MX9708928A - Process for producing cyclohexanonoxim and caprolactam. - Google Patents

Process for producing cyclohexanonoxim and caprolactam.

Info

Publication number
MX9708928A
MX9708928A MX9708928A MX9708928A MX9708928A MX 9708928 A MX9708928 A MX 9708928A MX 9708928 A MX9708928 A MX 9708928A MX 9708928 A MX9708928 A MX 9708928A MX 9708928 A MX9708928 A MX 9708928A
Authority
MX
Mexico
Prior art keywords
cyclohexanonoxim
caprolactam
producing
production
hydroxyl ammonium
Prior art date
Application number
MX9708928A
Other languages
Spanish (es)
Other versions
MXPA97008928A (en
Inventor
Franz-Josef Weiss
Hugo Fuchs
Eberhard Fuchs
Tom Witzel
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of MX9708928A publication Critical patent/MX9708928A/en
Publication of MXPA97008928A publication Critical patent/MXPA97008928A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D201/00Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02Preparation of lactams
    • C07D201/04Preparation of lactams from or via oximes by Beckmann rearrangement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/42Platinum
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/082Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14Hydroxylamine; Salts thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32Oximes
    • C07C251/34Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C251/44Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups being part of a ring other than a six-membered aromatic ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/41Preparation of salts of carboxylic acids
    • C07C51/412Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00Systems containing only non-condensed rings
    • C07C2601/12Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14The ring being saturated
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/52Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)

Abstract

The production of cyclohexanonoxim by the reaction of cyclohexanone with a hydroxyl ammonium salt, i.e. hydroxyl ammonium formiate, and the production of caprolactam by the Beckmann rearrangement of cyclohexanonoxim in a C1-C4 carboxylic acid.
MXPA/A/1997/008928A 1995-06-02 1997-11-19 Preparation of ciclohexanona oxima and caprolact MXPA97008928A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19520271A DE19520271A1 (en) 1995-06-02 1995-06-02 Process for the preparation of cyclohexanone oxime and caprolactam
DE19520271.6 1995-06-02
PCT/EP1996/002240 WO1996038407A1 (en) 1995-06-02 1996-05-24 Process for producing cyclohexanonoxim and caprolactam

Publications (2)

Publication Number Publication Date
MX9708928A true MX9708928A (en) 1998-03-31
MXPA97008928A MXPA97008928A (en) 1998-10-15

Family

ID=

Also Published As

Publication number Publication date
PL323676A1 (en) 1998-04-14
EA199700443A1 (en) 1998-06-25
CN1186484A (en) 1998-07-01
AU6000196A (en) 1996-12-18
WO1996038407A1 (en) 1996-12-05
CZ359197A3 (en) 1998-04-15
JPH11506440A (en) 1999-06-08
KR19990022175A (en) 1999-03-25
BR9608960A (en) 1999-05-04
TW342383B (en) 1998-10-11
DE19520271A1 (en) 1996-12-05
EP0828707A1 (en) 1998-03-18

Similar Documents

Publication Publication Date Title
MX9409080A (en) Titanium dioxide dispersibility.
PL314527A1 (en) Caprolactam producing method
EP0666320A3 (en) Process for producing alpha-hydroxy acid or alpha-hydroxyamide by microorganisms.
CA2181481A1 (en) Method of biologically removing nitrogen and system therefor
PH31685A (en) Method of producing l-glutamic acid by fermentation.
BG100942A (en) Method for the production of nicotinic acid amide
ES2058029A1 (en) Process for the production of clavulanic acid salts
GB9220327D0 (en) Process
MX9708928A (en) Process for producing cyclohexanonoxim and caprolactam.
AU3559200A (en) Process for producing gabapentine of pharmaceutical grade
WO2001077068A3 (en) Process for preparing 6-aminocaproamide
TW338035B (en) Process for the production of enantiomerically-pure-azetidine-2-carboxylic acid
HU9202489D0 (en) Method for producing new n-alkylated 1,4-dihydro-pyridine-dicarboxylic acid esters and pharmaceutical preparatives containing said compounds
NZ332155A (en) Improved process for the production of enantiomerically-pure azetidine-2-carboxylic acid
EP0233733A3 (en) Process for producing n-phthaloyl-p-nitro-l-phenylalanine
WO1995021145A3 (en) FERMENTATION PRODUCTION OF LONG CHAIN α,φ-DICARBOXYLIC ACIDS FROM ALKANES BY USE OF A MICROORGANISM
AU2001223714A1 (en) Method for producing n-methyl-n'-nitroguanidine
EP0785188A4 (en) Process for the preparation of epsilon-caprolactam
YU33303A (en) Improved process for production of gabapentin intermediate
GR3021889T3 (en) Diacetyl production
AU5482001A (en) Method for producing caprolactam on the basis of 6-aminocapronitrile and subsequent purification by crystallization
ATE213234T1 (en) METHOD FOR PRODUCING 3-AMINO-1,2,4-BENZOTRIAZINE DIOXIDE
CA2246538A1 (en) Crystalline protease and method for producing same
EP0197408A3 (en) A method of preparing omega -lactams, in particular caprolactam
EP0593058A3 (en) Peptide-surfactant, production process thereof and microorganisms producing the same.