KR20000067510A - Mineral antibiotic rosin chip by using silver, charcoal, plastics and its manufacturing process - Google Patents

Mineral antibiotic rosin chip by using silver, charcoal, plastics and its manufacturing process Download PDF

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Publication number
KR20000067510A
KR20000067510A KR1019990015391A KR19990015391A KR20000067510A KR 20000067510 A KR20000067510 A KR 20000067510A KR 1019990015391 A KR1019990015391 A KR 1019990015391A KR 19990015391 A KR19990015391 A KR 19990015391A KR 20000067510 A KR20000067510 A KR 20000067510A
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South Korea
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silver
charcoal
water
solution
antibacterial
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KR1019990015391A
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Korean (ko)
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최귀분
최문규
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최귀분
최문규
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Priority to KR1019990015391A priority Critical patent/KR20000067510A/en
Publication of KR20000067510A publication Critical patent/KR20000067510A/en

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    • A—HUMAN NECESSITIES
    • A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47J—KITCHEN EQUIPMENT; COFFEE MILLS; SPICE MILLS; APPARATUS FOR MAKING BEVERAGES
    • A47J43/00—Implements for preparing or holding food, not provided for in other groups of this subclass
    • A47J43/20—Shapes for preparing foodstuffs, e.g. meat-patty moulding devices, pudding moulds
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00—Shaping or working of foodstuffs characterised by the products
    • A23P10/20—Agglomerating; Granulating; Tabletting
    • A23P10/25—Agglomeration or granulation by extrusion or by pressing, e.g. through small holes, through sieves or between surfaces
    • G—PHYSICS
    • G05—CONTROLLING; REGULATING
    • G05G—CONTROL DEVICES OR SYSTEMS INSOFAR AS CHARACTERISED BY MECHANICAL FEATURES ONLY
    • G05G1/00—Controlling members, e.g. knobs or handles; Assemblies or arrangements thereof; Indicating position of controlling members
    • G05G1/02—Controlling members for hand actuation by linear movement, e.g. push buttons
    • G—PHYSICS
    • G05—CONTROLLING; REGULATING
    • G05G—CONTROL DEVICES OR SYSTEMS INSOFAR AS CHARACTERISED BY MECHANICAL FEATURES ONLY
    • G05G5/00—Means for preventing, limiting or returning the movements of parts of a control mechanism, e.g. locking controlling member
    • G05G5/05—Means for returning or tending to return controlling members to an inoperative or neutral position, e.g. by providing return springs or resilient end-stops

Abstract

PURPOSE: An inorganic antibacterial resin chip and its preparation method are provided, which resin chip uses silver, charcoal and synthetic resin and is used to maintain the freshness of food. CONSTITUTION: The inorganic antibacterial resin chip is prepared by melting 100 g of silver; adding the melted silver to water and heating it with adding silver nitrate slowly to obtain silver solution; adding 20 g of sodium aluminate to the silver solution to neutralize acid, filtering it and evaporating water to obtain purified silver; dissolving 100 g of the purified silver in 300 ml of water, adding 500 g of oak charcoal to the solution, stirring the solution, drying it and pulverizing it to obtain silver ion antibacterial charcoal; and mixing about 600 g of the silver ion antibacterial charcoal with 5000 g of synthetic resin, injecting the mixture into an extruder, and extruding and cutting it.

Description

은과 숯 및 합성수지를 이용한 무기항균수지칩 및 그 제조방법{Mineral antibiotic rosin chip by using silver, charcoal, plastics and its manufacturing process}Inorganic antibacterial resin chip using silver, charcoal and synthetic resin and its manufacturing method {Mineral antibiotic rosin chip by using silver, charcoal, plastics and its manufacturing process}

본 발명은 정제된 은에 분쇄된 숯가루를 투입혼합한 다음 건조하고, 다시 분쇄하여 은이온 항균숯을 얻고, 상기 은이온 항균숯을 합성수지와 골고루 혼합한 다음 압출 절단하여 무기항균수지칩을 얻고, 상기 무기항균수지칩을 나이론 망속에 담아 물탱크나 산업용 폐수의 살균용으로 사용하거나 혹은 압출 성형하여 식품보관용기나 포장용 필림으로 사용케하므로 식품의 신선도를 장기간 유지시킬 수 있도록 한 것이다.The present invention is mixed with the crushed charcoal powder in purified silver, dried, and then pulverized again to obtain a silver ion antimicrobial charcoal, and evenly mixed with the silver ion antibacterial charcoal synthetic resin and then extruded cut to obtain an inorganic antibacterial resin chip In addition, the inorganic antimicrobial resin chip is put in a nylon net to be used for sterilization of water tanks or industrial wastewater or extruded to be used as a food storage container or a packing film so that the freshness of food can be maintained for a long time.

은(銀)은 자연항생제로서 은용액을 제조하여 복용하기도 하였으며, 지금까지 연구기관에서 실험한 결과를 보면 (銀)은 지상의 모든 단세포병균을 살균한다는 것으로 보고되고 있다.Silver (銀) is a natural antibiotic that was produced by taking a silver solution, and the results of the experiment so far (銀) is reported to kill all the single cell germs on the ground.

숯은 예로부터 우리조상들이 여러용도로 사용하여 왔으며 숯 1g의 표면적이 약100평 정도의 넓이로서 흡착력이 탁월하다고 보고 되고 있다.Charcoal has been used for many purposes by our ancestors since ancient times, and the surface area of 1g of charcoal is about 100 pyeong, which is reported to have excellent adsorptive power.

숯이 가진 원천은 수많은 구멍들이며 박테리아, 바이러스, 독소등을 흡수한다는 학설이 있으며, 주성분이 탄소로서 음전기가 많기 때문에 물질이 부패하는 것을 막아준다는 학설도 있다.There are many theories that charcoal has many holes and it absorbs bacteria, viruses, and toxins. There is also a theory that carbon contains a lot of negative electrons, which prevents material from decaying.

또한 예로부터 질산 은을 물의 소독 및 살균에 사용하였고, 구연산은 녹농균제거에 사용하였으며, 염화아연은 목제 방부제로 사용하여 왔던 사실로서 그 역활을 알 수가 있다.In addition, silver nitrate was used to disinfect and sterilize water, citric acid was used to remove P. aeruginosa, and zinc chloride was used as a wood preservative.

그러나 위생처리목적으로 사용한 항생제는 4급 암모늄으로부터 시작된 유기화합물이 주종을 이루면서 유기수은, 유기크롬산, 구리화합물 등으로서 이들은 인체에 독성 및 유전변이성의 유발로 인하여 그 사용을 법적으로 규제하고 있다.However, antibiotics used for sanitary treatment mainly consist of organic compounds originating from quaternary ammonium, and organic mercury, organic chromic acid, and copper compounds, which are regulated by law because of their toxicity and genetic variation.

따라서 생활하수처리장, 위생폐수처리장, 식품공장폐수처리장에서는 폐수방류시 의무적으로 대장균등을 살균하기 위하여 염소살균을 하게 되나 염소는 발암물질의 원인이 되고, 또한 생태계를 파괴한다는 지적과 함께 비경제적인 등의 문제점이 있는 것이었다.Therefore, in domestic sewage treatment plants, sanitary wastewater treatment plants, and food factory wastewater treatment plants, chlorine sterilization is mandatory to sterilize E. coli in wastewater discharge, but chlorine causes carcinogens and destroys the ecosystem. There was a problem.

본 발명을 이러한 종래의 제반문제점들을 시정하고자 은이온을 분쇄된 숯가루와 혼합 건조한 다음 분쇄하여 은이온 항균 숯을 얻고, 상기 은이온 항균숯을 수지와 혼합한 다음 압출 절단하여 무기항균수지칩을 얻고, 상기 항균칩을 이용하여 다양한 용도로 사용할 수 있도록 한 것이다.In order to correct the above problems of the present invention, silver ions are mixed with pulverized charcoal powder, dried and pulverized to obtain silver ions antibacterial charcoal, and the silver ions antibacterial charcoal is mixed with a resin and then extruded to cut inorganic antibacterial resin chips. It is to be used for various purposes by using the antimicrobial chip.

한 예로서 무기항균수지칩을 나일론 망속에 넣어 폐수속에 넣어두면 대장균이나 박테리아가 살균되고, 물탱크나 물고기의 수족관속에 넣어 두면 대장균 및 비브리오균등의 증식을 억제하고 살균작용을 하게 된다.As an example, put an inorganic antibacterial resin chip in a nylon net and put it in the waste water, so that E. coli or bacteria are sterilized. If it is put in a water tank or an aquarium of fish, it inhibits the growth of E. coli and Vibrio bacteria and sterilizes them.

또한 본 발명의 항균수지칩을 사출성형기에 투입하여 항균프라스틱용기를 만들어 사용하거나 식품포장용 항균필름을 제조하여 사용케 하므로서 식품의 보존목적으로 사용하는 방부제의 사용을 줄임과 동시에 식품의 부패를 방지하여 장기간 신선도를 유지시킬 수 있게 된다.In addition, by inserting the antimicrobial resin chip of the present invention into an injection molding machine to make an antimicrobial plastic container or to produce and use an antimicrobial film for food packaging to reduce the use of preservatives used for the preservation of food and at the same time to prevent corruption of food. Long-term freshness can be maintained.

은과 숯(탄소)및 수지에 결합하고 있는 산소는 항균금속의 촉매작용에 의하여 부분적으로 활성산소(O2+, O2-,O)로 전환되고 상기 활성산소는 오존, 과산화수소, 염소 등과 같은 강력한 살균작용을 하게 되는 것이다.Oxygen bound to silver, charcoal (carbon) and resin is partially converted into active oxygen (O 2+ , O 2- , O) by the catalytic action of antibacterial metals, and the active oxygen is converted into ozone, hydrogen peroxide, chlorine, etc. Strong sterilization will be.

이하 본 발명의 실시예를 공정별로 상세히 설명하면 다음과 같다.Hereinafter, an embodiment of the present invention will be described in detail by process.

(실시예 1)(Example 1)

제1공정1st process

은괴100g을 용융시키고, 용융된 은을 물속에 소립하여 용해조에 넣어서 질산은을 서서히 첨가하면서 가열하면 은용액이 얻어진다.A silver solution is obtained by melting 100 g of silver ingot, sintering the molten silver into water, placing it in a dissolution tank, and heating it while gradually adding silver nitrate.

상기 은용액에 알루민산소오다 20g을 첨가하여 산을 중화시키고, 여과한 다음 증발 농축시킨 후 냉각하게 되면 작은 결창의 은을 정제한다.20 g of sodium aluminate is added to the silver solution to neutralize the acid, filtered, concentrated by evaporation, and cooled to purify the small intestinal silver.

제2공정2nd process

물300ml에 제1공정에서 얻어진 결창된 은100g을 넣어 용해한 다음, 1000메쉬로 분쇄된 참나무숯가루 500g을 투입혼합한 다음 건조시키고, 건조된 결정체를 다시 1000메쉬정도로 분쇄하여 은이온 항균숯을 얻는다.100 g of the silver obtained in the first step was dissolved in 300 ml of water, and then 500 g of oak charcoal crushed into 1000 mesh were mixed and dried, and the dried crystals were pulverized to about 1000 mesh to obtain silver ion antibacterial charcoal. .

제3공정3rd process

PE수지 5000g에 제2공정에서 얻어진 은이온항균숯 600g을 골고루 혼합교반 후 교반된 수지를 압출기에 투입하여 압출, 절단하므로서 모래와 같은 작은 무기항균수지칩의 제조가 완성된다.After mixing and stirring 600 g of the silver ion antibacterial charcoal obtained in the second step to 5000 g of PE resin, the stirred resin is put into an extruder to be extruded and cut to prepare a small inorganic antibacterial resin chip such as sand.

(실시예 2)(Example 2)

제1공정1st process

은괴100g을 용융시키고, 용융된 은을 물속에 소립하여 용해조에 넣어서 질산은을 서서히 첨가하면서 가열하면 은용액이 얻어진다.A silver solution is obtained by melting 100 g of silver ingot, sintering the molten silver into water, placing it in a dissolution tank, and heating it while gradually adding silver nitrate.

상기 은용액에 알루민산소오다 20g을 첨가하여 산을 중화시키고, 여과한 다음 증발 농축시킨 후 냉각하게 되면 작은 결창의 은을 정제한다.20 g of sodium aluminate is added to the silver solution to neutralize the acid, filtered, concentrated by evaporation, and cooled to purify the small intestinal silver.

제2공정2nd process

물300ml에 제1공정에서 얻어진 결창된 은100g을 넣어 용해한 다음, 1000메쉬로 분쇄된 참나무숯가루 500g을 투입혼합한 다음 건조시키고, 건조된 결정체를 다시 1000메쉬정도로 분쇄하여 은이온 항균숯을 얻는다.100 g of the silver obtained in the first step was dissolved in 300 ml of water, and then 500 g of oak charcoal crushed into 1000 mesh were mixed and dried, and the dried crystals were pulverized to about 1000 mesh to obtain silver ion antibacterial charcoal. .

제3공정3rd process

제2공정에서 얻어진 은이온 항균숯을 물에 녹여 직물가공용 수지와 혼합한 다음 직물의 표면에 코팅되게 한 다음 열처리하게 되면 은이온 항균숯이 직물에 고착되어 항균성을 가진 직물을 얻을 수 있게 된다.The silver ion antimicrobial charcoal obtained in the second process is dissolved in water, mixed with a resin for fabric processing and then coated on the surface of the fabric, and then heat treated to obtain a fabric having antimicrobial properties by fixing the silver ion antibacterial charcoal to the fabric.

상기에서 얻어진 무기항균수지칩은 다음과 같은 작용을 하게 된다.The inorganic antibacterial resin chip obtained above has the following function.

즉 은과 숯 및 수지에 결합하고 있는 산소는 항균금속의 촉매작용에 의하여 부분적으로 활성산소(O2+, O2-,O)로 전환되고, 상기 활성산소는 오존, 과산화수소, 염소등과 같은 강력한 살균작용을 하게 된다.That is, oxygen bound to silver, charcoal, and resin is partially converted into active oxygen (O 2+ , O 2- , O) by the catalytic action of the antibacterial metal, and the active oxygen is ozone, hydrogen peroxide, chlorine, and the like. Strong sterilization will be performed.

또한 많은 기공을 가지고 있는 숯은 1g의 표면적이 약100평 정도의 면적으로서 흡착력이 우수하고, 수많은 기공에 은이온이 치환되어 있기 때문에 숯의 흡착력에 의해 유기물을 흡착하는 효과와 함께 항균작용이 더욱 우수하고 탈취효과도 있다.In addition, charcoal having many pores has an area of about 100 pyeong with a surface area of 1g, which is excellent in adsorption power, and since silver ions are substituted in many pores, the charcoal adsorption force allows the adsorption of organic matter and antibacterial effect. Excellent and deodorizing effect.

따라서 상기에서와 같이 강한 흡착력과 살균작용을 이용하여 다용도로 사용할 수도 있다.Therefore, it can also be used for various purposes by using a strong adsorption and sterilization as described above.

본 발명에서 얻어진 무기항균수지칩을 나일론망속에 넣고 지하수물탱크, 옥상물탱크, 수족관 등에 넣어 사용하게 되면 대장균, 비브리오균 등의 세균을 살균하고, 폐수처리장의 폐수처리에 사용하게 되면 역시 살균효과를 얻을 수 있게 된다.When the inorganic antibacterial resin chip obtained in the present invention is put in a nylon net and used in an underground water tank, a rooftop tank, an aquarium, etc., the bactericidal effect of E. coli, Vibrio bacteria, and the like is used when used in wastewater treatment of a wastewater treatment plant. Will be obtained.

상기에서 사용되는 무기항균수지칩의 량은 물100 L당 1kg정도의 량으로 넣어 두게 되면 짧은 시간내에 90%이상 살균되었을 뿐 아니라 인체에 무해한 것으로 측정되었다.The amount of the inorganic antibacterial resin chip used in the above was measured to be more than 90% sterilization in a short time and harmless to the human body when put in an amount of about 1 kg per 100 L of water.

또한 본 발명에서 얻어진 무기항균수지칩을 이용하여 항균수지필림을 제조한 다음 식품포장용으로 사용하게 되면 식품의 부패를 방지할 뿐 아니라 신선도를 장기간 유지시킬 수 있게 되므로 식품제조시 장기 보존을 위하여 사용하는 방부제 사용량을 줄일 수 있어 유익하다.In addition, if the antimicrobial resin film is prepared using the inorganic antibacterial resin chip obtained in the present invention and then used for food packaging, it is possible to prevent food spoilage and maintain freshness for a long time. It is beneficial because it can reduce the amount of preservatives used.

본 발명의 무기항균수지칩을 이용하여 프라스틱용기로 성형한 다음 용기로 사용하게 될 경우에도 용기내에 저장되는 각종 음식물을 장기간 신선한 상태로 보존할 수 있게 된다.Even when molded into a plastic container using the inorganic antibacterial resin chip of the present invention and then used as a container, it is possible to keep various foods stored in the container in a fresh state for a long time.

따라서 본 발명은 종래 소독약으로 주로 사용하여 왔던 염소대용으로 무기항균수지칩을 사용케 하므로서, 염소를 소독약으로 사용함에 따른 발암의 위험성을 줄일 수 있게 될뿐 아니라 환경, 생태계 파괴현상을 예방할 수 있게 된다.Therefore, the present invention allows the use of inorganic antibacterial resin chips for chlorine, which has been mainly used as a conventional disinfectant, thereby reducing the risk of carcinogenesis by using chlorine as a disinfectant, as well as preventing environmental and ecosystem destruction. .

또한 살균하고자하는 식품폐수나 위생처리장, 상수도물탱크, 수족관 등에 필요한 량을 침지시켜 두므로서 각종 세균들을 짧은 시간에 살균할 수 있어 효과적일 뿐 아니라 인체에 전혀 무해하며 또한 장기간 사용할 수 있어 경제적으로 매우 유리하다.In addition, by sterilizing the necessary amount of food waste water, sanitary treatment plant, tap water tank, aquarium, etc. to sterilize, it is possible to sterilize various germs in a short time. Very advantageous.

본 발명의 무기항균 수지칩을 이용하여 식품포장용기나 필름으로 제조사용할 경우 식품의 부패를 막을 뿐 아니라 장기간 음식물의 신선도를 유지시켜 주게 되는 등의 효과가 있는 것이다.When used as a food packaging container or film using the inorganic antibacterial resin chip of the present invention will not only prevent food corruption but also maintain the freshness of food for a long time.

Claims (3)

은괴 100g을 용융한 다음 물속에 소립하여 용해조에 넣고 질산 은을 서서히 첨가하면서 가열하므로서 은 용액을 얻고, 상기 은용액에 알루민산소다 20g을 넣어 산을 중화시키고 여과한 다음 증발시켜 작은 결창의 정제 은을 얻고, 상기 정제 은를 100g을 물 300ml에 넣어 용해한 다음, 분쇄된 참나무숯 500g을 다시 첨가하여 혼합교반하고 건조후 분쇄하여 은이온 항균숯을 얻고, 상기 은이온항균숯 약600g을 5000g의 합성수지와 혼합한 다음 압출기에 투입, 압출 절단하여 작은 알갱이의 무기항균수지칩을 얻는 것을 특징으로 하는 은과 숯 및 합성수지를 이용한 무기항균수지칩의 제조방법.100 g of silver ingot is melted and then sintered into water to obtain a silver solution by heating while gradually adding silver nitrate, and 20 g of sodium aluminate is added to the silver solution to neutralize the acid, filtered and evaporated to refine the small silver crystal. 100 g of the purified silver was dissolved in 300 ml of water, and then 500 g of crushed oak charcoal was added again to stir and mixed and dried to obtain silver ionic antibacterial charcoal, and about 600 g of the silver ionic antibacterial charcoal was mixed with 5000 g of synthetic resin. The method for producing inorganic antimicrobial resin chips using silver, charcoal and synthetic resin, characterized in that the mixing and then put into an extruder, extrusion cutting to obtain a small grain of inorganic antibacterial resin chips. 은괴 200g을 용융한 다음 물속에 소립하여 용해조에 넣고 질산 은을 서서히 첨가하면서 가열하므로서 은 용액을 얻고, 상기 은용액에 알루민산소다 20g을 넣어 산을 중화시키고 여과한 다음 증발시켜 작은 결창의 정제 은을 얻고, 상기 정제은 100g을 물 300ml에 넣어 용해한 다음, 미분쇄된 참나무숯 500g을 다시 첨가하여 혼합교반하고 건조후 분쇄하여 은이온 항균숯을 얻고, 상기 은이온항균숯 약600g을 5000g의 합성수지와 혼합한 다음 압출기에 투입, 압출 절단하여 얻는 것을 특징으로 하는 은과 숯 및 합성수지를 이용한 무기항균수지칩.After melting 200 g of silver ingot, it is sintered into water and dissolved in a dissolving tank to obtain a silver solution by heating while gradually adding silver nitrate. 20 g of sodium aluminate is added to the silver solution to neutralize the acid, filtered and evaporated. To obtain the tablet, dissolve 100 g in 300 ml of water, and then add 500 g of finely ground oak charcoal to stir and mix and dry and pulverize to obtain silver ion antibacterial charcoal, about 600 g of silver ion antibacterial charcoal and 5000 g of synthetic resin. Inorganic antibacterial resin chips using silver, charcoal and synthetic resin, characterized in that obtained by mixing and then extruded and extruded. 은괴 100g을 용융한 다음 물속에 소립하여 용해조에 넣고, 질산 은을 서서히 첨가하면서 가열하므로서 은용액을 얻고, 상기 은용액에 알루민산소다 20g을 넣어 산을 중화시키고, 여과한 다음 분쇄된 참나무숯 500g을 다시 첨가하여 혼합교반하고 건조후 분쇄하여 은이온항균숯을 얻고, 상기 은이온 항균숯을 물에 녹여 직물가공용 수지와 혼합한 다음 직물의 표면에 코팅되게 하여서 된 은이온항균숯을 이용한 직물가공방법.100 g of silver bullion is melted and then granulated in water and placed in a dissolution tank. A silver solution is obtained by heating while gradually adding silver nitrate, and 20 g of sodium aluminate is added to the silver solution to neutralize the acid, filtered, and then 500 g of crushed oak charcoal. After adding and stirring again, drying and pulverizing to obtain silver ion antimicrobial charcoal, dissolving the silver ion antimicrobial charcoal in water and mixing it with the fabric processing resin, and then coating the surface of the fabric and processing the fabric using silver ion antimicrobial charcoal. Way.
KR1019990015391A 1999-04-29 1999-04-29 Mineral antibiotic rosin chip by using silver, charcoal, plastics and its manufacturing process KR20000067510A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100311832B1 (en) * 1999-08-18 2001-11-03 장재석 Synthetic Fibre with the Properties of Antibiotics, Deorderising and Far-infrared Ray Emmision
KR20020060654A (en) * 2002-06-14 2002-07-18 김제하 Health functional artificial fiber in which silver powder is synthesized, and a manufacturing method thereof.
KR20040009218A (en) * 2002-07-19 2004-01-31 최명부 The Production of Functional Vinyl Using Charcoal, Yellow Soil and their Compostite
KR20040014105A (en) * 2002-08-09 2004-02-14 최명부 The Manufacture of PP silk using charcoal and silver
KR100478494B1 (en) * 2002-06-12 2005-05-17 황승수 Master batch containing silver colloid

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100311832B1 (en) * 1999-08-18 2001-11-03 장재석 Synthetic Fibre with the Properties of Antibiotics, Deorderising and Far-infrared Ray Emmision
KR100478494B1 (en) * 2002-06-12 2005-05-17 황승수 Master batch containing silver colloid
KR20020060654A (en) * 2002-06-14 2002-07-18 김제하 Health functional artificial fiber in which silver powder is synthesized, and a manufacturing method thereof.
KR20040009218A (en) * 2002-07-19 2004-01-31 최명부 The Production of Functional Vinyl Using Charcoal, Yellow Soil and their Compostite
KR20040014105A (en) * 2002-08-09 2004-02-14 최명부 The Manufacture of PP silk using charcoal and silver

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