KR20000050064A - The process of amino acid liquid compost from high concentration organic waste water and molasses - Google Patents

The process of amino acid liquid compost from high concentration organic waste water and molasses Download PDF

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KR20000050064A
KR20000050064A KR1020000025691A KR20000025691A KR20000050064A KR 20000050064 A KR20000050064 A KR 20000050064A KR 1020000025691 A KR1020000025691 A KR 1020000025691A KR 20000025691 A KR20000025691 A KR 20000025691A KR 20000050064 A KR20000050064 A KR 20000050064A
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tank
photosynthetic bacteria
high concentration
amino acid
concentration organic
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KR1020000025691A
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Korean (ko)
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김용성
송민헌
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김용성
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    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F7/00—Fertilisers from waste water, sewage sludge, sea slime, ooze or similar masses
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F11/00—Other organic fertilisers
    • C05F11/08—Organic fertilisers containing added bacterial cultures, mycelia or the like
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/40—Treatment of liquids or slurries
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00—Fertilisers characterised by their form
    • C05G5/20—Liquid fertilisers
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
    • Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Biochemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Biotechnology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Molecular Biology (AREA)
  • Fertilizers (AREA)

Abstract

PURPOSE: A method for preparing an amino acid liquid fertilizer with high quality is provided which is economical and contributes to the reduction of environmental pollution by reusing an industrial waster water containing high concentration organic materials and also using photosynthetic bacteria which is optimum in treating the organic material-containing waster water. CONSTITUTION: A method for preparing an amino acid liquid fertilizer comprises adding molasses to waste water containing high concentration organic materials to mix them together; oxidizing the mixture in an aeration bath; saccharifying the treated water with sulfuric acid in a saccharification bath; neutralizing the saccharified water with sodium carbonate in a neutralization bath; adding photosynthetic bacteria, to the treated water; irradiating an ultraviolet light to the mixture in an ultraviolet light-sterilization bath to sterilize pathogenic bacteria and activate the photosynthetic bacteria; and fermenting and aging the irradiated mixture using the photosynthetic bacteria.

Description

고농도 유기 물질 폐수와 당밀을 주제로 한 아미노산 액체 비료 제조 방법{The process of amino acid liquid compost from high concentration organic waste water and molasses}The process of amino acid liquid compost from high concentration organic waste water and molasses}

통상 액체 비료 제조 방법으로는 병원성 사상균을 살균하지 않고 자연 발효 숙성 제조 하거나 또는 살균을 하여 호기성 세균( Bacillus Bacteria) 등을 첨가한 후 대량의 공기를 공급하여 발효 숙성하고 있는 현실인바, 고농도 유기 물질 폐수에는 혐기성 세균인 광합성 세균이 아니고는 처리가 불가하며 많은 경비의 부담과 고 품질 및 대량 생산을 기대할 수 없었다.In general, liquid fertilizer manufacturing method does not sterilize pathogenic filamentous fungi, but it is a natural fermentation preparation or sterilization by adding aerobic bacteria (Bacillus Bacteria) and then fermenting and fermenting a large amount of air. No anaerobic bacteria, photosynthetic bacteria, could not be processed, and high cost and high quality and mass production could not be expected.

본 발명은 각종 산업체에서 발생되고 있는 고농도 유기 물질 폐수를 재활용하여 이를 농산물의 품질 개선을 위하여 광합성 세균을 이용한 고품질의 아미노산 액체 비료를 제조토록 함으로서 경제적 이점과 더불어 환경오염 감소 등에 일신된 효과를 제공하고자 하는 것이다.The present invention is to recycle high-concentration organic material wastewater generated in various industries and to produce high quality amino acid liquid fertilizer using photosynthetic bacteria to improve the quality of agricultural products. It is.

제1도는 본 발명 고농도 유기 물질 폐수와 당밀을 주제로 한 아미노산 액체 비료의 제조 공정도1 is a manufacturing process chart of the amino acid liquid fertilizer based on the present invention high concentration organic matter wastewater and molasses

도면의 주요 부호에 대한 설명Description of the main symbols in the drawings

1 당밀 저장조 2 축산 폐수 저장조1 Molasses reservoir 2 Livestock wastewater reservoir

3 식품 폐수 저장조 3a 이송 펌프3 Food Wastewater Reservoir 3a Transfer Pump

3b 이송 펌프 4 혼합 산화 폭기조3b transfer pump 4 mixed oxidizing aeration tank

5 혼합 산화 폭기조 5a 이송 펌프5 mixed oxidation aeration tank 5a transfer pump

6 브로와 7 분해 당화조6 bro and 7 decomposition saccharification tank

7a 교반기 7b 이송 펌프7a stirrer 7b transfer pump

8 중화조 8a 교반기8 neutralizer 8a stirrer

9 중화조 9a 이송 펌프9 Neutralizer 9a Transfer Pump

9b 교반기 10 자외선 살균조9b Stirrer 10 UV Sterilizer

11 보이러 12 발효조11 Boilers 12 Fermenters

12a 이송펌프 (순환용) 12b 이송 펌프12a transfer pump (for circulation) 12b transfer pump

13 숙성조 13a 이송 펌프13 Aging Bath 13a Transfer Pump

14 침전조 15 탈수기14 Sedimentation Tank 15 Dehydrator

15a 이송 펌프 16 미량 원소 혼합조15a transfer pump 16 trace element mixing tank

16a 교반기 17 미량 원소 혼합조16a Stirrer 17 Trace Elements Mixing Tank

17a 교반기 17b 이송 펌프17a stirrer 17b transfer pump

18 액체 비료 저장조 19 액체 비료 저장조18 Liquid Fertilizer Storage Tank 19 Liquid Fertilizer Storage Tank

본 발명은 식품, 수산, 축산, 축 분뇨, 두부, 우유, 기타 산업체에서 발생된 고농도 유기 물질폐수에 당밀을 첨가하여 혼합, 산화, 당화, 중화 후 자외선 조사(1000-1500 LUX)를 실시, 살균하며 광합성 세균(Thiospirillum, Rhodothiospirillum, 홍색비유황세균)을 폐수 혼합액에 첨가 후 발효, 숙성이 최대로 활성화되면 광합성 세균이 혼입 된 아미노산 액체 비료(비타민, 핵산, 성장 호르몬, 포도당)가 제조되어 이를 사용하면 작물에 흡수성이 빠르고, 뿌리도 충실해져 성장을 돕고, 재배된 과실 또는 야채의 맛, 색상, 신선도가 월등하며, 작물의 연작이 가능하고, 특히 냉해에도 강력한 효과가 있으며, 양질의 토양을 유지 할 수 있는 기대 효과를 유도한 것이다.The present invention adds molasses to high concentration organic matter wastewater generated from food, fisheries, livestock, livestock manure, tofu, milk, and other industries, and performs ultraviolet sterilization (1000-1500 LUX) after mixing, oxidation, saccharification, and neutralization. When the photosynthetic bacteria (Thiospirillum, Rhodothiospirillum, red non-sulfur bacteria) are added to the wastewater mixture and fermented and matured to the maximum, the amino acid liquid fertilizer (vitamin, nucleic acid, growth hormone, glucose) mixed with photosynthetic bacteria is prepared and used. Its fast absorbency in crops, its roots are enriched to support growth, the taste, color and freshness of cultivated fruits or vegetables are excellent, and it is possible to cultivate crops, especially in cold water, and to maintain good soil. It is expected to have the expected effect.

제 1실시 예First embodiment

고농도 유기 물질 폐수와 당밀을 주제로 한 아미노산 액체 비료의 제조 방법Manufacturing method of amino acid liquid fertilizer on the theme of high concentration organic matter wastewater and molasses

제 1도는 고농도 유기 물질 폐수와 당밀을 이용한 아미노산 액체 비료 재생 가공 공정도로서 당밀 저장조(1) 축산 폐수 저장조(2) 식품 폐수 저장조(3)에 원료 액을 이송 펌프(3a)로 각각 주입한다.FIG. 1 is a flow chart of amino acid liquid fertilizer regeneration process using high concentration organic matter wastewater and molasses.

이 때 제조 혼합 중량 비율은 당밀 2: 축산 폐수 4: 식품 폐수 4의 비율로 하여 이송 펌프(3b)로 혼합 산화 폭기조(4)(5)로 보내지며 부로와(6)를 작동하여 24시간 혼합 산화 폭기 하면 BOD 10,000 ppm가 5,000 ppm로 떨어진다.At this time, the weight ratio of the manufactured mixture is molasses 2: livestock wastewater 4: food wastewater 4, and is sent to the mixed oxidation aeration tank 4, 5 by the transfer pump 3b, and the broth 6 is operated for 24 hours. Oxidation aeration causes 10,000 ppm of BOD to drop to 5,000 ppm.

이 처리액을 이송 펌프(5a)로 분해 당화조(7)로 이송하여 PH가 3이 되도록 황산(H2SO4)을 주입 후 교반기(7a)를 2시간 작동 교반한다. 처리된 액체를 이송 펌프(7b)를 사용하여 중화조 (8)(9)로 보낸 후 탄산소다 (Na2CO3)를 첨가하여 PH가 7이 되도록 중화처리하며 교반기 (8a)(9b)를 2시간 작동 교반한다.The treatment liquid is transferred to the decomposition saccharification tank 7 by the transfer pump 5a, and sulfuric acid (H 2 SO 4 ) is injected to have a pH of 3, and then the agitator 7a is stirred for 2 hours. The treated liquid is sent to a neutralization tank (8) (9) using a transfer pump (7b), and then neutralized by adding sodium carbonate (Na 2 CO 3 ) to a pH of 7 and the agitator (8a) (9b) Stir for 2 hours of operation.

운전 초기에는 광합성 세균 500 ppm/ton과 미생물 성장소 (NH2)2CO3(0.02%), 인산제일칼륨(KH2PO4) (0.02%), 미강분 (0.02%),미네랄(0.01%), BIOTIN (0.02%)을 각각 자외선 살균조 상부로 투입하면서 중화된 처리수를 이송 펌프 (9a)로 자외선 살균조(1000-1500 LUX, 다단 향류식 유출기)(10)로 이송과 동시에 자외선 살균 조명을 실시하면 병원성, 사상균은 사멸되고 광 에너지를 기호하는 광합성 세균은 활성화되면서 자외선 살균조 배출구를 통하여 발효조(12)로 낙하 저장된다.In the early stages of operation, 500 ppm / ton of photosynthetic bacteria and microorganisms (NH 2 ) 2 CO 3 (0.02%), potassium phosphate (KH 2 PO 4 ) (0.02%), rice bran (0.02%), minerals (0.01%) ) And BIOTIN (0.02%) are added to the upper part of the UV sterilization tank, and the neutralized treated water is transferred to the UV sterilization tank (1000-1500 LUX, multi-stage counterflow type outlet) 10 with a transfer pump (9a). When the germicidal illumination is carried out, pathogenic, filamentous fungi are killed and photosynthetic bacteria that symbolize light energy are activated and dropped into the fermentation tank 12 through the ultraviolet sterilization outlet.

보이러(12)를 가동하여 발효조(12) 숙성조(13)의 액체의 온도가 30'C가 되도록 조절하여 발효조 (12)에는 하루에 한번 광합성 세균 500 ppm/ton을 첨가하여 5일간 계속하며 이송 펌프(12b)를 통하여 숙성조(13)로 보내지며 광합성 세균 50 ppm/ton을 2일간 첨가하여 숙성 완료 한다.Boiler 12 is operated to adjust the temperature of the liquid in the fermentation tank 12 and the aging tank 13 to 30'C. The fermentation tank 12 is added with 500 ppm / ton of photosynthetic bacteria once a day for 5 days. It is sent to the aging tank 13 through the transfer pump (12b) to complete the aging by adding 50 ppm / ton photosynthetic bacteria for 2 days.

숙성 완료 후, 이송 펌프(13a)를 통하여 침전조(14)로 보내지며 탱크 용량의 20% 정도를 발효조(12)로 반송하여 주고 80%의 량은 탈수기(15)로 탈수한다.After the aging is completed, it is sent to the settling tank 14 through the transfer pump 13a to return about 20% of the tank capacity to the fermentation tank 12 and the amount of 80% is dewatered by the dehydrator 15.

탈수된 처리수를 이송 펌프(15a)로 미량 원소 혼합조 (16)(17)로 이송하여 미량 원소 적정량을 첨가하여 교반기(16a)(17a)로 혼합 교반 후 이송 펌프(17b)로 광합성 세균이 혼용된 액체 아미노산 액체 비료를 저장조 (18)(19)로 이송 저장한다.The dehydrated treated water is transferred to the trace element mixing tank (16) (17) by the transfer pump (15a), an appropriate amount of trace elements is added, mixed and stirred by the stirrers (16a) (17a), and photosynthetic bacteria are transferred to the transfer pump (17b). Mixed liquid amino acid liquid fertilizer is transferred to reservoirs 18 and 19 for storage.

광합성 세균을 활용하여 생산된 유기질 액체 비료를 사용함으로써 토양의 산성화를 막고, 식물에 유익한 영양분 및 미생물의 공급으로 고품질의 농산물 증대에 기여하고, 각종 고농도 유기질 폐수를 원료로 하여 재활용함으로써 환경 오염을 줄이는데 일신된 효과를 보일 수 있다.By using organic liquid fertilizer produced using photosynthetic bacteria, it prevents acidification of soil, contributes to the increase of high quality agricultural products by supplying nutrients and microorganisms that are beneficial to plants, and reduces environmental pollution by recycling various high concentration organic wastewater as raw materials. The effect can be renewed.

Claims (1)

고농도 유기 물질 축산 폐수 4 : 고농도 유기 물질 식품 폐수 4 : 당밀 2의 중량 비율로 폭기조(4)(5)에서 혼합 산화 폭기하면 BOD 10,000 ppm이 BOD 5,000 ppm으로 수치가 감소한다.Mixed organic aeration in aeration tanks (4) (5) at a weight ratio of high concentration organic matter livestock wastewater 4: high concentration organic matter food wastewater 4: molasses 2: 10,000 ppm BOD is reduced to 5,000 ppm BOD. 이 처리수를 분해 당화조(7)에서 황산(H2SO4)을 첨가하여 PH3로 당화한 후 중화조(8)(9)에서 탄산소다 (Na2CO3)를 첨가 PH7로 중화한다.The treated water is saccharified with PH3 by adding sulfuric acid (H 2 SO 4 ) in the decomposition saccharification tank (7) and neutralized with sodium carbonate (Na 2 CO 3 ) with the addition PH7 in the neutralization tank (8) (9). 처리후 광합성 세균 500 ppm/ton과 미생물 성장소 (NH2)2CO3(0.02%), 인산제일칼륨(KH2PO4)(0.02%), 미강분 (0.02%),미네랄(0.01%), BIOTIN (0.02%)/ton을 각각 첨가하면서 5일간 연속하여 자외선 살균조 (다단 향류식 유출기)로 순환 살균하면 병원성 사상균은 사멸함과 동시에 광합성 세균을 활성화시킨다.After treatment, 500 ppm / ton of photosynthetic bacteria and microorganism growth point (NH 2 ) 2 CO 3 (0.02%), potassium phosphate (KH 2 PO 4 ) (0.02%), rice bran (0.02%), mineral (0.01%) After circulating sterilization with UV sterilization tank (multistage counterflow type outlet) for 5 consecutive days while adding BIOTIN (0.02%) / ton, respectively, pathogenic filamentous fungi are killed and photosynthetic bacteria are activated. 발효조(12)와 숙성조(13)의 액체 온도를 30'C로 유지시킨 후 침전조 (14)로 이송하여 탱크 용량의 20%의 량은 발효조(12)로 반송하여 주고 나머지 80%는 탈수기(15)로 탈수하여 미량 원소 혼합조(16)(17)로 보내지며 여기서 적정량의 미량 원소를 첨가 혼합하여 광합성 세균이 혼용된 아미노산 액체 비료를 저장조(18)(19)에 저장한다.The liquid temperature of the fermentation tank 12 and the aging tank 13 is maintained at 30'C and then transferred to the settling tank 14 to return 20% of the tank capacity to the fermentation tank 12 and the remaining 80% of the dehydrator ( 15) is dehydrated and sent to the trace element mixing tanks 16 and 17, where an appropriate amount of trace elements is added and mixed to store the amino acid liquid fertilizer mixed with photosynthetic bacteria in the storage tanks 18 and 19.
KR1020000025691A 2000-05-15 2000-05-15 The process of amino acid liquid compost from high concentration organic waste water and molasses KR20000050064A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20030016527A (en) * 2001-08-21 2003-03-03 윤창규 Production of microbial fertilizer from food waste and its microbial fertilizer
US7776124B2 (en) 2005-10-14 2010-08-17 Archer-Daniels-Midland Company Fertilizer compositions and methods of using
CN109265235A (en) * 2018-09-06 2019-01-25 广西桉盛丰肥业有限公司 Special fertilizer with insecticidal activity

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