 방법으로 비누를 제조하였다.Comparative Examples 1 and 2 were prepared in the same manner as in Example except for mixing with the components shown in Table 1.

(단위 : 중량부)(Unit: parts by weight) 실시예Example 비교예 1Comparative Example 1 비교예 2Comparative Example 2 소지(팜유/팜핵류:6/4)Possession (Palm oil / Palm nucleus: 6/4) 98.698.6 98.698.6 98.698.6 트리클로산Triclosan 0.30.3 0.30.3 -- 벤잘코늄 클로라이드(50%)Benzalkonium Chloride (50%) 0.20.2 -- -- 키토산Chitosan 0.30.3 0.30.3 0.30.3 조조바 오일Jojoba oil 0.20.2 0.20.2 0.20.2 모노 소듐 코코일 글루타메이트Mono Sodium Cocoyl Glutamate 0.50.5 0.50.5 0.50.5 글리세린glycerin 0.30.3 0.30.3 0.30.3 테트라소듐 이디티에이Tetrasodium ID 0.20.2 0.20.2 0.20.2

1) 살균력 분석시험1) Sterilization test

상기 실시예 및 비교예 1, 2에서 제조한 비누를 37℃ 항온배양기에서 24±3시간 동안 배양한 후, 미생물의 성장 균수와 살균력을 관찰하였다.After the soaps prepared in Examples and Comparative Examples 1 and 2 were incubated in a 37 ° C. incubator for 24 ± 3 hours, the growth bacteria and bactericidal activity of the microorganisms were observed.

결과는 표 2 및 표 3에 나타내었다.The results are shown in Table 2 and Table 3.

(단위 : cfu/㎖)(Unit: cfu / ml) 대장균Escherichia coli 살모넬라균Salmonella 황색포도상구균Staphylococcus aureus 일반세균General bacteria 실시예Example < 100<100 3.04×102 3.04 × 10 2 < 100<100 < 50<50 비교예 1Comparative Example 1 1.73×104 1.73 × 10 4 9.60×103 9.60 × 10 3 1.12×103 1.12 × 10 3 < 50<50 비교예 2Comparative Example 2 8.55×104 8.55 × 10 4 7.26×104 7.26 × 10 4 4.54×103 4.54 × 10 3 < 50<50 대조군Control 2.04×104 2.04 × 10 4 1.65×105 1.65 × 10 5 1.27×104 1.27 × 10 4 4.37×104 4.37 × 10 4

(단위 : %)(unit : %) 대장균Escherichia coli 살모넬라균Salmonella 황색포도상구균Staphylococcus aureus 일반세균General bacteria 실시예Example 99.999.9 99.899.8 98.598.5 99.999.9 비교예 1Comparative Example 1 91.591.5 94.294.2 91.291.2 99.999.9 비교예 2Comparative Example 2 58.158.1 66.066.0 64.364.3 99.999.9

표 2에 나타난 바와 같이, 본 발명의 비누 조성물이 비교예 1(트리클로산이 빠진 비누 조성물)과 비교예 2(트리클로산과 벤잘코늄 클로라이드가 모두 빠진 비누 조성물)의 비누 조성물 보다 잔존하는 미생물의 성장 균수가 적음을 알 수 있다.As shown in Table 2, the number of microbial growth bacteria remaining in the soap composition of the present invention was higher than that of Comparative Example 1 (soap composition lacking triclosan) and Comparative Example 2 (soap composition lacking both triclosan and benzalkonium chloride). It can be seen that less.

또한 표 3에 나타난 바와 같이, 본 발명의 비누 조성물에서 미생물 살균력이 현저히 높음을 확인하였다.In addition, as shown in Table 3, it was confirmed that the microbial bactericidal power in the soap composition of the present invention is significantly high.

따라서, 본 발명의 비누 조성물은 트리클로산과 벤잘코늄 클로라이드의 살균작용에 의해 살균효과가 우수함을 알 수 있다.Therefore, it can be seen that the soap composition of the present invention has an excellent bactericidal effect by the bactericidal action of triclosan and benzalkonium chloride.

실험예 2 : 보습효과 시험 Experimental Example 2 Moisturizing Effect Test

20대 ~ 30대 연령의 남녀 30명(남 10, 여 20)을 2개조로 나뉘어, 상기 실시예에 의해 제조한 비누를 사용하여 세안한 후, 1일 10회 15일간 피부의 보습력을 측정하였다.Thirty men and women (male 10, female 20) in their 20s to 30s were divided into two sets and washed with soap prepared according to the above example, and then the skin's moisturizing power was measured 10 times a day for 15 days. .

실험에 참여한 대상중 95% 이상이 촉촉하다고 응답하였다.More than 95% of the participants participated in the experiment.

따라서, 본 발명의 비누 조성물은 보습효과가 우수함을 알 수 있다.Therefore, it can be seen that the soap composition of the present invention is excellent in the moisturizing effect.

본 발명의 비누 조성물은 트리클로산과 벤잘코늄 클로라이드를 함유하므로써, 기존의 비누 조성물보다 현저히 향상된 살균효과와 우수한 보습력을 나타내는 작용효과가 있다.Since the soap composition of the present invention contains triclosan and benzalkonium chloride, there is an action effect showing a significantly improved bactericidal effect and excellent moisturizing power than conventional soap compositions.

Claims (6)

트리클로산, 벤잘코늄 클로라이드를 포함함을 특징으로 하는 비누 조성물Soap compositions characterized by comprising triclosan, benzalkonium chloride 제 1항에 있어서, 팜유/팜핵류를 6/4 또는 7/3의 비율로 혼합한 소지를 비누 기재로 사용하는 비누 조성물The soap composition according to claim 1, wherein a base obtained by mixing palm oil / palm nucleus in a ratio of 6/4 or 7/3 is used as a soap base. 제 1항에 있어서, 트리클로산은 0.01 내지 5.0 중량부를 포함함을 특징으로 하는 비누 조성물The soap composition of claim 1, wherein the triclosan comprises 0.01 to 5.0 parts by weight. 제 1항에 있어서, 벤잘코늄 클로라이드는 0.01 내지 5.0 중량부를 포함함을 특징으로 하는 비누 조성물The soap composition of claim 1, wherein the benzalkonium chloride comprises 0.01 to 5.0 parts by weight. 제 1항 내지 제 4항에 있어서, 피부 보습제, 유화제, 경수연화제를 포함함을 특징으로 하는 비누 조성물The soap composition according to any one of claims 1 to 4, comprising a skin moisturizer, an emulsifier, and a water softener. 제 1항 내지 제 5항에 의해 제조된 고형 비누Solid soap prepared according to claim 1
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