KR100267351B1 - Process for preparing illite synthetic cotton - Google Patents
Process for preparing illite synthetic cotton Download PDFInfo
- Publication number
- KR100267351B1 KR100267351B1 KR1019980005799A KR19980005799A KR100267351B1 KR 100267351 B1 KR100267351 B1 KR 100267351B1 KR 1019980005799 A KR1019980005799 A KR 1019980005799A KR 19980005799 A KR19980005799 A KR 19980005799A KR 100267351 B1 KR100267351 B1 KR 100267351B1
- Authority
- KR
- South Korea
- Prior art keywords
- illite
- master batch
- preparing
- fiber
- spinning
- Prior art date
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Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/58—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products
- D01F6/62—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products from polyesters
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Artificial Filaments (AREA)
Abstract
Description
본 발명은 항균성과 항곰팡이성 및 유해가스 흡착성이 특히 높은 일라이트를 미세분말로 만들어 폴리에스테르칩에 혼합하여 상당시간 가열 교반하므로서 일라이트가 부착된 폴리에스테르칩 마스터베치를 제조하고 이를 합성섬유제조용 폴리에스테르칩과 5:5의 비율로 혼합하여 열풍으로 건조시킨 다음 상사용 호-퍼에 넣고 용융방사하여 모노필라멘트를 얻은 다음 이를 연신하고 연사, 합사하는 가공공정을 거쳐 일라이트 함유비율 0.5~0.7중량%정도가 되는 합성섬유를 제조하는 것이다.The present invention is made of fine powder made of illite having high antibacterial, anti-mildew and noxious gas adsorption, into a fine powder to prepare a polyester chip masterbatch with illite attached to the polyester chip by heating and stirring for a considerable time and producing synthetic fiber Mix with polyester chip at 5: 5 ratio, dry it with hot air, put it in a commercial hopper and melt-spun to obtain monofilament, and stretch it, twist and spun it. It is to produce a synthetic fiber that is about weight percent.
일라이트(illite)원적외성을 방사하는 연질운모광물이고 충북 영동산 일라이트의 성분은 Sio2> Al2O3> K2O > Fe2O3>순으로 구성되어 있으며 일반적으로 K의 함량이 적고 결정수가 많으며 구조적으로는 Momtmorillonite와 Muscovite의 중간구조를 갖고 있으며 분자식은 KAl4(AlSi7O20)(OH4)로 원적외선과 음이온을 방출하므로 세균의 번식을 억제하고 살균하는 항균성과 곰팡이의 번식을 억제하고 곰팡이를 죽여 악취의 발생을 막고 냄새를 제거하는 항곰팡이성을 가지고 있으면서 일라이트에서 방출되는 원적외선은 인체에 가장 좋은 5~20파장범위에 속하는 원적외선이기 때문에 인체에 가장 깊숙이 침투하여 신진대사를 촉진해주고 혈액순환을 좋게 하여 효소의 생성을 부활시키고 노화된 세포를 활성화시켜 인체내의 노폐물과 잉여 지방질의 배설을 촉진시키는 작용을 하는 것으로 알려져 있으며 유해 가스의 흡착제거 성능도 우수한 물질로 알려져 있다.Illite is a soft mica mineral that emits far-infrared rays and consists of Sio 2 > Al 2 O 3 > K 2 O> Fe 2 O 3 >. It has a small number of crystals and structurally has an intermediate structure between Momtmorillonite and Muscovite.The molecular formula is KAl 4 (AlSi 7 O 20 ) (OH 4 ), which emits far infrared rays and anions. It has anti-fungal properties that prevents the occurrence of odors by killing mold and removes odors and removes odors, while far-infrared rays that are emitted from the light are the far-infrared rays within the 5-20 wavelength range that is best for the human body. Promotes blood circulation, improves blood circulation, revitalizes the production of enzymes, activates aged cells, and promotes the excretion of waste and excess fat in the human body. It is known to act also known as an excellent material for adsorbing and removing harmful gas performance.
그러므로 이를 섬유로 만들어 의류나 생활용품을 제조하게 되면 인체에 원적외선을 방사하여 신진대사를 촉진시켜주고 세포활성화를 통해 피로회복 및 성인병 예방에 기여할 수 있는 효과를 낼수 있고 인체에 가해지는 각종의 유해가스를 흡착제거하여 인체를 보호하는 기능성 직물지를 만들 수 있다.Therefore, the manufacture of clothing or household goods by making this fiber can stimulate far metabolism by radiating far-infrared rays to the human body, and have the effect of contributing to recovery of fatigue and prevention of adult diseases through cell activation and various harmful gases applied to the human body. It can make functional textile paper to protect the human body by adsorption.
종래에도 맥반석을 비롯하여 세라믹물질을 섬유제조에 이용하는 것은 공지되어 있다.Conventionally, it is also known to use ceramic materials, including elvan, for fiber production.
그러나 종래의 세라믹물질 함유섬유는 황토를 소성하여 분쇄한것과 세라믹물질을 합성수지에 혼합하여 제조하는 것으로 분말의 입자가 비교적 크기 때문에 미세한 섬유에 혼입할수 없는 불편이 있어서 고급직물지를 제조할수 없는 불편이 있었다.However, the conventional ceramic material-containing fiber is produced by calcining ocher and mixing the ceramic material with a synthetic resin, which is inconvenient to be incorporated into fine fibers because the particles of the powder are relatively large. .
본 발명은 위와 같은 종래의 결점이나 문제점을 개선하여 우리나라에서 부담없이 구입할수 있는 점토성분인 일라이트를 소성시키지 않고 미세분말로 가공하여 합성수지에 혼합하기전에 마스터베치를 만들어 혼합하므로서 일라이트를 균등하게 혼합시켜 원적외선과 음이온의 방출이 효과적으로 달성케하고 항균 항곰팡이 성능이 우수한 기능성 섬유를 제조하는 것인데 이를 보다 상세히 설명하면 다음과 같다.The present invention improves the above-mentioned defects or problems of the prior art by processing the fine powder without firing the clay component illite that can be purchased in Korea without fine firing by mixing the synthetic resin to make the master beech evenly By mixing the far infrared and anion to effectively achieve and to produce a functional fiber excellent antibacterial antifungal performance, which will be described in more detail as follows.
1500~3000멧쉬정도의 미세분말로 만든 일라이트분말(일라이트를 물에 분산하여 체취한 가공법)을 섬유제조용 폴리에스테르칩에 1~1.4중량%의 비율로 혼합하여 가열교반기 속에 넣고 150℃정도에서 약 1시간정도 교반하여 일라이트분말이 폴리에스테르칩에 골고루 부착된 마스터베치(Master batch)를 얻고 이를 섬유용 폴리에스테르칩과 5:5의 비율로 혼합하여 회전건조기에 투입하여 25~30분간 회전시키면서 150℃로 가열 건조시켜서 수분을 제거시키고 이를 방사용 호-퍼에 투입하고 스크류방사기의 온도가 260℃~270℃정도되게 하여 용융방사하여 모노필라멘트를 얻고 이를 공지된 방법에 따라 연신하고 합사하는 가공을 하므로서 일라이트 성분의 함량이 0.5~0.7중량%가 되는 멀티필라멘트사를 제조하게 되며 또한 연신된 섬유는 일정길이 (38mm정도)로 절단하고 방적기를 통해 방사하여 방적사고 만들어서 일라이트 함유비율이 0.7중량%정도되는 일라이트 섬유를 얻는 것이다.The illite powder (processing method obtained by dispersing illite in water) made of fine powder of 1500 ~ 3000 mesh is mixed with polyester chip for fiber manufacturing at a ratio of 1 to 1.4% by weight and put in a heating stirrer at about 150 ° C. Stir for about 1 hour to obtain a master batch with the illite powder evenly attached to the polyester chip, mix it with the polyester chip for fiber at a ratio of 5: 5, and put it in a rotary dryer to rotate for 25 to 30 minutes. While drying by heating to 150 ℃ to remove moisture and put it in the spinning hopper-furnace and melt spinning the temperature of the screw spinning machine to about 260 ℃ ~ 270 ℃ to obtain a monofilament and stretched and spliced according to a known method By processing, multifilament yarns with 0.5 to 0.7% by weight of illite component are produced. The drawn fibers are cut to a certain length (about 38mm) and then By spinning through the timely spinning spinning accident to obtain an illite fiber with an illite content of about 0.7% by weight.
이와 같이 본 발명은 일라이트를 1500~3000멧쉬정도로 미세분말하여 일정량을 합성섬유제조용 폴리에스테르칩에 부착시켜 마스터베치를 만들어서 이를 합성섬유제조용 폴리에스테르칩과 5:5의 비율로 혼합하여 열풍으로 건조시키고 이것을 용융방사기에 투입하여 용융방사기 때문에 폴리에스테르보다 비중이 큰 미세일라이트분말이라 할지라도 골고루 합성수지에 혼합시킬수 있고 혼합량이 1%미만이므로 방사과정이나 연신과정에서 절사가 생기지 않는 일라리트 혼합섬유를 제조할수 있어서 용융방사된 모노필라멘트를 연신하고 연사할수 있어서 멀티필라멘트사는 물로 방적사로 제조할수 있는 장점이 있고 일라이트를 혼합하기 때문에 0.5~0.7중량%정도의 적은량을 넣어도 90%선에 가까운 원적외선 방출효과를 낼수가 있어서 경제적인 효과가 있고 이 섬유로 만든 직물지로 의류나 도구를 제조하여 사람이 사용하게 되면 원적외선의 작용효과에 따라 인체의 신진대사를 촉진시켜주고 피부를 통해 인체에 작용하는 유해가스 까지 흡착제거하여 인체를 보호 할뿐 아니라 피로회복 및 성인병 예방에 기여할 수 있는 획기적인 효과를 낼 수가 있어서 지금까지 알려진 바이오세라믹 혼합섬유보다 탁월한 성능을 발휘하게 되는 장점을 얻는 것이다.As described above, the present invention finely powders the illite to 1500 ~ 3000 mesh and attaches a certain amount to the polyester chip for synthetic fiber manufacturing to make a master beech, and mixes it with the polyester chip for synthetic fiber manufacturing at a ratio of 5: 5 to dry with hot air. It can be mixed into synthetic resin even if fine illite powder having a higher specific gravity than polyester because of melt spinning machine, and mixed with synthetic resin and less than 1%. Multifilament yarns have the advantage of being manufactured by spinning yarns with water because they can be manufactured and stretched by melt-spun monofilament, and the effect of emitting far infrared rays close to 90% even when a small amount of 0.5-0.7% by weight is mixed. It can be economically effective When a person manufactures clothes or tools using the fabric made of Euro, it can promote the metabolism of the human body according to the effect of far infrared rays and absorb and remove harmful gas acting on the human body through the skin to protect the human body, It is possible to produce a breakthrough effect that can contribute to the prevention of adult diseases, so that the performance is superior to the bioceramic mixed fiber known so far.
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Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019980005799A KR100267351B1 (en) | 1998-02-19 | 1998-02-19 | Process for preparing illite synthetic cotton |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019980005799A KR100267351B1 (en) | 1998-02-19 | 1998-02-19 | Process for preparing illite synthetic cotton |
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| Publication Number | Publication Date |
|---|---|
| KR19990070763A KR19990070763A (en) | 1999-09-15 |
| KR100267351B1 true KR100267351B1 (en) | 2000-10-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019980005799A KR100267351B1 (en) | 1998-02-19 | 1998-02-19 | Process for preparing illite synthetic cotton |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101960457B1 (en) * | 2018-07-30 | 2019-03-21 | 주식회사 파텍스 | Production method of high-functionality filament yarn containing illite |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20030006069A (en) * | 2001-07-11 | 2003-01-23 | 권정돈 | Synthetic thread manufacturing process mixing black mica ceramics powder |
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1998
- 1998-02-19 KR KR1019980005799A patent/KR100267351B1/en not_active IP Right Cessation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101960457B1 (en) * | 2018-07-30 | 2019-03-21 | 주식회사 파텍스 | Production method of high-functionality filament yarn containing illite |
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| Publication number | Publication date |
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| KR19990070763A (en) | 1999-09-15 |
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