KR20000009495A - Process for manufacturing onion beverage - Google Patents

Process for manufacturing onion beverage Download PDF

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Publication number
KR20000009495A
KR20000009495A KR1019980029950A KR19980029950A KR20000009495A KR 20000009495 A KR20000009495 A KR 20000009495A KR 1019980029950 A KR1019980029950 A KR 1019980029950A KR 19980029950 A KR19980029950 A KR 19980029950A KR 20000009495 A KR20000009495 A KR 20000009495A
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South Korea
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onion
cyclodextrin
grams
beverage
precipitation
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KR1019980029950A
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Korean (ko)
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정동옥
정순택
박양균
강성국
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정동옥
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Priority to KR1019980029950A priority Critical patent/KR20000009495A/en
Publication of KR20000009495A publication Critical patent/KR20000009495A/en

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/30Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2250/00Food ingredients
    • A23V2250/50Polysaccharides, gums
    • A23V2250/51Polysaccharide
    • A23V2250/5112Cyclodextrin

Abstract

PURPOSE: Stable onion beverage is manufactured by removing onion's specific smell not to generate precipitation for storage and marketing period by delaying formation of precipitation for long times in accordance with addition product without removing precipitable material in advance. CONSTITUTION: A process for manufacturing stable onion beverage in marketing period consisted of manufacturing onion extracts by adding purified water of 2-10 times to onion raw material weight by intercepting after peeling coat of onion after heating and extracting in 80-120°C for 0.5-3 hours, and amplexus reaction with agitation by adding cyclodextrine mixture to 1-5 weight% of onion extracts after agitating and dissolving for 10-30 minutes by adding purified water in cyclodextrine mixture.

Description

양파음료 제조방법Onion Beverage Manufacturing Method

본 발명은 침전을 방지할 수 있고 독특한 양파의 향을 부드럽게 할 수 있는 양파음료 제조 방법에 관한 것이다.The present invention relates to a method for producing an onion beverage that can prevent precipitation and soften the flavor of the unique onion.

양파는 호남의 주요 원예작물의 하나로서 전국생산량의 약 45%을 차지하고 있으며 특히, 전남 무안군은 우리나라의 최대 양파, 마늘 생산지로서 전국생산량의 25%를 생산하고 있다. 양파는 조생종과 만생종 두 종류가 생산되고 있는데 조생종은 4∼5월에 수확되나 저장성이 떨어지는 반면 6∼7월에 수확되는 만생종은 조생종에 비해 저장성이 큰 것으로 알려졌다. 양파는 다른 야채에 비하여 온도, 습도만 잘 조절되면 저장성이 좋은편이나 최근 2∼3년간 양파의 과잉생산으로 가격이 폭락하여 생산농가에 큰 경제적 타격을 주고 있다. 이에 반하여 양파의 생산량이 줄어들면 양파가격이 폭등하여 소비자 물가에 큰 영향을 주고 있으며 이와 같은 양파가격의 폭락, 폭등은 매년 3∼4년을 주기로 되풀이되고 있다. 양파가격의 안정을 위해서는 양파가공기술이 개발되어야 하며 양파의 수요를 일정하게 유지함으로써 안정적으로 양파가격파동을 막을 수 있다. 양파의 대량소비 및 수급조절을 위해서는 양파를 주원료로한 고급혼합음료의 개발이 필수적이다.Onion is one of the major horticultural crops in Honam, accounting for about 45% of the national production. In particular, Muan-gun, Jeonnam, is the country's largest onion and garlic producer, producing 25% of the national production. Two types of onions are produced, both early and late, which are harvested in April-May, but are inferior in shelf life. Onions are better in shelf life when temperature and humidity are better controlled than other vegetables, but the price has fallen due to overproduction of onions in the last two to three years. On the other hand, when onion production decreases, onion prices are soaring, which greatly affects consumer prices. Such plunge and soaring onion prices are repeated every three to four years every year. In order to stabilize onion prices, onion processing technology must be developed and onion price fluctuations can be stably prevented by keeping onion demand constant. In order to control the mass consumption and supply and demand of onions, it is essential to develop high quality mixed drinks with onion as the main ingredient.

양파는 육류의 냄새를 없애고 맛을 좋게 하는데 효과적이며, 신선한 양파나 양파 건조물육가공, 스우프류, 소오스류, 천연건조 조미료, 제과, 제빵 등의 식품가공의 중간소재로서 널리 사용되고 있다. 양파는 향신료 이외에 고대 이집트, 로마, 인도, 중국 등에서 마늘과 함께 약재로 사용되어 해열, 구충, 해독, 장염, 종양치료에 사용하였으며, 최근의 연구에서는 심혈관계 질환의 예방효과, 혈전증 치료효과, 혈당저하 효과, 항산화효과, 항균작용, 항진균작용 및 중금속 해독작용이 있다. 현재 양파의 이용방법은 생양파를 구입하여 가열 등의 방법으로 조리하여 식용하거나 독특한 매운맛과 향을 이용하기 위해 음식에 첨가하여 식용하는 것이 대부분이고, 식품가공용으로는 건조 양파면, 건조 양파분말, 양파식초 등으로 제조되며 가정에서는 양파 장아찌를 만들어 식용하여 왔을 뿐이다. 그러나 양파의 수요확대를 위해서는 양파를 소재로하는 새로운 가공식품의 개발이 절실히 요구되고 있다. 1990년에 들어서면서, 청량음료에서 재래식 건강음료에 대한 관심이 옮겨지면서 국내 농산물을 원료로한 건강 재래음료(식혜, 수정과, 대추, 양파, 마늘, 인삼, 당귀, 영지등)에 대한 수요가 매년 급격히 증가되고 있다. 이와 같은 관심을 기본으로 무안 양파를 주원료로한 고급 혼합음료를 개발하면 양파의 대량 소비가 가능하며 양파의 가격 안정화에 기여하게 되고 결국 양파 재배 농민들은 양파 재배로 안정적 수입을 얻을 수 있을 것이다. 그러나 양파음료는 기타 첨가물과의 상호반응, 용액의 pH등 여러 가지 요인에 의하여 장기간 보관 및 유통과정 중에서 혼탁이 발생되고 침전물이 생성되며 양파특유의 냄새 때문에 상품의 가치가 저하되고 있다. 이와 같은 상품의 가치를 저하시키는 침전물의 생성억제, 침전생성 가능물의 사전제거 또는 양파특유냄새 제거 등은 여러 가지 측면에서 시도되고 있지만 아직까지 획기적인 방법이 개발되지 않는 실정이다.Onion is effective in eliminating the smell of meat and improving the taste, and is widely used as an intermediate material for food processing such as fresh onion, onion dry meat processing, scoops, sauces, natural dry seasonings, confectionery, and baking. In addition to spices, onions are used as herbs in ancient Egypt, Rome, India, China, etc. with garlic to treat antipyretic, antiparasitic, detoxification, enteritis, and tumors. Recent research has shown that cardiovascular disease prevention, thrombosis, blood sugar It has a lowering effect, antioxidant effect, antibacterial effect, antifungal effect and heavy metal detoxification effect. Currently, onions are used to buy raw onions and cook them by heating, etc., or to add them to foods in order to use unique spicy and flavored foods. For food processing, dried onion noodles, dried onion powder, It is made of onion vinegar, etc., and only families have made onion pickles to eat. However, to increase the demand of onions, the development of new processed foods based on onions is urgently required. Entering the 1990s, the shift from interest in soft drinks to conventional health beverages shifted the demand for healthy beverages (Sikhye, fertilized fruit, jujube, onion, garlic, ginseng, Angelica, Ganoderma, etc.) made from domestic agricultural products. It is increasing rapidly every year. On the basis of such interests, developing high-quality mixed drinks based on Muan onions will enable the mass consumption of onions and contribute to stabilizing onion prices, and eventually onion farmers will be able to earn stable income from onion cultivation. However, onion beverages have turbidity during the long-term storage and distribution due to various factors such as interaction with other additives, pH of solution, precipitates are generated, and the value of commodities is deteriorated due to the smell of onion. Inhibition of sediment formation, preliminary removal of sediment formation possible, or removal of onion-specific odors, such as degrading the value of such commodities, has been attempted in various aspects, but no groundbreaking method has yet been developed.

미세여과, 초원심분리, 저온방치후 여과등의 방법은 침전생성가능물을 사전에 제거하는 방법이다. 이 방법은 제조 공정시설이 복잡해질뿐 아니라 공정시간이 길어져 비경제적이다. 침전의 미립자의 침강 외에도 화학적 반응에 따른 현상으로서 침전이 생성되기도 하므로 사전침전의 생성이 가능한 물질제거란 거의 불가능하다고 할수 가 있다. 그리고 정도의 차이는 있지만 이러한 과정을 거쳐 제조된 양파음료도 시간이 경과함에 따라 결국은 침전이 생성되게 된다.Microfiltration, ultracentrifugation, low temperature filtration and the like are the methods for removing precipitates in advance. This method is not only economical because the manufacturing process is complicated but also the process time is long. In addition to sedimentation of the fine particles of the precipitate, as a phenomenon caused by the chemical reaction, precipitation is generated, and thus it is almost impossible to remove the material capable of generating the presedimentation. And, although there is a difference in degree, the onion beverage prepared through this process will eventually generate a precipitate over time.

따라서 본 발명에서는 침전가능물질을 미리 제거하지 않고 첨가물질에 의하여 침전의 생성을 장기간 지연시킴으로서 저장, 유통기간중의 침전이 발생하지 않도록하고 양파특유의 냄새를 제거하여 안정된 양파음료 제조방법을 제공하여 용이한 방법으로 품질을 높이는데 목적이 있다.Therefore, the present invention does not remove the precipitable substances in advance, but by delaying the production of precipitates by the additives for a long time, so that precipitation during storage and distribution period does not occur, and by removing the smell peculiar to onions to provide a stable onion beverage manufacturing method The purpose is to increase the quality in an easy way.

양파음료는 양파를 주원료로 하여 여기에 감미제, 교미제 등을 첨가하여 액제로 하며 병 또는 캔 포장하여 제조한다. 여기에서 양파는 주로 물로 추출하여 추출물 그대로 사용하거나 혹은 농축하여 엑기스상의 것을 사용한다. 첨가제로는 시중에서 시판되고 있는 일반 드링크류와 유사하게 감미제로써는 백당, 포도당, 과당, 벌꿀 등이 교미제로써는 글루타민산나트륨, 염화나트륨 등이 산미제로는 구연산, 구연산나트륨, 사과산등이 방부제로는 안식향산나트륨, 파라핀계통의 물질들이 첨가제로써 사용된다.Onion drinks are prepared by adding onions as the main ingredients and adding sweeteners and copulation agents to the liquids and packing them into bottles or cans. The onion is mainly extracted with water and used as it is, or concentrated to extract. As an additive, similar to commercial drinks commercially available, white sugar, glucose, fructose and honey are sweeteners such as sodium glutamate and sodium chloride, and citric acid, sodium citrate and malic acid are antiseptics and sodium benzoate as an antiseptic. Paraffin-based materials are used as additives.

본 발명은 양파음료 제조에 있어서 침전생성에 대한 안정성을 높이고 양파특유의 향을 부드럽게 하기 위하여 싸이클로덱스트린을 사용하는 것을 특징으로 한다. 싸이클로덱스트린은 전분에 효소를 작용시켜 제조하는 가식성의 환상올리고당으로 특이한 포접작용이 있기 때문에 최근에 이에 대한 연구와 이용이 급속도로 증가하여 식품, 의약품, 화장품, 농약등의 분야에 이용되고 있는 제품이다. 또한 싸이클로덱스트린은 1976년 일본 후생성 식품화학과에 의해 천연식품 첨가물로 지정된 이래 많은 연구가 진행되었으며 국내에서는 1985년에 베타-싸이클로덱스트린 혼합물이 식품첨가물로 허가를 받았다.The present invention is characterized by the use of cyclodextrin to increase the stability to the precipitation production in the production of onion beverage and to soften the flavor unique to onions. Cyclodextrin is a edible cyclic oligosaccharide manufactured by enzyme action on starch. Because of its specific inclusion effect, cyclodextrin has recently been used in fields such as food, medicine, cosmetics, and pesticides due to its rapid increase in research and use. . In addition, since the cyclodextrin was designated as a natural food additive by the Ministry of Health, Food and Welfare in 1976, many studies have been conducted. In 1985, the beta-cyclodextrin mixture was approved as a food additive.

현재까지 알려진 싸이클로덱스트린의 용도는 의약품과 식품 분야가 대종을 이루고 있으며 의약품에서는 주로 베타-싸이틀로덱스트린과 의약품과의 포접반응에서 생성된 포접물을 부작용의 경감, 약효의 지속화, 안정성 증가등의 용도로 사용돠고 있다. 그러나 식품분야에서는 베타-싸이클로덱스트린이 사용되는 예도 있으나 가격이 고가임으로 싸이클로덱스트린 혼합물이 사용되는 경우가 많다. 싸이클로덱스트린의 사용목적은 향료, 향신료, 색소 등의 불안정한 첨가물 또는 성분 안정화제, 천연 유화제, 고미이취의 은폐제로서 이용된다. 싸이클로덱스트린의 특징은 이러한 성질을 포괄적으로 지니고 있다. 실제로 식품첨가물 중에는 각각의 특성을 갖는 물질은 많으나 유화제, 감미료, 안정화제, 중량부형제의 특성을 동시에 지닌 것이 싸이클로덱스트린의 장점이다.Cyclodextrins, which are known to date, are widely used in medicines and foods.In medicines, the inclusions of beta-cyclodextrins in the reaction between the drug and the drug are alleviated from side effects, continuity of drug efficacy, and stability. It is used for a purpose. However, the beta-cyclodextrin is used in the food field, but the cyclodextrin mixture is often used because of its high price. The purpose of the cyclodextrin is to be used as an unstable additive or ingredient stabilizer, natural emulsifier, high odor concealing agent such as perfume, spice and pigment. Cyclodextrins have a comprehensive set of properties. In fact, many food additives have their own characteristics, but they have the characteristics of emulsifiers, sweeteners, stabilizers, and weight excipients.

본 발명은 이러한 특성을 가진 싸이클로덱스트린중에서 가격이 저렴한 사이클로덱스트린 혼합물을 양파음료에 적용하여 장시간 보존시에 침전생성에 대한 안정도를 높이고 양파특유의 향을 부드럽게 해줌으로써 보다 안정화된 양파음료를 제조하였다.In the present invention, a cyclodextrin mixture having a low price among cyclodextrins having such characteristics is applied to onion beverages to produce more stabilized onion beverages by increasing the stability of sedimentation and softening the flavor of onions during long-term storage.

본 발명의 특징은 사이클로덱스트린 혼합물은 양파추출물과 반응시켜 안정화된 양파-싸이클로덱스트린 화합물을 제조하여 양파음료를 제조하거나 싸이클로덱스트린 혼합물을 배합공정중에 첨가하여 포접화 반응을 거쳐 양파음료의 안정화를 도모하는 것이다.A feature of the present invention is that the cyclodextrin mixture is reacted with onion extract to prepare a stabilized onion-cyclodextrin compound to prepare onion beverage or to add a cyclodextrin mixture during the compounding process to stabilize the onion beverage will be.

이상과 같은 양파음료의 제조방법은 공정별로 서술하면 다음과 갖다.The method of producing the onion drink as described above has the following description by process.

양파음료 제조공정예 1Onion beverage manufacturing process example 1

(1) 양파추출물의 제조공정 :(1) Onion extract manufacturing process:

원료양파의 외피를 박피한후 절편하여 양파원료 중량의 3∼10배량의 정제수를 가하고 85∼120℃에서 30분∼3시간정도 가열 추출한후 5마이크로∼1마이크로 필터로 여과하여 제조한다.The skin of the raw onion is peeled, then sliced, and purified water of 3 to 10 times the weight of onion is added, and extracted by heating at 85 to 120 ° C. for 30 minutes to 3 hours, followed by filtration with a 5 micro to 1 micro filter.

(2) 배합 및 포접화 반응공정 :(2) Mixing and Inclusion Reaction Process:

싸이클로덱스트린 혼합물 약 100그람에 정제수 1리터를 가하여 10∼30분 교반 용해한후 50∼80℃ 온도에서 1∼3킬로그람에 해당하는 양파추출물을 가하여 교반시켜 가면서 30∼2시간 반응시켜 포접화합물을 제조한다.1 liter of purified water was added to about 100 grams of cyclodextrin mixture, and then dissolved by stirring for 10 to 30 minutes. Then, the onion extract corresponding to 1 to 3 kilograms was added at 50 to 80 ° C. and stirred for 30 to 2 hours to prepare a clathrate compound. do.

(3) 배합공정 :(3) Mixing process:

일반적인 배합공정에 의거 배합조에 백당, 과당등의 감미료를 가하여 교반 가온 용해후 구연산, 구연산나트륨, 사과산등의 산미제를 용해하고 기타 교미제 및 방부제를 가하여 정제수로 전체적인 용량을 맞춘다.According to the general mixing process, sweeteners such as sucrose and fructose are added to the mixing tank, and after stirring and melting, acidic agents such as citric acid, sodium citrate and malic acid are dissolved, and other coagulants and preservatives are added to adjust the overall capacity with purified water.

양파음료 제조공정예 2Onion beverage manufacturing process example 2

(1) 양파추출물의 제조공정 : 제조공정예 1과 동일(1) Manufacturing process of onion extract: same as manufacturing process example 1

(2) 배합 및 포접화 반응 :(2) compounding and inclusion reaction:

일반적인 배합공정에 의거 배합조에 감미료, 산미제, 교미제, 방부제 및 양파추출물을 투입한후 80∼95℃에서 30분정도 교반후 전체용량의 0.1∼2%의 싸이클로덱스트린 혼합물을 가하며 30분∼2시간 정도 더 교반하여 포접화 반응을 시킨다. 이때 작업공정상의 특성에 따라 배합순서가 결정되어질 수 있다.According to the general mixing process, sweeteners, acidifiers, copulation agents, preservatives and onion extracts were added to the mixing tank, stirred at 80-95 ° C for 30 minutes, and then 0.1-2% of the cyclodextrin mixture was added. It is stirred for about a further time to cause the clathrate reaction. At this time, the mixing order may be determined according to the characteristics of the working process.

지금까지 시도되었던 침전 생성 방지법으로서는 안정화제로서 계면활성제의 첨가, 효소를 이용한 침전생성 가능물의 분해, 추출물의 초원심분리, 초밀입자 여과, 용매를 첨가한 석출된 침전의 제거, 이온교환수지나 칼람 충진제를 통한 분리등의 방법이 검토되었거나 어느것도 제제화에 적절히 이용된 예는 없다. 이 방법들이 어느 정도의 효과는 있다하더라도 우선 비경제적이었다. 이러한 관점에서 본 발명에 사용된 싸이클로덱스트린 혼합물은 경제적으로도 어느정도 만족을 주며 양파의 특유한 향을 부드럽게 해주면서 침전의 생성을 상당한 기간동안 방지할 수 있다. 본 발명의 침전생성 지연 효과는 다음의 실시예들에서 확인하였다.As attempts to prevent precipitation, attempts have been made to add surfactants as stabilizers, to decompose precipitates using enzymes, ultracentrifugation of extracts, ultrafiltration of ultrafine particles, removal of precipitated precipitates with solvents, ion exchange resins or columns Methods of separation through fillers, etc. have been reviewed or none have been properly used in the formulation. Although these methods had some effect, they were uneconomic at first. In this respect, the cyclodextrin mixture used in the present invention is economically satisfactory to some extent and can soften the distinctive flavor of the onion while preventing generation of precipitation for a considerable period of time. Precipitation delaying effect of the present invention was confirmed in the following examples.

< 실시예 1 ><Example 1>

(1) 처방(1) prescription

내용물contents 100미리리터중Of 100 milliliters 양파추출물고과당시럽벌꿀싸이클로덱스트린액구연산구연산나트륨글루타민산나트륨염화나트륨안식향산나트륨정제수Onion Extract High Fructose Syrup Honey Cyclodextrin Liquid Citric Acid Sodium Citrate Sodium Glutamate Sodium Chloride Sodium Benzoate 20그람12그람1 그람300미리그람(500미리그람, 1그람)120미리그람40미리그람40미리그람20미리그람50미리그람적량20 grams 12 grams 1 gram 300 grams (500 grams, 1 gram) 120 milligrams 40 milligrams 40 milligrams 20 milligrams 50 milligrams

(2) 양파음료 제조(2) Onion Beverage Manufacturing

1) 싸이클로덱스트린 혼합물 30그람, 50그람, 100그람을 각각 정제수 500미리리터에 용해후 교반한다1) Dissolve 30 grams, 50 grams and 100 grams of cyclodextrin mixture in 500 milliliters of purified water and stir.

2) 여기에 양파추출물 2킬로그람을 70℃에서 서서히 투입하면서 1시간 동안 교반한다. 대조치로서 싸이클로덱스트린 혼합물을 사용하지 아니한 양파추출물만을 준비한다.2) To this, add 2 kilograms of onion extract at 70 ° C and stir for 1 hour. Prepare only the onion extract without the cyclodextrin mixture as a control.

3) 따로 고과당시럽 1200그람에 정제수 5리터를 가하여 95℃까지 올려 가온 용해후 서서히 냉각시켜 70℃까지 온도를 낮춘다.3) Separately, add 5 liters of purified water to 1200 grams of high fructose syrup, raise it to 95 ℃, cool it slowly, and slowly cool it to 70 ℃.

4) 3)의 용액에 벌꿀 100그람, 구연산 12그람, 구연산나트륨 42그람, 글루타민산나트륨 42그람, 염화나트륨 2그람, 안식향산나트륨 52그람을 가하여 교반 용해시킨다.4) Add 100 grams of honey, 12 grams of citric acid, 42 grams of sodium citrate, 42 grams of sodium glutamate, 2 grams of sodium chloride, and 52 grams of sodium benzoate to the solution of 3).

5) 2)의 양파추출물과 싸이클로덱스트린 혼합물의 포접화물을 4)의 용액에 가하고 충분히 교반시킨후 정제수로 전체용량을 10리터로 맞춘다. 대조치에는 양파추출물만을 가하고 정제수를 가하여 10리터로 한다.5) Add the clathrate of the onion extract of 2) and the cyclodextrin mixture to the solution of 4), stir well, and adjust the total volume to 10 liters with purified water. To the control value add only onion extract and purified water to make 10 liters.

(3) 안정성 실험(3) stability test

상기와 같이 제조한 4종류의 양파음료에 대하여 실온 및 40℃의 인큐베이타에 보관하면서 침전생성에 따른 경시변화를 관찰한 결과 다음 표 1, 표 2 와 같은 결과를 얻었다.The four kinds of onion beverages prepared as described above were stored in an incubator at room temperature and 40 ° C., and the change over time according to precipitation was obtained. The results shown in Table 1 and Table 2 were obtained.

표 1. 실온에서의 경시변화Table 1. Changes over time at room temperature

구분시간(개월)Division time (month) 싸이클로덱스트린 혼합물 300㎎Cyclodextrin mixture 300 mg 싸이클로덱스트린 혼합물 500㎎Cyclodextrin Mix 500 mg 싸이클로덱스트린 혼합물 1g1 g cyclodextrin mixture 대조치Contrast 00 -- -- -- -- 1One -- -- -- -- 22 -- -- -- -- 33 -- -- -- ±± 44 -- -- -- ±± 66 -- -- -- ++ 88 ±± -- -- ++ 1010 ±± ±± -- ++++ 1212 ++ ±± -- ++++

- : 침전이 없는 상태, ± : 육안으로 자세히 관찰한때 약간의 침전이 있는 상태,-: No precipitation, ±: slight precipitation when visually observed

+ : 완전히 육안으로 침전이 확인되는 상태, ++ : 성당량의 침전이 생성된 상태.+: Completely visible precipitation, ++: Cathedral yield.

표 2. 40℃에서의 경시변화Table 2. Changes over time at 40 ℃

구분시간(일)Division time (days) 싸이클로덱스트린 혼합물 300㎎Cyclodextrin mixture 300 mg 싸이클로덱스트린 혼합물 500㎎Cyclodextrin Mix 500 mg 싸이클로덱스트린 혼합물 1g1 g cyclodextrin mixture 대조치Contrast 00 -- -- -- -- 55 -- -- -- -- 1010 -- -- -- -- 1515 -- -- -- -- 2020 -- -- -- ±± 2525 -- -- -- ++ 3030 -- -- -- ++ 3535 -- -- -- ++++ 4040 ±± -- -- ++++ 4545 ±± -- -- ++++ 5050 ±± -- -- ++++ 5555 ++ ±± -- ++++ 6060 ++ ±± -- ++++

표 1, 2에서와 같이 실온 및 40℃에서 사이클로덱스트린 혼합물을 사용한 경우와 사용하지 않은 대조치는 침전 생성물에 안정성에 있어 현저한 차이가 있음을 알 수 있다. 특히 1그람을 사용할 경우 40℃에서 60일, 실온에서 12개월 경과시에도 침전생성을 확인할 수 없었다.As shown in Tables 1 and 2, the control and unused cyclodextrin mixtures at room temperature and 40 ° C. showed significant differences in stability in the precipitated products. Particularly, when 1 gram was used, precipitation could not be confirmed even after 60 days at 40 ° C. and 12 months at room temperature.

< 실시예 2 ><Example 2>

(1) 처방 : 실시예 1과 동일한 처방으로 실시하였다.(1) Prescription: The same prescription as in Example 1 was carried out.

(2) 양파음료 제조 :(2) Onion Beverage Manufacturing:

1) 고과당시럽 1200그람에 정제수 5리터를 가하여 95℃까지 올려 가온 용해후 서서히 냉각시켜 70℃까지 온도를 낮춘다.1) Add 5 liters of purified water to 1200 grams of high fructose syrup.

2) 1)의 용액에 벌꿀 100그람, 구연산 12그람, 구연산나트륨 4그람, 글루타민산나트륨 4그람, 염화나트륨 2그람, 안식향산나트륨 5그람을 가하여 교반 용해시킨다.2) Add 100 grams of honey, 12 grams of citric acid, 4 grams of sodium citrate, 4 grams of sodium glutamate, 2 grams of sodium chloride, and 5 grams of sodium benzoate to the solution in 1).

3) 싸이클로덱스트린 혼합물 30그람, 50그람, 100그람을 각각 2)의 용액에 교반 용해시킨다. 대조치에는 싸이클로덱스트린 혼합물을 가하지 않는다.3) 30 grams, 50 grams and 100 grams of the cyclodextrin mixture were dissolved in the solution of 2) by stirring. No control is added to the cyclodextrin mixture.

4) 양파추출물 2킬로그램을 3)에 서서히 투입하면서 1시간동안 교반하여 포접화 반응을 시킨후 정제수를 가하여 전체용량을 10리터로 한다.4) Add 2 kilograms of onion extract to 3) and stir for 1 hour to allow inclusion reaction. Add purified water to make 10 liters total volume.

(3) 안정성 실험(3) stability test

상기와 같이 제조한 4종류의 양파음료를 실시예 1의 안정성 실험과 동일한 방법으로 실시하였다. 그 결과는 표 3, 표 4와 같고 실시예 1과 거의 같은 결과를 얻었다.Four types of onion beverage prepared as described above was carried out in the same manner as the stability experiment of Example 1. The result was as Table 3 and Table 4, and the same result as Example 1 was obtained.

표 3. 실온에서의 경시변화Table 3. Changes over time at room temperature

구분시간(개월)Division time (month) 싸이클로덱스트린 혼합물 300㎎Cyclodextrin mixture 300 mg 싸이클로덱스트린 혼합물 500㎎Cyclodextrin Mix 500 mg 싸이클로덱스트린 혼합물 1g1 g cyclodextrin mixture 대조치Contrast 00 -- -- -- -- 1One -- -- -- -- 22 -- -- -- -- 33 -- -- -- ±± 44 -- -- -- ±± 66 -- -- -- ++ 88 ±± ±± -- ++ 1010 ±± ±± -- ++++ 1212 ++ ±± -- ++++

- : 침전이 없는 상태, ±: 육안으로 자세히 관찰한때 약간의 침전이 있는 상태,-: No precipitation, ±: slight precipitation when visually observed

+ : 완전히 육안으로 침전이 확인되는 상태, ++ : 성당량의 침전이 생성된 상태.+: Completely visible precipitation, ++: Cathedral yield.

표 4. 40℃에서의 경시변화Table 4. Changes over time at 40 ℃

구분시간(일)Division time (days) 싸이클로덱스트린 혼합물 300㎎Cyclodextrin mixture 300 mg 싸이클로덱스트린 혼합물 500㎎Cyclodextrin Mix 500 mg 싸이클로덱스트린 혼합물 1g1 g cyclodextrin mixture 대조치Contrast 00 -- -- -- -- 55 -- -- -- -- 1010 -- -- -- -- 1515 -- -- -- -- 2020 -- -- -- ±± 2525 -- -- -- ++ 3030 -- -- -- ++ 3535 -- -- -- ++++ 4040 ±± -- -- ++++ 4545 ±± -- -- ++++ 5050 ±± ±± -- ++++ 5555 ++ ±± -- ++++ 6060 ++++ ±± -- ++++

< 실시예 3 ><Example 3>

(1) 처방 :(1) Prescription:

실시예 1과 동일한 싸이클로덱스트린 혼합물의 사용량은 500미리그람으로 하였으며 대조치에는 싸이클로덱스트린 혼합물을 사용하지 않았다.The same cyclodextrin mixture as in Example 1 was used at 500 mg and no control was used for the cyclodextrin mixture.

(2) 양파음료 제조 :(2) Onion Beverage Manufacturing:

실시예 1의 제조방법과 동일하게 실시하였으며 2)항에서의 양파추출물과 싸이클로덱스트린 혼합물과의 반응 온도만을 달리하여 각각 10℃, 30℃, 50℃,70℃, 90℃에서 실시하였다.It was carried out in the same manner as in the production method of Example 1 and was carried out at 10 ℃, 30 ℃, 50 ℃, 70 ℃, 90 ℃ by varying only the reaction temperature of the onion extract and the cyclodextrin mixture in 2).

(3) 안정성 실험(3) stability test

상기와 같이 제조한 6종류의 양파음료를 40℃인큐베이타에 보관하여 60일간 보관하면서 침전이 육안으로 관찰되기까지의 경과일수를 5일 간격으로 측정한 결과 싸이클로덱스트린 혼합물을 첨가한 5종류는 거의 모두 55일만에 침전이 확인되었으며 싸이클로덱스트린 혼합물을 사용하지 않는 대조치보다는 약 3배가 연장되었다.The six kinds of onion beverages prepared as described above were stored at 40 ° C. incubator for 60 days, and the number of days until the sediment was observed visually was measured at five days intervals. Almost all of the precipitate was confirmed in 55 days and was about three times longer than the control without the cyclodextrin mixture.

양파추출물에 싸이클로덱스트린 혼합믈을 첨가하여 양파음료를 제조함으로써 유통과정중 일어나는 침전생성 속도를 현저히 지연시킬 수 있어 양파음료의 품질의 안정화를 도모할 수 있다.By adding a cyclodextrin mixture to the onion extract to prepare the onion beverage can significantly delay the rate of precipitation occurs during the distribution process can be stabilized the quality of the onion beverage.

Claims (1)

양파의 외피를 박피한 후 절편하여 양파원료 중량의 2~10배의 정제수를 가하고 80~120℃에서 0.5~3시간 가열 추출한 후 5~1 마이크로필터로 양파추출물을 제조하는공정과 싸이클로덱스트린 혼합물에 정제수를 가하여 10~30분 교반용해한 후 싸이클로덱스트린 혼합물을 양파추출물의 1~5 중량% 첨가하여 교반하면서 0.5~2시간 포접반응시키는 것을 특징으로 하는 양파음료 제조방법.Peel the outer skin of the onion and slice it, add 2 ~ 10 times purified water of onion raw material, heat extract it for 0.5 ~ 3 hours at 80 ~ 120 ℃, and prepare onion extract with 5 ~ 1 micro filter and cyclodextrin mixture. Method of producing an onion beverage, characterized in that by adding purified water and stirring for 10 to 30 minutes, the cyclodextrin mixture is added by 1 to 5% by weight of onion extract and stirred for 0.5 to 2 hours while stirring.
KR1019980029950A 1998-07-24 1998-07-24 Process for manufacturing onion beverage KR20000009495A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20020028974A (en) * 2002-02-27 2002-04-17 최병수 The drink carbonic of onion
KR20030008110A (en) * 2001-07-16 2003-01-24 유논수 a making method for drink
KR20030024041A (en) * 2001-09-15 2003-03-26 (주)늘푸른샘 Preparation of a beverage containing onion and garlic extracts
KR20030024040A (en) * 2001-09-15 2003-03-26 (주)늘푸른샘 Preparation of a beverage containing an onion extract
KR100402418B1 (en) * 2000-03-28 2003-10-22 한국식품개발연구원 Manufacturing Method for Deodorized and Clarified Onion Beverage Using Organic Acids
KR100757674B1 (en) * 2006-06-14 2007-09-10 조남철 Manufacturing method of granules comprised onion extract

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100402418B1 (en) * 2000-03-28 2003-10-22 한국식품개발연구원 Manufacturing Method for Deodorized and Clarified Onion Beverage Using Organic Acids
KR20030008110A (en) * 2001-07-16 2003-01-24 유논수 a making method for drink
KR20030024041A (en) * 2001-09-15 2003-03-26 (주)늘푸른샘 Preparation of a beverage containing onion and garlic extracts
KR20030024040A (en) * 2001-09-15 2003-03-26 (주)늘푸른샘 Preparation of a beverage containing an onion extract
KR20020028974A (en) * 2002-02-27 2002-04-17 최병수 The drink carbonic of onion
KR100757674B1 (en) * 2006-06-14 2007-09-10 조남철 Manufacturing method of granules comprised onion extract

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