KR20000001727A - Manufacturing method for illite nylon filament yarn - Google Patents

Manufacturing method for illite nylon filament yarn Download PDF

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Publication number
KR20000001727A
KR20000001727A KR1019980022119A KR19980022119A KR20000001727A KR 20000001727 A KR20000001727 A KR 20000001727A KR 1019980022119 A KR1019980022119 A KR 1019980022119A KR 19980022119 A KR19980022119 A KR 19980022119A KR 20000001727 A KR20000001727 A KR 20000001727A
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South Korea
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illite
manufacturing
filament yarn
fiber
nylon filament
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KR1019980022119A
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Korean (ko)
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KR100407219B1 (en
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문태수
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문태수
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Publication of KR20000001727A publication Critical patent/KR20000001727A/en
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Publication of KR100407219B1 publication Critical patent/KR100407219B1/en

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    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/58—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products
    • D01F6/60—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products from polyamides
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00—Formation of filaments, threads, or the like
    • D01D5/08—Melt spinning methods
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • D01F1/103—Agents inhibiting growth of microorganisms

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Artificial Filaments (AREA)

Abstract

PURPOSE: A manufacturing method for an illite nylon filament yarn is provided to increase an antibacterial, an anti-fungal and an adsorption of hazardous gas. CONSTITUTION: A manufacturing method for an illite nylon filament yarn comprises: a master batch formed by mixing 10¯30 wt% of illite powder fine-powdered to 1¯2 micron with a polyamide chip for manufacturing a fiber; mixing the master batch with the polyamide chip for manufacturing the fiber in weight ratio of 10:90; inserting the mixture to a rotary dryer for dehydrating by rotating and heating at a temperature of 110¯130°C for 25¯30 minutes; inserting the dried mixture into a spinning hopper for cooling by melt spinning to air in state of 285¯293°C of inner temperature of a screw spinner; and drawing for 1.3¯1.5 times for maintaining 0.7¯2.3 wt% of the content of the illite element.

Description

일라이트 나일론 필라멘트사 제조방법Manufacturing method of illite nylon filament yarn

본 발명은 항균성과 항곰팡이성 및 유해가스 흡착성이 특히 높은 일라이트를 미세분말로 만들어 폴리아미드칩에 혼합하여 마스터베치를 제조하고 이를 합성섬유 제조용 폴리아미드칩과 10 : 90 중량%로 혼합하여 가열건조시킨 다음 방사용 호-퍼에 넣고 공기중에 용융방사하여 냉각시킨후 1.3 - 1.5배로 연신하여 일라이트 나일론 필라멘트사를 제조함으로서 항균성과 항곰팡이성 및 유해가스 흡착기능이 있는 나일론사를 제조하고 이를 이용하여 의류나 생활용품을 제조할 수 있게 한 것이다.The present invention is made of fine powder made of illite having high antibacterial, anti-fungal and noxious gas adsorption, into a fine powder to prepare a masterbatch and heat it by mixing it with a polyamide chip for synthetic fiber manufacturing at 10: 90% by weight. After drying, it is put in a spinning hopper and melt-spun in air, cooled, and stretched 1.3-1.5 times to prepare an illite nylon filament yarn, thereby preparing nylon yarn having antibacterial, anti-mildew and harmful gas adsorption function. It is to be able to manufacture clothes or household goods.

일라이트(illite)[KAℓ4(AℓSi7O20)(OH4)]는 점토광물로서 바이오세라믹과 같이 원적외선과 음이온을 방출하므로 공기중에서 세균의 번식을 억제하고 살균하는 항균성과 곰팡이의 번식을 억제하고 곰팡이를 죽여 악취의 발생을 막고 냄새를 제거하는 항곰팡이성을 가지고 있으면서 일라이트에서 방출되는 원적외선은 인체에 가장 좋은 5∼20파장범위에 속하는 원적외선이기 때문에 인체에 깊숙이 침투하여 신진대사를 촉진해주고 혈액순환을 좋게 하여 효소의 생성을 부활시키고 노화된 세포를 활성화시켜 인체내의 노폐물과 잉여지방질의 배설을 촉진시키는 작용을 하는 것으로 알려져 있고 유해가스의 흡착제거 성능도 우수한 물질로 이미 확인이 되어 있다.Illite [KAℓ 4 (AℓSi 7 O 20 ) (OH 4 )] is a clay mineral that emits far-infrared rays and anions like bioceramic. And far-infrared rays emitted from illite while preventing the occurrence of odors by killing molds and removing odors, are far-infrared rays within the range of 5-20 wavelengths, which is the best for the human body. It improves blood circulation, revitalizes the production of enzymes and activates aged cells to promote the excretion of waste and excess fats in the human body.

그러므로 이를 섬유에 혼합하여 의류나 생활용품을 제조하게 되면 인체에 원적외선을 방사하여 신진대사를 촉진시켜주고 세포활성화를 통해 피로회복 및 성인병 예방에 기여할 수 있는 등의 각종 효과를 낼 수 있고 인체에 가해지는 각종의 유해가스도 흡착제거 하여 인체를 보호하는 역할을 할 수 있다.Therefore, the manufacture of clothing or household goods by mixing them with fibers can produce various effects such as radiating far infrared rays to the human body to promote metabolism and contribute to recovery of fatigue and prevention of adult diseases through cell activation. It can also serve to protect human body by adsorption and removal of various harmful gases.

그러므로 종래에도 맥반석을 비롯하여 바이오세라믹과 같은 물질을 섬유제조에 이용하는 것이 공지되어 있는 실정이고 이건 출원인은 폴리에스텔사에 일라이트를 혼합하여 직물지를 제조하는 방법과 그 섬유에 대한 특허출원을 해 놓고 있다.Therefore, conventionally, it is known to use materials such as elvan and bioceramic for the manufacture of fibers, and the applicant has filed a patent for a method of manufacturing textile paper by mixing elite with polyester yarn and its fibers. .

그러나 종래 바이오세라믹 함유섬유는 바이오세라믹이 20여종의 금속물질과 점토를 혼합하여 1500℃로 가열하여 분말로 가공하여 만든 것을 사용하므로 분말의 입자가 상당히 크기 때문에 섬유에 혼입하게 되면 섬유의 절사를 초래하여 세장한 함유로 만들수가 없는 문제점이 있었고 이를 해소하기 위해 바이오세라믹의 량을 적게 하면 원적외선의 방출효과가 미미하여 소망하는 효과를 거둘수가 없는 불편이 있었으며 가격도 고가로 되는 문제점이 있었다.However, conventional bioceramic-containing fibers are made of bioceramic mixed with 20 kinds of metals and clay and heated to 1500 ℃ and processed into powder. Therefore, the particles of the powder are so large that when they are mixed into the fiber, the fiber is cut off. There was a problem that can not be made into a fine content, and to solve this problem, if the amount of bioceramic is small, the emission effect of far infrared rays is insignificant, and there is a problem that the desired effect cannot be achieved and the price is also expensive.

본 발명은 위와 같은 종래의 결점과 문제점을 개선하여 우리나라에서 부담없이 구입할 수 있는 점토광물인 일라이트를 미세분말로 가공하여 극히 소량을 섬유와 혼합하여 비교적 많은 원적외선과 음이온이 방출되게 하므로서 항균 항곰팡이 성능이 우수한 기능성 섬유를 얻어 이를 의류와 생활용품에 활용할 수 있게 한 것인데 보다 상세히 설명하면 다음과 같다.The present invention improves the above-mentioned drawbacks and problems of the present invention by processing the fine mineral clay which can be easily purchased in Korea with fine powder and mixing a very small amount with fibers to release a lot of far-infrared rays and anions antibacterial antifungal To obtain a functional fiber with excellent performance it can be used in clothing and household goods, which will be described in more detail as follows.

1 내지 2 마이크론 크기로 미세분말한 일라이트 분말을 섬유제조용 폴리아미드칩에 10∼30 중량%를 혼합하여 가열건조시켜 마스터베치(Master batch)를 얻고 이를 섬유용 폴리아미드칩과 10 : 90 중량%비율로 혼합하여 회전건조기에 투입하여 25∼30분간 회전시키면서 110∼130℃로 가열건조시켜서 수분을 제거시키고 이를 방사용 호-퍼에 투입하고 스크류방사기의 내부 온도가 285∼293℃정도되는 상태에서 용융시킨후 공기중에 방사하여 공지된 방법에 따라 냉각하고 1.3∼1.5배 연신하여 일라이트 성분의 함량이 0.7∼2.3 중량%가 되는 일라이트 나일론필라멘트사를 제조한다.The illite powder finely divided into 1 to 2 microns in size was mixed with 10 to 30% by weight of the polyamide chip for fiber production, followed by heat drying to obtain a master batch, which was 10: 90% by weight with the polyamide chip for fiber. After mixing at a ratio, it is added to a rotary dryer and rotated for 25 to 30 minutes while heating to 110 to 130 ℃ to remove moisture, and then it is put into a spinning hopper and the internal temperature of the screw spinning machine is about 285 to 293 ℃. After melting, spinning in air, cooling according to a known method, stretching 1.3 to 1.5 times to prepare an illite nylon filament yarn having a content of an illite component of 0.7 to 2.3% by weight.

이와 같이 본 발명은 일라이트를 1 내지 2 마이크론 크기로 미세분말하여 일정량을 섬유제조용 폴리아미드칩에 부착시켜 마스터베치를 만들고 이를 합성섬유제조용 폴리아미드칩과 10 : 90 중량%의 비율로 혼합하여 가열건조시키고 이것을 용융방사기로 공기중에 방사하여 필라멘트사를 제조하기 때문에 소량의 일라이트로 원적외선의 방출량이 풍부한 섬유를 얻을 수 있고 적은 량을 혼합하여 섬유를 제조하기 때문에 방사과정에서 절사가 생기지 않는 일라이트 나일론사를 제조할 수 있고 이로인해 연신과 연사가 가능한 필라멘트사를 제조할 수 있을 뿐 아니라 방적사도 제조할 수 있기 때문에 일라이트는 0.7∼2.3 중량%정도의 적은량을 넣어도 90선에 가까운 원적외선 방출효과를 낼 수가 있어서 경제적이며 미세분말체로 가공하여 합성섬유제조용 폴리아미드칩에 묻혀 마스터베치를 만들어 사용하므로 함량이 정확한 생산이 가능케 되는 것이다.As described above, the present invention finely powders the illite to 1 to 2 microns in size, attaches a predetermined amount to the polyamide chip for fiber manufacturing, and makes a master beech, and mixes it with a polyamide chip for synthetic fiber manufacturing at a ratio of 10: 90 wt% and heats it. Since the filament yarn is manufactured by drying and spinning it in the air with a melt spinning machine, it is possible to obtain a fiber having abundant emission of far infrared rays with a small amount of illite. Since nylon yarns can be manufactured and filament yarns that can be stretched and twisted can be manufactured as well as spun yarns, illite can produce far infrared rays near 90 lines even when a small amount of 0.7 to 2.3% by weight is added. It is economical and can be processed into fine powder to produce synthetic fibers. It is possible to produce the exact content by using the master bead buried in the liamide chip.

따라서 본 발명의 필라멘트사로 제직을 하여 의류나 생활용품을 제조하여 사람이 사용하게 되면 원적외선과 음이온이 인체에 작용하는 신진대사를 촉진시켜주고 위생상태를 좋게 할뿐 아니라 유해가스까지 흡착제거 하여 인체를 보호하며 피로회복 및 성인병 예방에 기여할 수 있는 등의 효과를 낼 수가 있어서 지금까지 알려진 바이오세라믹 혼합섬유보다 탁월한 성능을 발휘하게 되는 장점을 얻는 것이다.Therefore, weaving with the filament yarn of the present invention to manufacture clothing or household goods when used by humans to promote the metabolism of far-infrared rays and negative ions to the human body to improve the hygiene state, as well as adsorption and removal of harmful gases to human body It can protect and contribute to fatigue and prevention of geriatric diseases, so it has the advantage of exerting better performance than the bioceramic mixed fibers known to date.

Claims (1)

1내지 2 마이크론 크기로 미세분말한 일라이트 분말을 섬유제조용 폴리아미드칩에 10∼30 중량%를 혼합하여 마스터베치(Master batch)를 만들고 이를 섬유용 폴리아미드칩과 10 : 90 중량%비율로 혼합하여 회전건조기에 투입하여 25∼30분간 회전시키면서 110∼130℃로 가열건조시켜서 수분을 제거시키고 이를 방사용 호-퍼에 투입하여 스크류방사기의 내부 온도가 285∼293℃정도되는 상태에서 공기중에 용융방사하여 냉각시키고 1.3∼1.5배 연신하여 일라이트 성분의 함량이 0.7∼2.3 중량%가 유지되게 한 일라이트 나일론필라멘트사 제조방법1 to 2 micron finely powdered illite powder is mixed with 10 to 30% by weight of the polyamide chip for fiber manufacturing to make a master batch, which is mixed with the polyamide chip for fiber at a ratio of 10: 90% by weight. And put it into a rotary dryer and rotate it for 25 to 30 minutes while heating it to 110 ~ 130 ℃ to remove moisture, and then put it into a spinning hopper to melt it in air while the internal temperature of the screw spinning machine is about 285 ~ 293 ℃. Method for producing illite nylon filament yarn by spinning and cooling and stretching 1.3-1.5 times to keep the content of illite component 0.7-2.3 wt%
KR10-1998-0022119A 1998-06-10 1998-06-10 Manufacturing method of illite nylon filament yarn KR100407219B1 (en)

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KR100407219B1 KR100407219B1 (en) 2004-03-12

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20000018829A (en) * 1998-09-03 2000-04-06 문태수 Method for producing synthetic fiber mixed with illite
KR100494336B1 (en) * 2002-06-18 2005-06-13 이교근 Method of making un-woven textile emitting an anion
KR100547628B1 (en) * 2004-03-05 2006-01-31 박재익 Textile paper with antibacterial, insect repellent and electromagnetic shielding
KR100845803B1 (en) * 2007-11-26 2008-07-11 성원산업 주식회사 A nylon fiber method
KR101960457B1 (en) * 2018-07-30 2019-03-21 주식회사 파텍스 Production method of high-functionality filament yarn containing illite

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2578469B2 (en) * 1988-04-19 1997-02-05 宇部日東化成株式会社 Heat-fusible composite fiber
JP2716810B2 (en) * 1989-08-24 1998-02-18 宇部興産株式会社 Polyamide resin composition for filament and filament
JPH0781222B2 (en) * 1990-12-03 1995-08-30 東レ株式会社 Polyamide sewing thread
KR940014655A (en) * 1992-12-24 1994-07-19 하기주 Inorganic Filled Polyamide Resin Composition
JP3075946B2 (en) * 1994-12-09 2000-08-14 帝人株式会社 Masterbatch for dyeing polyamide and yarn for dyeing polyamide using the same
JPH10121328A (en) * 1996-10-15 1998-05-12 Unitika Ltd Polyamide staple fiber
KR100310080B1 (en) * 1998-01-15 2001-12-17 문태수 Manufacturing method of functional cotton

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20000018829A (en) * 1998-09-03 2000-04-06 문태수 Method for producing synthetic fiber mixed with illite
KR100494336B1 (en) * 2002-06-18 2005-06-13 이교근 Method of making un-woven textile emitting an anion
KR100547628B1 (en) * 2004-03-05 2006-01-31 박재익 Textile paper with antibacterial, insect repellent and electromagnetic shielding
KR100845803B1 (en) * 2007-11-26 2008-07-11 성원산업 주식회사 A nylon fiber method
KR101960457B1 (en) * 2018-07-30 2019-03-21 주식회사 파텍스 Production method of high-functionality filament yarn containing illite

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