KR19990022175A - 시클로헥사논 옥심 및 카프로락탐의 제조 방법 - Google Patents

시클로헥사논 옥심 및 카프로락탐의 제조 방법 Download PDF

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Publication number
KR19990022175A
KR19990022175A KR1019970708654A KR19970708654A KR19990022175A KR 19990022175 A KR19990022175 A KR 19990022175A KR 1019970708654 A KR1019970708654 A KR 1019970708654A KR 19970708654 A KR19970708654 A KR 19970708654A KR 19990022175 A KR19990022175 A KR 19990022175A
Authority
KR
South Korea
Prior art keywords
formic acid
mixture
cyclohexanone oxime
hydroxylammonium
cyclohexanone
Prior art date
Application number
KR1019970708654A
Other languages
English (en)
Korean (ko)
Inventor
프란츠-요셉 바이쓰
휴고 푹스
에버하르트 푹스
톰 비첼
Original Assignee
스타르크, 카르크
바스프 악티엔게젤샤프트
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 스타르크, 카르크, 바스프 악티엔게젤샤프트 filed Critical 스타르크, 카르크
Publication of KR19990022175A publication Critical patent/KR19990022175A/ko

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/42Platinum
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/082Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14Hydroxylamine; Salts thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32Oximes
    • C07C251/34Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C251/44Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups being part of a ring other than a six-membered aromatic ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/41Preparation of salts of carboxylic acids
    • C07C51/412Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D201/00Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02Preparation of lactams
    • C07D201/04Preparation of lactams from or via oximes by Beckmann rearrangement
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00Systems containing only non-condensed rings
    • C07C2601/12Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14The ring being saturated
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/52Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Catalysts (AREA)
KR1019970708654A 1995-06-02 1996-05-24 시클로헥사논 옥심 및 카프로락탐의 제조 방법 KR19990022175A (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19520271.6 1995-06-02
DE19520271A DE19520271A1 (de) 1995-06-02 1995-06-02 Verfahren zur Herstellung von Cyclohexanonoxim und Caprolactam

Publications (1)

Publication Number Publication Date
KR19990022175A true KR19990022175A (ko) 1999-03-25

Family

ID=7763514

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019970708654A KR19990022175A (ko) 1995-06-02 1996-05-24 시클로헥사논 옥심 및 카프로락탐의 제조 방법

Country Status (12)

Country Link
EP (1) EP0828707A1 (ru)
JP (1) JPH11506440A (ru)
KR (1) KR19990022175A (ru)
CN (1) CN1186484A (ru)
AU (1) AU6000196A (ru)
BR (1) BR9608960A (ru)
CZ (1) CZ359197A3 (ru)
DE (1) DE19520271A1 (ru)
EA (1) EA199700443A1 (ru)
PL (1) PL323676A1 (ru)
TW (1) TW342383B (ru)
WO (1) WO1996038407A1 (ru)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1091763C (zh) * 1999-07-26 2002-10-02 巴陵石化鹰山石油化工厂 一种防止磷酸羟胺肟化法制造己内酰胺的无机液中羟胺分解的方法
CN102626645B (zh) * 2012-03-27 2013-11-27 长沙理工大学 氟石膏在酮肟Beckmann重排中的应用
CN109453820A (zh) * 2018-11-27 2019-03-12 中国天辰工程有限公司 一种液相贝克曼重排催化剂及其制备方法和应用
CN115819344A (zh) * 2023-01-13 2023-03-21 神马实业股份有限公司 液相贝克曼重排生产己内酰胺同时副产硫酸酯的工艺方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2721199A (en) * 1953-12-15 1955-10-18 Du Pont Production of amides or lactams from oximes
NL301053A (ru) * 1963-11-27
US4105575A (en) * 1976-10-12 1978-08-08 Imc Chemical Group, Inc. Partial resolution of pentaerythritol waste liquors
DE4311420A1 (de) * 1993-04-07 1994-10-13 Basf Ag Hydrierungskatalysator auf der Basis eines mit feinteiligem Schwefel partiell vergifteten Platinmetalls

Also Published As

Publication number Publication date
AU6000196A (en) 1996-12-18
TW342383B (en) 1998-10-11
MX9708928A (es) 1998-03-31
CN1186484A (zh) 1998-07-01
EA199700443A1 (ru) 1998-06-25
JPH11506440A (ja) 1999-06-08
BR9608960A (pt) 1999-05-04
CZ359197A3 (cs) 1998-04-15
DE19520271A1 (de) 1996-12-05
PL323676A1 (en) 1998-04-14
WO1996038407A1 (de) 1996-12-05
EP0828707A1 (de) 1998-03-18

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