PL323676A1 - Method of obtaining cyclohexanone and caprolactam oxime - Google Patents

Method of obtaining cyclohexanone and caprolactam oxime

Info

Publication number
PL323676A1
PL323676A1 PL96323676A PL32367696A PL323676A1 PL 323676 A1 PL323676 A1 PL 323676A1 PL 96323676 A PL96323676 A PL 96323676A PL 32367696 A PL32367696 A PL 32367696A PL 323676 A1 PL323676 A1 PL 323676A1
Authority
PL
Poland
Prior art keywords
caprolactam
oxime
obtaining cyclohexanone
cyclohexanone
obtaining
Prior art date
Application number
PL96323676A
Inventor
Franz-Josef Weiss
Hugo Fuchs
Eberhard Fuchs
Tom Witzel
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of PL323676A1 publication Critical patent/PL323676A1/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/42Platinum
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/082Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14Hydroxylamine; Salts thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32Oximes
    • C07C251/34Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C251/44Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups being part of a ring other than a six-membered aromatic ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/41Preparation of salts of carboxylic acids
    • C07C51/412Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D201/00Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02Preparation of lactams
    • C07D201/04Preparation of lactams from or via oximes by Beckmann rearrangement
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00Systems containing only non-condensed rings
    • C07C2601/12Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14The ring being saturated
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/52Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
PL96323676A 1995-06-02 1996-05-24 Method of obtaining cyclohexanone and caprolactam oxime PL323676A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19520271A DE19520271A1 (en) 1995-06-02 1995-06-02 Process for the preparation of cyclohexanone oxime and caprolactam
PCT/EP1996/002240 WO1996038407A1 (en) 1995-06-02 1996-05-24 Process for producing cyclohexanonoxim and caprolactam

Publications (1)

Publication Number Publication Date
PL323676A1 true PL323676A1 (en) 1998-04-14

Family

ID=7763514

Family Applications (1)

Application Number Title Priority Date Filing Date
PL96323676A PL323676A1 (en) 1995-06-02 1996-05-24 Method of obtaining cyclohexanone and caprolactam oxime

Country Status (12)

Country Link
EP (1) EP0828707A1 (en)
JP (1) JPH11506440A (en)
KR (1) KR19990022175A (en)
CN (1) CN1186484A (en)
AU (1) AU6000196A (en)
BR (1) BR9608960A (en)
CZ (1) CZ359197A3 (en)
DE (1) DE19520271A1 (en)
EA (1) EA199700443A1 (en)
PL (1) PL323676A1 (en)
TW (1) TW342383B (en)
WO (1) WO1996038407A1 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1091763C (en) * 1999-07-26 2002-10-02 巴陵石化鹰山石油化工厂 Method for preventing hydroxylamine from decomposing in inorganic solution for preparing caprolactam by using hydroxylamine phosphate oximation method
CN102626645B (en) * 2012-03-27 2013-11-27 长沙理工大学 Application of fluorgypsum in ketoxime Beckmann rearrangement
CN109453820A (en) * 2018-11-27 2019-03-12 中国天辰工程有限公司 A kind of liquid phase Beckmann rearrangement catalyst and its preparation method and application
CN115819344A (en) * 2023-01-13 2023-03-21 神马实业股份有限公司 Process method for producing caprolactam and coproducing sulfuric ester by liquid phase Beckmann rearrangement

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2721199A (en) * 1953-12-15 1955-10-18 Du Pont Production of amides or lactams from oximes
NL301053A (en) * 1963-11-27
US4105575A (en) * 1976-10-12 1978-08-08 Imc Chemical Group, Inc. Partial resolution of pentaerythritol waste liquors
DE4311420A1 (en) * 1993-04-07 1994-10-13 Basf Ag Hydrogenation catalyst based on a platinum metal partially poisoned with finely divided sulfur

Also Published As

Publication number Publication date
MX9708928A (en) 1998-03-31
EA199700443A1 (en) 1998-06-25
CN1186484A (en) 1998-07-01
AU6000196A (en) 1996-12-18
WO1996038407A1 (en) 1996-12-05
CZ359197A3 (en) 1998-04-15
JPH11506440A (en) 1999-06-08
KR19990022175A (en) 1999-03-25
BR9608960A (en) 1999-05-04
TW342383B (en) 1998-10-11
DE19520271A1 (en) 1996-12-05
EP0828707A1 (en) 1998-03-18

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