KR100267350B1 - Process for preparing illite synthetic cotton - Google Patents

Process for preparing illite synthetic cotton Download PDF

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Publication number
KR100267350B1
KR100267350B1 KR1019980006034A KR19980006034A KR100267350B1 KR 100267350 B1 KR100267350 B1 KR 100267350B1 KR 1019980006034 A KR1019980006034 A KR 1019980006034A KR 19980006034 A KR19980006034 A KR 19980006034A KR 100267350 B1 KR100267350 B1 KR 100267350B1
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illite
cotton
spinning
master batch
preparing
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KR1019980006034A
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KR19990070911A (en
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문태수
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문태수
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    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/58—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products
    • D01F6/62—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products from polyesters
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00—Formation of filaments, threads, or the like
    • D01D5/08—Melt spinning methods
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • D01F1/103—Agents inhibiting growth of microorganisms

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Artificial Filaments (AREA)

Abstract

PURPOSE: A process for preparing synthetic cotton by pulverizing illite as a clay component and mixing synthetic fibers is provided, thereby producing functional cotton having excellent antibacterial and anti fungal performance and harmful gas absorption removing performance. CONSTITUTION: The process for producing the titled synthetic cotton comprises the steps of: preparing a master batch by mixing illite with a size of 1,500 to 3,000 mesh with polyester chips for the manufacture of fibers in a ratio of 2 to 5% by weight and agitating at 150deg.C for about 1 hr in a heating agitator; introducing the master batch and polyester chips in a ratio of 5 : 5 in a rotary drier, rotating for 25 to 30min and drying at 150deg.C; melting at 260 to 270deg.C and spinning with a thickness of 6 to 15 denier; drawing melt-spun monofilaments; and crimp-processing and cutting.

Description

일라이트 합성솜의 제조방법Manufacturing method of illite synthetic cotton

본 발명은 항균성과 항곰팡이성 및 유해가스 흡착성이 특히 높은 일라이트를 미세분말로 만들어 폴리에스테르칩에 혼합하여 상당시간 가열 교반하므로서 일라이트가 부착된 마스터베치를 제조하고 이를 합성섬유제조용 폴리에스테르칩과 5 : 5의 비율로 혼합하여 열풍으로 건조시킨 다음 방사용 호-퍼에 넣고 용융방사하여 일라이트 함유비율이 적어도 0.9∼2.3중량% 정도되는 모노필라멘트를 얻고 이를 연신하면서 크림프 가공하고 절단하는 순서로 솜을 제조하므로서 원적외선의 방출량이 양호한 일라이트 합성솜을 얻는 것인데 이렇게 제조된 일라이트솜은 유연성과 촉감 보온성이 좋으면서 항균성과 항곰팡이성 및 유해가스 흡착기능이 높은 기능을 가지게 된다.The present invention is made of fine powder made of illite having high antibacterial, anti-mildew and noxious gas adsorption, into a fine powder, mixed with a polyester chip to prepare a masterbatch with an illite by heating and stirring it for a considerable time, and a polyester chip for producing synthetic fibers And 5: 5, mixed with hot air, dried in a hot hopper and melt spun to obtain monofilaments having an illite content of at least 0.9 to 2.3% by weight, crimped and stretched while drawing them. The production of furnace cotton is to obtain a good illite synthetic cotton with far-infrared emission, the illite cotton thus prepared has a high function of antibacterial, anti-mildew and harmful gas adsorption, while having good flexibility and warmth.

일라이트(illite)는 원적외선을 방사하는 연질운모광물로서 분자식 KAl4(AlSi7O20)(OH)4이다Illite is a soft mica mineral that emits far infrared rays and has the molecular formula KAl 4 (AlSi 7 O 20 ) (OH) 4 .

특히, 충북 영동산 일라이트의 성분은 SiO2>Al2O3>K2O>Fe2O3순으로 구성되어 있으며 K의 함량이 적고 결정수가 많으며 Momtmorillonite와 Muscovite의 중간구조를 갖고 있으며 음이온도 방출하는 이중작용으로 세균의 번식을 억제하고 살균하는 항균성과 곰팡이의 번식을 억제하고 곰팡이를 죽여 악취의 발생을 막고 냄새를 제거하는 항곰팡이성을 가지고 있으면서 인체에 가장 좋은 5~20파장범위에 속하는 원적외선을 상온에서도 방출되기 때문에 인체에 접촉하면 신진대사를 촉진해주고 혈액순환을 좋게 하여 효소의 생성을 부활시키고 노화된 세포를 활성화시켜 인체내의 노폐물과 잉여 지방질의 배설을 촉진시키는 작용을 하는 것으로 알려져 있으며 유해 가스의 흡착제거 성능도 우수한 물질임은 이미 공지된 바이다.In particular, the composition of Yeongdongsan Illite, Chungbuk is composed of SiO 2 > Al 2 O 3 > K 2 O> Fe 2 O 3 , and contains small amount of K, high crystallization, intermediate structure of Momtmorillonite and Muscovite, and anion. It has the antimicrobial ability to suppress and sterilize the growth of bacteria by the dual action of release, and to prevent the development of odor by killing mold and to prevent the occurrence of odor and to remove the odor. Far-infrared rays are released at room temperature, so when they come into contact with the human body, they promote metabolism, improve blood circulation, revive the production of enzymes, and activate the aging cells to promote the excretion of waste and excess fat in the human body. It is already known that the adsorption and removal performance of the harmful gas is also excellent.

그러므로 이를 합성섬유에 혼합하여 솜으로 만들게 되면 유연성과 촉감이 좋고 원적외선의 방출도 활발하므로 인체에 유익한 가능성 솜을 공급할수 있게 된다. 종래에도 맥반석을 비롯한 세라믹물질을 섬유제조에 이용하는 것이 공지되어 있다.Therefore, if it is mixed with synthetic fibers to make cotton, it has good flexibility and feel and also emits far-infrared rays. Background Art Conventionally, it is known to use ceramic materials, including elvan, for fiber production.

그러나, 종래의 세라믹물질은 황토를 소성하여 분말한 것과 금속물질을 혼합하여 사용하므로 세라믹입자가 크고 특유의 색상을 가지고 있기 때문에 합성섬유에 혼합시키는 것이 기술적으로 어렵게되는 불편이 있었다.However, the conventional ceramic material has a disadvantage in that it is technically difficult to mix the synthetic fiber because the ceramic particles are large and have a unique color because the ceramic material is used by mixing the powdered and the metallic material by firing ocher.

본 발명은 위와 같은 종래의 결점을 해소하여 우라나라에서 부담없이 구입할수 있는 점토성분인 충북 영동산 일라이트를 미세분말로 가공하여 합성섬유와 혼합하여 솜을 제조하므로서 항균, 항곰팡이 성능 및 유해가스 흡착제거능력이 우수한 기능성 솜을 제공하는 것인데 이를 보다 상세히 설명하면 다음과 같다.The present invention solves the above-mentioned drawbacks by processing the fine powder of Chungbuk Yeongdongsan illite, which can be easily purchased in Uranara, by mixing with synthetic fibers to produce cotton and antibacterial, anti-fungal performance and harmful gas It is to provide a functional cotton with excellent adsorption and removal capacity, which will be described in more detail as follows.

1500∼3000멧쉬정도의 미세분말로 가공(일라이트를 물에 분산시켜 체취하는 가공방법)된 일라이트 분말을 섬유제조용 폴리에스테르칩에 2∼5중량%의 비율로 혼합하여 가열교반기 속에 넣고 150℃정도에서 약 1시간정도 교반하여 일라이트분말이 폴리에스테르칩의 표면에 부착된 마스터베치(Master batch)를 얻고 이를 섬유용 폴리에스테르칩과 5 : 5의 비율로 혼합하여 회전건조기에 투입하여 25∼30분간 회전시키면서 150℃로 가열하여 수분을 제거시키고 이를 방사용 호-퍼 투입하고 스크류방사기의 온도 260℃∼270℃정도되는 상태에서 6-15데니어 정도의 굵기로 용융방사하여 일라이트 함량이 0.9∼2.3중량% 범위가 되는 모노필라멘트를 얻고 이를 공지된 방법에 따라 연신하면서 크림프 가공하고 2∼15cm크기로 절단하여 일라이트솜을 제조하는 것이다.The illite powder processed into 1500 ~ 3000 mesh fine powder (processing to disperse the illite in water) is mixed into polyester chip for fiber manufacturing at a ratio of 2 to 5% by weight and put into a heating stirrer at 150 ° C. Stir for about 1 hour to obtain a master batch in which the illite powder is attached to the surface of the polyester chip, mixed with a polyester chip for fiber at a ratio of 5: 5 and put into a rotary dryer to 25 ~ Heated at 150 ℃ while rotating for 30 minutes to remove moisture, and it was injected into a spinning hopper and melt-spun at a thickness of about 6-15 denier at a temperature of 260 ℃ ~ 270 ℃ of a screw spinning machine, so that the illite content was 0.9 To obtain a monofilament in the range of -2.3% by weight, it is crimped while stretching according to a known method, and is cut into 2 to 15 cm in size to produce an illite cotton.

이안 같이된 본 발명은 일라이트를 1500∼3000멧쉬정도로 미세분말하여 합성섬유제조용 폴리에스테르칩과 마스터베치를 만들어서 합성섬유제조용 폴리에스테르칩과 5 : 5의 비율로 혼합하고 건조시킨후 용융방사기에 투입하여 용융압출하기 때문에 일라이트를 합성섬유에 골고루 혼합시킬수 있는 장점이 있고 일라이트를 가열하지 않고 미세분말로 만들어 합성수지에 혼합하기 때문에 유연성이 양호하고 방사시에 섬유의 절단이 발생하지 않아 연신율을 높혀 클림프사를 제조할수 있기 때문에 탄력성도 양호한 솜이 만들어지고 일라이트에서 방출되는 원적외선의 작용으로 보온성이 양호하게 되면서 항균성과 항곰팡이성 그리고 유해가스 흡착성능이 높은 효과를 낼수가 있고 일라이트를 미세분말체(1500∼3000멧쉬정도)로 가공하여 합성섬유제조용칩에 묻혀 마스터베치를 제조하고 이를 합성섬유와 일정비율로 혼합하여 방사하기 때문에 일라이트 함량이 정확하게 혼합되고 방사 및 가공이 용이하게되어 양질의 솜을 만들 수 있는 것이다.The present invention as described in the present invention finely powdered illite to 1500 to 3000 mesh to make a polyester chip and master beet for synthetic fiber manufacturing, mixed with a polyester chip for synthetic fiber manufacturing in a ratio of 5: 5 and dried and put into a melt spinning machine Because it melts and extrudes, it has the advantage of uniformly mixing illite with synthetic fiber.Because it is made of fine powder without heating the illite and mixed with synthetic resin, the flexibility is good and the elongation is not increased because the fiber is not cut during spinning. Since it can be manufactured with a crimp yarn, a cotton with good elasticity is made, and the warmth is good due to the action of far-infrared rays emitted from the illite, which has high antibacterial, anti-mildew and harmful gas adsorption performance. Chips for manufacturing synthetic fibers by processing (1500 ~ 3000 mesh) Buried is prepared a master batch, and this is exactly the illite content mixed because radiation a mixture of synthetic fibers and a percentage facilitate the spinning and processing is to create a high quality cotton.

따라서, 본 발명의 일라이트 솜을 보온재로 사용하게 되면 보온성은 물론 원적외선의 작용효과에 따라 인체의 신진대사를 촉진시켜주고 피부를 통해 인체에 작용하는 유해가스까지 흡착제거하여 인체를 보호 할뿐 아니라 피로회복 및 성인병 예방에 기여할 수 있는 획기적인 효과를 낼 수가 있어서 지금까지 알려진 다른 종류의 기능성 솜보다 이용가치가 높은 장점을 발휘하게 된다.Therefore, when the illite cotton of the present invention is used as a heat insulating material, it promotes the metabolism of the human body according to the effect of warmth as well as the far infrared rays, and absorbs and removes harmful gases acting on the human body through the skin to protect the human body as well as fatigue. It can have a dramatic effect that can contribute to the recovery and prevention of geriatric diseases, and has the advantage of higher use value than other types of functional cotton known to date.

Claims (1)

1500∼3000멧쉬정도의 미세분말로 만든 일라이트를 섬유제조용 폴리에스테르칩에 2∼5중량%비율로 혼합하고 가열교반기 속에 넣고 150℃정도에서 약 1시간정도 교반하여 일라이트분말이 폴리에스테르칩에 부착되도록 하는 마스터베치(Master batch) 제조공정과, 마스터베치와 섬유제조용 폴리에스테르칩을 5 : 5의 비율로 혼합하여 회전건조기에 투입하여 25∼30분간 회전시키면서 150℃로 가열 건조시켜서 수분을 제거하는 건조공정과, 건조된 소재를 방사용 호-퍼에 투입하고 스크류방사기로 260℃∼270℃로 용융시켜 6∼15데니어 정도의 굵기로 용융방사하는 방사공정과 용융방사된 모노필라멘트를 연신하면서 크림프 가공하고 절단하는 가공공정으로 이루어지는 일라이트 합성솜의 제조방법.The illite made of fine powder of 1500 ~ 3000 mesh is mixed in polyester chip for fiber manufacturing at 2 ~ 5% by weight, and it is put in a heating stirrer and stirred at 150 ℃ for about 1 hour. Master batch manufacturing process to be attached, and master batch and polyester chip for fiber manufacturing are mixed at a ratio of 5: 5, and put into a rotary dryer and heated and dried at 150 ℃ while rotating for 25 to 30 minutes to remove moisture. The drying process, the dried material is put into a spinning hopper and melted at 260 ° C. to 270 ° C. with a screw spinning machine, and the spinning process is melt spinning to a thickness of about 6 to 15 deniers and the melt spun monofilament is stretched. A method for producing an illite synthetic cotton comprising a processing step of crimping and cutting.
KR1019980006034A 1998-02-20 1998-02-20 Process for preparing illite synthetic cotton KR100267350B1 (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100407220B1 (en) * 2000-03-20 2003-11-28 (주)성신텍스타일 method for manufacturing of functional fiber clay and mica as base material
KR20170000307A (en) 2015-06-23 2017-01-02 김민재 Multi function pp filament and Products of mixture of polypropylene resin with illite
KR101907688B1 (en) 2017-11-30 2018-10-15 주식회사 큐링 Latent potential crimped filament yarn with far-infrared radiation function and preparation method thereof
KR101960457B1 (en) 2018-07-30 2019-03-21 주식회사 파텍스 Production method of high-functionality filament yarn containing illite

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Publication number Priority date Publication date Assignee Title
KR20010020071A (en) * 1999-08-31 2001-03-15 조민호 Manufacturing method of far infrared radiation polyester fiber containing loess.
KR20010074214A (en) * 2001-04-10 2001-08-04 김동주 Anfibacterial cotton manafacturing and antibscterial which is manufactuved by
KR100467101B1 (en) * 2001-08-13 2005-01-24 김희삼 A manufacturing method of man made fiber and nonwoven fabric to use illite
KR100438382B1 (en) * 2002-02-06 2004-07-02 정형식 Method for making synthetic cotton
KR102026086B1 (en) 2018-10-26 2019-09-27 전병민 Composition for preparing febrific synthetic cotton and preparation of the febrific synthetic cotton by using it
KR102229914B1 (en) * 2020-09-03 2021-03-19 바이오신텍스 주식회사 A manufacturing method of man made fiber using clay mineral

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100407220B1 (en) * 2000-03-20 2003-11-28 (주)성신텍스타일 method for manufacturing of functional fiber clay and mica as base material
KR20170000307A (en) 2015-06-23 2017-01-02 김민재 Multi function pp filament and Products of mixture of polypropylene resin with illite
KR101907688B1 (en) 2017-11-30 2018-10-15 주식회사 큐링 Latent potential crimped filament yarn with far-infrared radiation function and preparation method thereof
KR101960457B1 (en) 2018-07-30 2019-03-21 주식회사 파텍스 Production method of high-functionality filament yarn containing illite

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