KR19990078990A - Refined alkali water and process for preparation of the same - Google Patents
Refined alkali water and process for preparation of the same Download PDFInfo
- Publication number
- KR19990078990A KR19990078990A KR1019990036099A KR19990036099A KR19990078990A KR 19990078990 A KR19990078990 A KR 19990078990A KR 1019990036099 A KR1019990036099 A KR 1019990036099A KR 19990036099 A KR19990036099 A KR 19990036099A KR 19990078990 A KR19990078990 A KR 19990078990A
- Authority
- KR
- South Korea
- Prior art keywords
- water
- purified water
- passing
- ocher
- present
- Prior art date
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 64
- 238000000034 method Methods 0.000 title claims abstract description 17
- 239000003513 alkali Substances 0.000 title 1
- 239000008213 purified water Substances 0.000 claims abstract description 33
- 238000001914 filtration Methods 0.000 claims abstract description 25
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 25
- 239000011707 mineral Substances 0.000 claims abstract description 25
- 238000004519 manufacturing process Methods 0.000 claims abstract description 9
- 230000001954 sterilising effect Effects 0.000 claims description 13
- 238000004659 sterilization and disinfection Methods 0.000 claims description 10
- 239000003673 groundwater Substances 0.000 claims description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 239000006228 supernatant Substances 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000002352 surface water Substances 0.000 claims description 6
- 239000008399 tap water Substances 0.000 claims description 6
- 235000020679 tap water Nutrition 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- -1 polypropylene Polymers 0.000 claims description 3
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- 239000002689 soil Substances 0.000 claims description 3
- 229910021536 Zeolite Inorganic materials 0.000 claims description 2
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 2
- 229910052900 illite Inorganic materials 0.000 claims description 2
- VGIBGUSAECPPNB-UHFFFAOYSA-L nonaaluminum;magnesium;tripotassium;1,3-dioxido-2,4,5-trioxa-1,3-disilabicyclo[1.1.1]pentane;iron(2+);oxygen(2-);fluoride;hydroxide Chemical compound [OH-].[O-2].[O-2].[O-2].[O-2].[O-2].[F-].[Mg+2].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[K+].[K+].[K+].[Fe+2].O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2 VGIBGUSAECPPNB-UHFFFAOYSA-L 0.000 claims description 2
- 229910001562 pearlite Inorganic materials 0.000 claims description 2
- 238000001556 precipitation Methods 0.000 claims description 2
- 239000010457 zeolite Substances 0.000 claims description 2
- 239000004743 Polypropylene Substances 0.000 claims 2
- 229920001155 polypropylene Polymers 0.000 claims 2
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims 1
- 229910052622 kaolinite Inorganic materials 0.000 claims 1
- 229910052901 montmorillonite Inorganic materials 0.000 claims 1
- 238000010998 test method Methods 0.000 abstract description 4
- 229910001385 heavy metal Inorganic materials 0.000 abstract description 2
- 238000011109 contamination Methods 0.000 abstract 2
- 230000001580 bacterial effect Effects 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 235000020188 drinking water Nutrition 0.000 description 7
- 239000003651 drinking water Substances 0.000 description 7
- 238000012360 testing method Methods 0.000 description 7
- 241000894006 Bacteria Species 0.000 description 6
- 235000013361 beverage Nutrition 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 241000588724 Escherichia coli Species 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000000460 chlorine Substances 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- 238000010971 suitability test Methods 0.000 description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- YNQLUTRBYVCPMQ-UHFFFAOYSA-N Ethylbenzene Chemical compound CCC1=CC=CC=C1 YNQLUTRBYVCPMQ-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000008235 industrial water Substances 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 235000019645 odor Nutrition 0.000 description 2
- 239000005416 organic matter Substances 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- 239000002351 wastewater Substances 0.000 description 2
- 238000004065 wastewater treatment Methods 0.000 description 2
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 1
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- 239000005949 Malathion Substances 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 239000003957 anion exchange resin Substances 0.000 description 1
- 238000011001 backwashing Methods 0.000 description 1
- 239000003729 cation exchange resin Substances 0.000 description 1
- 238000013098 chemical test method Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000012217 deletion Methods 0.000 description 1
- 230000037430 deletion Effects 0.000 description 1
- 238000010612 desalination reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- FHIVAFMUCKRCQO-UHFFFAOYSA-N diazinon Chemical compound CCOP(=S)(OCC)OC1=CC(C)=NC(C(C)C)=N1 FHIVAFMUCKRCQO-UHFFFAOYSA-N 0.000 description 1
- JXSJBGJIGXNWCI-UHFFFAOYSA-N diethyl 2-[(dimethoxyphosphorothioyl)thio]succinate Chemical compound CCOC(=O)CC(SP(=S)(OC)OC)C(=O)OCC JXSJBGJIGXNWCI-UHFFFAOYSA-N 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000002538 fungal effect Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 230000000415 inactivating effect Effects 0.000 description 1
- 239000010842 industrial wastewater Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 229960000453 malathion Drugs 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- LCCNCVORNKJIRZ-UHFFFAOYSA-N parathion Chemical compound CCOP(=S)(OCC)OC1=CC=C([N+]([O-])=O)C=C1 LCCNCVORNKJIRZ-UHFFFAOYSA-N 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 239000012286 potassium permanganate Substances 0.000 description 1
- 238000003908 quality control method Methods 0.000 description 1
- 238000013441 quality evaluation Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000001223 reverse osmosis Methods 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 239000013535 sea water Substances 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229950011008 tetrachloroethylene Drugs 0.000 description 1
- UBOXGVDOUJQMTN-UHFFFAOYSA-N trichloroethylene Natural products ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/30—Treatment of water, waste water, or sewage by irradiation
- C02F1/32—Treatment of water, waste water, or sewage by irradiation with ultraviolet light
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Medicinal Chemistry (AREA)
- Water Treatment By Sorption (AREA)
- Physical Water Treatments (AREA)
Abstract
본 발명은 미네랄이 다량 함유된 알칼리성 정제수 및 그 제조방법에 관한 것으로 물에 1∼50 중량%의 황토를 로타리교반기에 혼합 투입하여 50∼150 rpm으로 교반한 다음 30∼60분 침전시킨 후 그 상층액을 모터펌프를 이용하여 다단계 여과시스템으로 강제 이송시켜 여과시킨 후 자외선 살균기를 통과시켜 살균하여 제조됨을 특징으로 하는 알칼리성 정제수 제조방법과 그 제조장치를 제공하며, 이와 같이 제조된 알칼리 정제수는 먹는 물 수질공정시험법에 의거 시험결과 중금속 오염 및 세균오염이 없으며 미네랄이 다량 함유하고 20℃에서 pH가 8.0 이상 알칼리성을 나타내는 뛰어난 발명이다.The present invention relates to alkaline purified water containing a large amount of minerals and a method for manufacturing the same. 1 to 50 wt% of ocher is mixed with water in a rotary stirrer, stirred at 50 to 150 rpm, and then precipitated for 30 to 60 minutes. The liquid is forced to a multi-stage filtration system using a motor pump and filtered, and then sterilized by passing through an ultraviolet sterilizer, and a method for manufacturing alkaline purified water, and a manufacturing apparatus thereof. According to the water quality test method, it is an excellent invention which shows no heavy metal contamination and bacterial contamination, contains a large amount of minerals, and has an alkaline pH above 8.0 at 20 ℃.
Description
본 발명은 미네랄이 다량 함유된 알칼리성 정제수 및 그 제조방법에 관한 것이다. 더욱 상세하게는, 본 발명은 물에 황토를 첨가 후 교반하여 침전시킨 다음 상층수를 모터펌프를 이용하여 다단계 여과시스템으로 강제 이송시켜 정제 후 살균처리하여서 되는 알칼리 정제수 및 그 제조방법에 관한 것이다.The present invention relates to alkaline purified water containing a large amount of minerals and a method for producing the same. More specifically, the present invention relates to alkaline purified water and a method for producing the same, which are added by the addition of ocher to water, precipitated, precipitated, and then forcedly transferred to a multi-stage filtration system using a motor pump to sterilize after purification.
종래에도 오염된 지하수 또는 수도수(water tap)를 정제하여 정제수를 얻는 방법이 다수 공지 공용되어 왔다. 정수를 취식한다는 것은 최근과 같이 하천이 오염되고 지하수까지 오염된 수질 및 토양 환경하에서는 가장 긴요하고도 긴박한 실정에 있다. 원수(原水) 예컨대 상수도, 지표수, 지하수 및 폐수를 적절히 처리한 처리수를 정제수로 공급하기 위하여 활성탄 여과장치(carbon filter system)가 공지되어 있다. 이와 같은 시스템은 활성탄(active carbon)의 강력한 흡착력을 이용하여 처리하고자 하는 원수의 맛, 냄새, 잔류염소 또는 유기물을 제거할 수 있어 음료수 제조장치 및 폐수처리장치 등에 활용되어 왔다.Conventionally, a number of methods for obtaining purified water by purifying contaminated ground water or water tap have been commonly known. In recent years, drinking water is most critical and urgent under the contaminated water quality and soil environment. Activated carbon filter systems are known for supplying purified water to raw water, such as tap water, surface water, groundwater, and wastewater. Such a system has been utilized in a beverage production apparatus and wastewater treatment apparatus because it can remove the taste, smell, residual chlorine or organic matter of raw water to be treated by using strong adsorption power of active carbon.
또, 이온교환수지시스템(Mixed Bed-deionizer system)은 밀폐된 용기내에 양이온 교환수지와 음이온 교환수지를 혼합 충진하고 원수를 통과시켜 원수중의 각종 양·음이온 성분을 제거하여 순수만을 제조하는 장치이며, 이온수지의 성능이 저하되면 염산과 NaOH를 사용하여 재생하여 연속적으로 이용할 수 있는 것이다. 이와 같은 시스템은 정밀화학 및 반도체분야의 전자공업용수 제조에 사용되어 왔다.In addition, the mixed bed-deionizer system is a device that mixes and fills a cation exchange resin and an anion exchange resin in a sealed container, and passes only raw water to remove various positive and negative ions from raw water to produce pure water only. In addition, when the performance of the ion resin is degraded, it can be regenerated using hydrochloric acid and NaOH and used continuously. Such systems have been used for the production of electronic industrial water in the fine chemicals and semiconductor fields.
한편, 역삼투여과시스템(Reverse osmosis system)은 극히 최근에 도입된 여과방식으로 원수를 가압처리하여 상변화없이 용질을 분리 농축하는 방법에 의하여 순수(H2O)만 여과시키고 이온이나 기타 물질의 분자를 제거하는 것으로 음료수를 비롯하여 해수의 담수화 시스템, 전자 및 반도체 장비산업 기타 폐수처리분야에 이르기까지 광범위하게 응용되고 있다.Reverse osmosis system, on the other hand, is a very recently introduced filtration method that pressurizes raw water to separate and concentrate solutes without phase change, filtering only pure water (H 2 O), and generating molecules of ions or other substances. It has been widely applied to beverages, seawater desalination systems, electronics and semiconductor equipment industries and other wastewater treatment fields.
상술한 바와 같이, 오염된 상수도, 지표수, 지하수를 비롯한 공업용수 그리고 폐수에 이르기까지 원수 또는 폐수로부터 미생물, 유기물 기타 불순물을 제거하고 정화하여 순수로 제조하기 위한 다양한 여과시스템이 연구 개발되어 왔으나, 지금까지 지하수, 상수도, 지표수에 황토 등을 첨가하여 인체에 필요한 미네랄을 다량 용출시켜 이를 알칼리 정제수로 제조하는 방법이나 그 시스템은 전혀 공지된 바 없었다.As described above, various filtration systems have been researched and developed to remove and purify microorganisms, organic matter and other impurities from raw or waste water, including contaminated tap water, surface water, ground water, industrial water, and wastewater. Until now, groundwater, tap water, surface water, ocher, etc. were added to elute a large amount of minerals necessary for the human body, and a method of preparing them into alkaline purified water, or a system thereof, was not known at all.
본 발명은 상기와 같은 점을 감안하여 안출한 것으로 본 발명의 목적은 미네랄이 다량 함유된 알칼리성 정제수를 제공함에 있다. 본 발명의 다른 목적은, 미네랄이 다량 함유되어 알칼리성을 띄우며 세균 등 미생물, 유기물 기타 불순물이 제거된 정제수를 제조하는 방법을 제공한다. 본 발명의 또 다른 목적은, 상기 미네랄이 다량 함유된 알칼리성 정제수의 제조방법에 가장 바람직한 여과방법을 제공함에 있다.The present invention has been made in view of the above point, and an object of the present invention is to provide an alkaline purified water containing a large amount of minerals. Another object of the present invention is to provide a method for preparing purified water containing a large amount of minerals to promote alkalinity and remove microorganisms such as bacteria, organic substances and other impurities. Still another object of the present invention is to provide a filtration method which is most preferable for a method of preparing alkaline purified water containing a large amount of the mineral.
본 발명의 상기 목적은 원수(原水)에 황토를 첨가하여 교반기를 이용하여 교반한 다음 그 상층액(supernatant)만을 모터펌프를 이용하여 다단계 여과시스템으로 강제 이송시켜 여과시키고 자외선 살균기(UV sterilizer)로 살균하여 미네랄이 함유된 알칼리성 정제수를 얻은 다음 이 정제수에 대하여 음료수로서의 적합성을 평가하므로써 달성하였다.The above object of the present invention is added to the raw water (ocher) and stirred by using a stirrer and then only the supernatant is forced to the multi-stage filtration system using a motor pump to filter and UV sterilizer (UV sterilizer) It was achieved by sterilizing to obtain alkaline purified water containing minerals and then evaluating its suitability as a beverage.
이하, 본 발명의 구체적인 구성 및 작용을 바람직한 도면 및 공정별 실시예를 들어 상세히 설명하지만 본 발명의 권리범위가 이들 실시예에만 한정하지 아니하고, 당업자가 상기 실시예의 범위내에서 얼마든지 일부 구성의 부가 또는 삭제에 의하여 설계 변경하여 실시할 수 있음은 물론이며, 이러한 경우 본 발명의 권리를 침해하는 것이다.Hereinafter, the specific configuration and operation of the present invention will be described in detail with reference to preferred drawings and process-specific embodiments, but the scope of the present invention is not limited only to these embodiments, and those skilled in the art can add some configurations within the scope of the above embodiments. Or by changing the design can be carried out by deletion, of course, in this case violates the rights of the present invention.
도 1은 본 발명 알칼리성 정제수 제조방법의 바람직한 실시예를 도시한 개략공정도이다.1 is a schematic process chart showing a preferred embodiment of the present invention for producing alkaline purified water.
도 2는 본 발명 방법의 다단계 여과시스템의 바람직한 실시예를 도시한 그림이다.Figure 2 shows a preferred embodiment of a multistage filtration system of the method of the present invention.
본 발명의 바람직한 실시예는 도 1과 도 2에 도시하였다. 이들 도면에 의하면, 본 발명은 원수에 황토를 첨가하는 단계와; 상기 미네랄 공급원이 되는 황토가 혼합된 원료를 교반기에서 교반함으로써 미네랄을 용출하는 단계와; 30∼60분간 침전단계와; 미네랄이 용출된 본 발명의 원료수가 되는 상층액(supernatant)을 모터펌프에 의하여 다단계 여과시스템으로 강제 이송시켜 여과하는 단계와; 여과된 정수를 UV 살균기를 통과시켜 살균하는 단계의 결합으로 구성됨을 특징으로 한다.Preferred embodiments of the invention are shown in FIGS. 1 and 2. According to these figures, the present invention comprises the steps of adding ocher to raw water; Eluting the minerals by stirring the raw material mixed with ocher to be the mineral source in a stirrer; A precipitation step for 30 to 60 minutes; Forcing the supernatant, which is the raw material water of the present invention, in which the mineral is eluted, to the multistage filtration system by means of a motor pump and filtering the same; Characterized in that it consists of a combination of the steps of sterilizing the filtered purified water through a UV sterilizer.
본 발명에서 원수(原水)는 수도수(water tap), 지하수, 지표수 어느것이라도 무방하다. 상기 원수의 종류에 따라서 황토를 혼합하여 교반할 때 동일한 조건하에서 황토로부터 유리되는 미네랄(Minerals)의 함량은 차이가 날 수 있다. 한편, 동일한 원수(原水)에 첨가되는 황토의 경우에도 그 출처 즉 산지와 황토의 종류에 따라서도 큰 차이가 있다. 첨가되는 황토의 종류로서 Kaolirite, illite, Montmollilonite, zeolite, pearlite 중에서 필요에 따라 어느것이든 선택하여 첨가할 수 있다.In the present invention, the raw water may be any of tap water, ground water, and surface water. The content of minerals liberated from ocher under the same conditions may vary when the ocher is mixed and stirred according to the type of raw water. On the other hand, in the case of ocher added to the same raw water (原 水) there is a big difference also depending on the source, namely the mountain and the type of loess. As the type of ocher to be added, any one of Kaolirite, illite, Montmollilonite, zeolite and pearlite can be selected and added as necessary.
미네랄 공급원이 되는 황토를 원수에 투입하는 장치로서는 콘베이어 벨트 시스템이 가장 바람직하다. 그리고 교반기는 Rotary type이 가장 바람직하지만 어떠한 공업용 교반기도 무방하다. 로타리 교반기에서 미네랄 공급을 유도하기 위하여 필요한 교반속도는 크게 중요하지 않으나 50∼150 rpm 정도이면 만족스럽다.Conveyor belt systems are most preferred as a device for introducing loess, which is a mineral source, into raw water. And the stirrer is the most preferred rotary type, but any industrial stirrer may be used. The stirring speed required to induce the mineral supply in the rotary stirrer is not critical but is satisfactory at around 50 to 150 rpm.
필요한 경우, 교반기 대신 원심분리기를 사용할 수도 있다.If necessary, a centrifuge may be used instead of the stirrer.
한편, 원수에 첨가하는 황토의 수준은 1∼50 중량%가 바람직하나 더욱 바람직하기로는 20∼30 중량%이다. 황토로부터 미네랄 공급수준을 높히기 위해서는 황토를 autoclave 등에 의하여 121℃에서 15분간 가열하여 태우지 않고 사용하는 것이다. 또, 태우지 않은 생황토(生黃土)로부터 미네랄 용출량을 증대시키기 위한 수단이 채용될 수 있다.On the other hand, the level of ocher added to the raw water is preferably 1 to 50% by weight, more preferably 20 to 30% by weight. In order to increase the level of mineral supply from loess, loess is used without heating by heating at 121 ° C for 15 minutes by autoclave. In addition, a means for increasing the amount of mineral leaching from unburned raw yellow soil can be employed.
교반 후 황토침전에 필요한 시간은 황토의 종류와 첨가량 및 불에 태우는가 그렇지 않은가의 처리여부와 관련되지만 대체로 30∼60분이면 만족스럽다. 교반 후 황토잔류물(Residues)은 필요에 따라 생약재를 첨가하여 피부맛사지용 황토팩에 제공할 수 있다.The time required for ocher settling after stirring is related to the type and amount of ocher and whether it is burned or not, but it is generally satisfactory if it is 30 to 60 minutes. After stirring, ocher residues (Residues) can be provided to the ocher pack for skin massage by adding herbal medicines as needed.
한편, 황토층 위에 분리된 상층액(Supernatant)은 모터펌프에 의하여 다단계 여과시스템을 통과하면서 여과정수된다(도 2참조). 본 발명의 바람직한 다단계 여과시스템은 제1∼4단계를 포함한다.On the other hand, the supernatant separated on the ocher layer is filtered through a multi-stage filtration system by a motor pump (see FIG. 2). Preferred multistage filtration systems of the present invention comprise first to fourth stages.
제1단계는 압력여과장치(Pressure filter system)로서 황토로부터 미네랄이 용출된 상기 상층액으로부터 녹(rust), 먼지(dreg), 이물질(particle) 및 미생물(microbes)을 제거하는 단계(Ⅰ 단계)이다.The first step is a pressure filter system to remove rust, dregs, foreign particles and microbes from the supernatant of minerals eluted from the loess (step I). to be.
상기 장치는 밀폐된 용기내의 하부에 집수장치를 만들고 그 위에 지지재로서 Silica sand와 Silica gravel을 충진하여 원수가 이 여재를 통과하면서 상기 혼탁물질을 제거하여 탁도를 저하시키는 것이다. 상기 여과장치는 역세척 공정을 거쳐 이물질을 외부로 방출하여 재사용할 수 있으며 Vertical type으로 구성되어 여과면적이 크고, 따라서 균일한 수질을 얻을 수 있다.The device is to make a collecting device in the lower part of the sealed container and fill Silica sand and Silica gravel as a support material thereon to remove turbidity as raw water passes through the filter medium to reduce turbidity. The filtration apparatus may be reused by releasing foreign substances to the outside through a backwashing process, and is configured in a vertical type so that the filtration area is large, thus obtaining uniform water quality.
제2단계는 백필터 시스템(Bag filter system)으로 상기 제1단계를 거친 유체에 존재하는 먼지(dust) 등 부유물질을 제거하는 단계(Ⅱ 단계)이다. 백필터의 Pore size는 25∼150㎛가 바람직하며, 재질은 Poly prophylene이 적합하다.The second step is a bag filter system (step II) to remove suspended substances such as dust present in the fluid that passed through the first step. The pore size of the bag filter is preferably 25 ~ 150㎛, and the material is poly prophylene.
제3단계는 마이크로필터 시스템(Microfiler system)으로 상기 제1 및 2단계 여과공정에서 미처 제거되지 못한 분자량이 더 작은 중금속, virus 기타 오염물질(pollutants)을 제거하는 단계(Ⅲ 단계)이다.The third step is a microfilter system (Step III) to remove heavy metals, viruses and other pollutants of smaller molecular weight that were not removed in the first and second filtration processes.
이 단계의 여과는 poly prophylene 재질의 filter가 채택되고 필터의 Pore size는 0.2∼50㎛의 범위내의 것을 선택함이 바람직하다. 더욱 정밀한 여과를 위하여는 Micro filter system은 예컨대, Pore size 1㎛의 filter로 이루어진 filter cartridge로 채운 제1 여과기와 0.45㎛의 filter로 이루어진 filter cartridge로 채운 제2 여과기를 설치할 수 있다.In this step, polyprophylene filter is used, and the pore size of the filter is preferably in the range of 0.2-50㎛. For more precise filtration, the micro filter system may, for example, install a first filter filled with a filter cartridge made of a filter having a pore size of 1 μm and a second filter filled with a filter cartridge made of a filter of 0.45 μm.
제4단계는 활성탄 여과시스템(Post carbon filter system)으로 원수(原水)중에 잔류하는 염소(dissolved chlorine), 트리할로메탄(trihalomethane), H2S 등 각종 개스 및 냄새물질(odors)를 제거하는 단계(Ⅳ 단계)이다.The fourth stage is a post carbon filter system that removes various gases and odors such as chlorine, trihalomethane, and H 2 S remaining in raw water. Step IV.
본 발명의 바람직한 상기 다단계 여과시스템은 도 2에 Ⅰ, Ⅱ, Ⅲ 및 Ⅳ 단계로 표시하여 두었다.Preferred multistage filtration systems of the present invention are shown in Figures I, II, III and IV steps.
상기 단계 여과시스템을 통과한 정제수(purified water)는 자외선 살균기(UV sterilizer)를 통과시켜 살균한다. 단파인 자외선을 254mm의 파장에서 대체로 모든 미생물 세포를 접촉시켜 핵내 DNA를 불활성화하고 물리적인 충격을 가하여 파괴시킨다.Purified water passed through the filtration system is sterilized by passing through a UV sterilizer. Ultraviolet rays, which are shortwaves, contact all microbial cells at a wavelength of 254 mm, inactivating DNA in the nucleus and destroying them by applying a physical shock.
이와 같이 하여 정제된 정제수는 황토로부터 미네랄이 다량 용출된 알칼리성 음료이면서 동시에 E. coli 등 세균 및 어떠한 종류의 곰팡이 포자 및 유기물도 존재하지 않으며 탈취가 완전하여 이미나 이취가 전혀 없는 것으로 평가되었다.Purified water thus purified was an alkaline drink with a large amount of minerals eluted from ocher, and at the same time, bacteria and other fungal spores and organics such as E. coli were not present.
이하에서는, 본 발명의 상기 다단계 여과공정에 의하여 제조된 정제수에 대하여 음료수로서의 적합성을 조사하였다.In the following, the suitability as a drinking water to the purified water produced by the multi-stage filtration step of the present invention was investigated.
실험예 1 : 본 발명 정수의 음료수 적합성 시험Experimental Example 1: Drinking water suitability test of the present invention
본 발명 방법에 따라 제조된 정제수(精制水)의 음료수로서의 적합여부를 확인 평가하기 위하여 시료(試料)를 한국화학시험연구원에 1999. 8. 10 TK-17695호로 의뢰한 결과 다음 표 1a 및 1b와 같은 시험성적을 얻었다. 공시재료로 사용한 본 발명 제품 정수시료의 평가치는 3점의 시료를 조사하여 그 평균치를 얻어 표시하였다.In order to confirm and evaluate the suitability of purified water prepared according to the method of the present invention as a beverage, the samples were submitted to TK-17695 by Korean Chemical Testing Institute as of Aug. 10, 1999 and the following Tables 1a and 1b. The same test results were obtained. The evaluation value of the product purified water sample of this invention used as a test material was investigated by displaying three samples, and displayed the average value.
표 1a 및 1b에서 확인되는 바와 같이, 수질평가 결과는 먹는물 수질공정 시험법에 의거 이루어졌으며 색도 1, 탁도 0.1, 냄새와 맛은 적합한 것으로 나타났고 pH는 20℃에서 8.2로 나타났다.As confirmed in Tables 1a and 1b, the results of water quality evaluation were made according to the drinking water quality test method, color 1, turbidity 0.1, odor and taste were found to be suitable, and pH was 8.2 at 20 ° C.
또한, 본 발명 정제수 제품은 일반세균과 E. coli가 검출되지 아니하여 음료수로서 적합한 것으로 확인되었다. 일반 세균과 E. coli 기타 유기물이 검출되지 않은 것은 본 발명 다단계 여과공정을 거쳐 최종적으로 UV 살균기를 통과하기 때문인 것으로 확인되었다.In addition, the purified water product of the present invention was found to be suitable as a beverage because the normal bacteria and E. coli was not detected. It was confirmed that the general bacteria and E. coli other organics were not detected through the UV sterilizer through the multi-stage filtration process of the present invention.
실험예 2 : 황토의 전처리 유무와 물시료의 적합성 여부조사Experimental Example 2: Investigation of the presence of pretreatment of ocher and suitability of water sample
본 발명 제품 정제수를 제조하기 위하여 첨가하는 황토는 지하수 : 황토의 비율을 5 : 1로 하였으며 황토를 사전에 auto clave에서 121℃에서 15분 살균 처리한 후 사용하여 제조된 검체(檢體)를 A로 하고, 살균을 하지 않은 생황토(生黃土)를 직접 사용하여 제조된 검체를 B로 하여 제조된 정수에 대하여 각각의 미네랄 함유량을 평가한 결과는 다음 표 2와 같다.The ocher added to prepare the purified water of the present invention was ground water: ocher ratio of 5: 1, and the sample was prepared by sterilizing the ocher for 15 minutes at 121 ° C. in an auto clave in advance. As a result of evaluating the respective mineral content with respect to the purified water prepared by using B as a raw material without direct sterilization (生 黃土), the results are shown in Table 2 below.
본 실험은 대전에 소재하는 기초과학연구소(Tel. 042-865-3440∼9) 동위원소팀에 분석의뢰하여 이루어졌다.This experiment was conducted by requesting an isotope team to the Institute of Basic Science (Tel. 042-865-3440-9) in Daejeon.
표 2에서 알 수 있는 바와 같이, 본 발명 물시료는 Al(200>), Cr(50>), Mn(300>), As(50>), Se(10>) 이하로서 음료수로서 적합한 것을 확인하였으며 생황토를 사용하여 제조된 정수의 미네랄 함량이 높아 알칼리도가 높았음이 확인되었다.As can be seen from Table 2, the water sample of the present invention was found to be suitable as a beverage with Al (200>), Cr (50>), Mn (300>), As (50>), Se (10>) or less. It was confirmed that the alkalinity was high due to the high mineral content of purified water prepared using fresh loess.
실험예 3 : 본 발명 제품 정수의 살균효과 실험Experimental Example 3 Experiment of Sterilization Effect of Water Purification Products of the Invention
본 발명 방법과 시스템을 이용하여 제조된 본 발명 제품 정제수의 살균효과를 시험하기 위하여 본 발명자들에 의하여 제작된 UV sterilizer HS-4HW에 검체를 통과시킨 결과 살균율은 다음 표 3과 같다.In order to test the sterilization effect of the purified water of the product of the present invention prepared using the method and system of the present invention, the sterilization rate of the result of passing the sample through the UV sterilizer HS-4HW produced by the present inventors is shown in Table 3 below.
상기 실험결과와 같이 본 발명 살균장치를 통과하는 경우 모든 Microbes와 Bacteria가 살균되는 것을 확인할 수 있었다.When passing through the sterilization apparatus of the present invention as shown in the experimental results it was confirmed that all the microbes and Bacteria sterilized.
이상 실시예와 실험예를 통하여 확인되는 바와 같이, 본 발명은 지금까지 존재하지 아니하는 미네랄이 다량 함유된 신규한 알칼리성 정제수를 제공하는 효과가 있다. 그 뿐만 아니라, 본 발명 방법 및 시스템에 의하면 오염된 지하수, 지표수, 수도수 어느것이든 정제하여 사용할 수 있게되어 환경공해가 없는 새로운 type의 신규한 음료를 제공하는 뛰어난 효과가 있으므로 음료산업 및 환경산업상 매우 유용한 발명인 것이다.As confirmed through the above examples and experimental examples, the present invention has the effect of providing a novel alkaline purified water containing a large amount of minerals that do not exist so far. In addition, according to the method and system of the present invention, any contaminated groundwater, surface water, or tap water can be purified and used, thereby providing an excellent effect of providing a new type of new drink without environmental pollution. It is a very useful invention.
Claims (6)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AU55334/99A AU5533499A (en) | 1999-08-28 | 1999-09-04 | Purified, alkaline water rich in minerals and process for preparing the same |
| PCT/KR1999/000522 WO2001016033A1 (en) | 1999-08-28 | 1999-09-04 | Purified, alkaline water rich in minerals and process for preparing the same |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR19990035246 | 1999-08-24 | ||
| KR1019990035246 | 1999-08-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR19990078990A true KR19990078990A (en) | 1999-11-05 |
Family
ID=54765618
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019990036099A KR19990078990A (en) | 1999-08-24 | 1999-08-28 | Refined alkali water and process for preparation of the same |
Country Status (1)
| Country | Link |
|---|---|
| KR (1) | KR19990078990A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100394196B1 (en) * | 2000-06-30 | 2003-08-06 | 박기문 | A Mineral health beverage which in made from mudyellow-water and manufacturing method thereof |
| KR20040005301A (en) * | 2002-07-09 | 2004-01-16 | 류연수 | a manufacturing method of unrefined rice wine |
| KR100798273B1 (en) * | 2007-07-31 | 2008-01-24 | 유영수 | A device and method of manufacturing purified yellow ocher water |
| KR20220141484A (en) * | 2021-04-13 | 2022-10-20 | 이상언 | Method for producing kimchi using ginseng |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5567388A (en) * | 1978-11-16 | 1980-05-21 | Kiichiro Nakajima | Manufacture of mineral water |
| KR960036907A (en) * | 1995-04-07 | 1996-11-19 | 류도옥 | Hydroponic Cultivation Method of Edible Herbs Using Yellow Clay Water |
| KR19980033476A (en) * | 1998-04-17 | 1998-07-25 | 조삼태 | Water Purification Method Using Loess |
| KR19990015582A (en) * | 1997-08-02 | 1999-03-05 | 안갑환 | Development of ocher filter media for water purifiers |
| KR19990046755A (en) * | 1999-04-21 | 1999-07-05 | 김갑태 | Method of fabrication alcoholic liquors using solution of yellow soil as diluted solution |
-
1999
- 1999-08-28 KR KR1019990036099A patent/KR19990078990A/en active Search and Examination
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5567388A (en) * | 1978-11-16 | 1980-05-21 | Kiichiro Nakajima | Manufacture of mineral water |
| KR960036907A (en) * | 1995-04-07 | 1996-11-19 | 류도옥 | Hydroponic Cultivation Method of Edible Herbs Using Yellow Clay Water |
| KR19990015582A (en) * | 1997-08-02 | 1999-03-05 | 안갑환 | Development of ocher filter media for water purifiers |
| KR19980033476A (en) * | 1998-04-17 | 1998-07-25 | 조삼태 | Water Purification Method Using Loess |
| KR19990046755A (en) * | 1999-04-21 | 1999-07-05 | 김갑태 | Method of fabrication alcoholic liquors using solution of yellow soil as diluted solution |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100394196B1 (en) * | 2000-06-30 | 2003-08-06 | 박기문 | A Mineral health beverage which in made from mudyellow-water and manufacturing method thereof |
| KR20040005301A (en) * | 2002-07-09 | 2004-01-16 | 류연수 | a manufacturing method of unrefined rice wine |
| KR100798273B1 (en) * | 2007-07-31 | 2008-01-24 | 유영수 | A device and method of manufacturing purified yellow ocher water |
| KR20220141484A (en) * | 2021-04-13 | 2022-10-20 | 이상언 | Method for producing kimchi using ginseng |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US5405532A (en) | Process for the purification of industrial waste-waters | |
| CA2079820C (en) | Mixed filter bed composition and method of use | |
| KR100955914B1 (en) | Device and Method for Producing Drinking Water by Treating Waste Water | |
| US7678278B2 (en) | Method of treating water with an inorganic powder reagent | |
| EP1838623B1 (en) | Filter media and process to prepare the same | |
| JPH0415035B2 (en) | ||
| JPH04227099A (en) | Method for purifying underground water and waste water | |
| KR19990078990A (en) | Refined alkali water and process for preparation of the same | |
| Reddy et al. | Water treatment process in pharma industry-A review | |
| KR20000012503A (en) | Massage pack composition for removing skin effate matterials | |
| KR102036844B1 (en) | Method for preparation of organic germamium from granite | |
| KR101709476B1 (en) | Mineral oil-containing waste water purification system | |
| KR20000012567A (en) | Yellow soil panel and said manufacturing process | |
| Yettefti et al. | Performance evaluation of sand filter for tertiary treatment of secondary effluent of wastewater: effect of hydraulic loading evaluation des performances des filtres a sable pour le traitement tertiaire de l’effluent secondaire des eaux usees: effet de la charge hydraulique | |
| Kiran et al. | Remediation of textile effluents via physical and chemical methods for a safe environment | |
| KR20000012329A (en) | Refined alkali water and process for preparation of the same | |
| KR20000012359A (en) | Non-polluted alkaline washing compound | |
| KR20000012821A (en) | Refined alkaline water for culturing fishes and process for preparation of the same | |
| Patel et al. | Nanofiltration applications for potable water, treatment, and reuse | |
| KR20030027460A (en) | Water Purification method | |
| KR20000012502A (en) | Non-polluted soap for skin massage | |
| Dean | Processes for water reclamation | |
| KR20000012566A (en) | Yellow soil brick composition and the said manufacturing process | |
| KR20000017924A (en) | Yellow soil mortar composition and the said manufacturing process | |
| Hidayah et al. | Performance of Alum Coagulation and Adsorption on Removing Organic Matter and E. coli |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A201 | Request for examination |