KR19990015782A - Method for preparing kelp beverages containing kelp extract as a main ingredient - Google Patents

Method for preparing kelp beverages containing kelp extract as a main ingredient Download PDF

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KR19990015782A
KR19990015782A KR1019970038084A KR19970038084A KR19990015782A KR 19990015782 A KR19990015782 A KR 19990015782A KR 1019970038084 A KR1019970038084 A KR 1019970038084A KR 19970038084 A KR19970038084 A KR 19970038084A KR 19990015782 A KR19990015782 A KR 19990015782A
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kelp
extract
present
preparing
extraction
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KR1019970038084A
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Korean (ko)
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김우준
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조성문
주식회사 산하종합식품
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Abstract

본 발명은 다시마에 함유된 식물성 섬유이면서 생리활성을 갖는 알긴산, 푸고이단, 라미나린, 클로로필 등과 칼륨, 칼슘 등의 미네랄성분, 비타민 등을 열수 추출 또는 산성 추출하여 당류와 유기산을 첨가하여 다시마 추출물을 주성분으로 하는 다시마음료의 제조방법에 관한 발명이다. 본 발명의 다시마는 남해안의 청정해역에서 채취된 깨끗한 다시마를 수세, 분쇄, 추출, 원심분리, 여과 등을 거쳐 수용성 다당류와 미네랄, 클로로필 등을 열수 추출한 후 잔사에 산성용액을 가하여 생리활성물질과 해조다당류를 추출하여 얻은 이상의 두가지 추출물을 혼합하는 것을 특징으로 하는 다시마음료 제조방법으로서 본 발명에 의해 제조된 다시마음료는 맛과 향취가 좋고 몸에 좋은 영양성분이 풍부할 뿐만 아니라 우리나라 청정해역의 풍부한 수산자원을 원료로 자급할 수 있어서 어민의 소득증대에 크게 기여할 수 있을 것이다.The present invention is a vegetable fiber contained in kelp and physiologically active alginate, fugoidan, laminarin, chlorophyll and other minerals, such as potassium, calcium, hot water extraction or acidic extraction by adding sugars and organic acids to extract the kelp extract The present invention relates to a method for producing a kelp beverage containing as a main component. The kelp of the present invention is a hot kelp collected in the clean waters of the south coast through water washing, grinding, extraction, centrifugation, filtration, etc., and then hot water extraction of water-soluble polysaccharides and minerals, chlorophyll, etc. As a method for preparing kelp beverages, characterized by mixing two or more extracts obtained by extracting polysaccharides, the kelp beverage prepared according to the present invention is not only rich in flavor and flavor and good for nutrients, but also rich in fisheries in Korea's clean waters. Resources can be self-sustaining, which will greatly contribute to the income increase of fishermen.

Description

다시마 추출물을 주성분으로 하는 다시마 음료의 제조방법Method for preparing kelp beverages containing kelp extract as a main ingredient

본원 발명은 다시마에 함유된 식물성 섬유이면서 생리활성을 갖는 알긴산, 푸고이단, 라미나린 등과, 칼륨, 칼슘 등의 미네랄 성분, 클로로필 등을 중성의 열수에서 추출하고, 잔사에 산성용액을 첨가하여 잔류성분을 재차 추출하여 당류, 유기산 등을 혼합한 다시마를 주성분으로 한 다시마 음료의 제조방법에 관한 발명이다.The present invention extracts alginic acid, fugoidan, laminarin, and the like, vegetable fibers and physiological activity in kelp, mineral components such as potassium and calcium, chlorophyll and the like from neutral hot water, and an acidic solution is added to the residue to remove residual components. The present invention relates to a method for preparing a kelp beverage mainly containing kelp mixed with sugars, organic acids, and the like.

다시마는 전통적인 해조식품으로서 대소사의 음식상에 국물요리나 고급요리의 조미료로 애용되어 왔다. 다시마와 관련된 음료의 제조방법에 관한 선행기술로서 한국특허출원 91-11992(공개93-1825) 미역,다시마를 이용한 음료의 제조방법과 한국특허출원 95-15089(공개97-86)미역귀를 주성분으로 한 쥬스 제조방법 등이 있으나 다시마 그 자체를 이용하여 음료나 쥬스를 제조하는 방법이므로 식감이 좋지 못하고 맛과 향기 등이 강하여 음료로서 부적합한 면이 없지 않다.Kelp is a traditional seaweed food that has been widely used as a seasoning for soup and high-quality dishes on foods of major sosa. As a prior art related to a method for preparing a beverage related to kelp, Korean Patent Application No. 91-11992 (Publication 93-1825), a method for preparing a beverage using seaweed and kelp, and Korean Patent Application No. 95-15089 (Publication 97-86) There is a juice production method, etc., but it is a method of preparing a drink or juice using kelp itself, so the texture is not good and the taste and fragrance are strong, so it is not suitable as a drink.

해조류 중에서 미역과 더불어 다시마 성분의 생리활성에 대한 연구는 많이 이루어져 일본과 한국에서도 알긴산을 주재로 한 음료가 상품화되었고, 다시마를 갈아서 퓨레를 만들어 조미료나 약용으로 판매되고 있으나 음료로 상품화된 사례는 없는 것으로 알려져 있다. 다시마는 각종 영양성분과 알긴산, 푸고이단, 라미나린 등 생리활성성분과 크로로필 등의 수용성 식물섬유의 장내기능, 칼륨과 칼슘 등의 무기물과 비타민은 체내 신진대사를 촉진시키는 물질로서 음료로 개발한다면 현대인의 영양불균형이나 생리활성성분을 보충할 수 있어서 건강음료로서 기대가 모아진다.Among seaweeds, research on the biological activity of kelp ingredients along with seaweed was commercialized, and beverages based on alginic acid were commercialized in Japan and Korea, and puree from kelp is sold as seasonings or medicinal products, but there are no commercialized beverages. It is known. Kelp is a nutritious ingredient, physiologically active ingredients such as alginic acid, fugoidan, and laminarin, intestinal function of water-soluble plant fiber such as chlorophyll, minerals such as potassium and calcium, and vitamins are developed as beverages to promote metabolism in the body. If you can supplement the nutritional imbalances and physiologically active ingredients of modern people, expectations are raised as a health drink.

다시마에 들어 있는 주요성분으로서 알긴산은 콜레스테롤 저하로 동맥경화 예방, 소금으로부터 오는 고혈압 예방, 중금속 배설로 중독 예방과 푸코이단은 콜레스테롤 저하로 동맥경화 예방, 혈전예방과 라미나린은 혈압강화작용으로 고혈압 예방과 푸코스테롤은 혈중콜레스테롤 저하로 동맥경화 예방과 클로로필은 입냄새 제거로 청량감과 EPA는 혈소판응집제로 혈전 예방과 식이섬유는 대장암 예방, 변비 예방, 당뇨병 예방과 칼슘은 골격강화와 골다공증 예방 및 혈압강하와 마그네슘은 심장병 예방과 철은 빈혈 예방과 요드 인은 갑상선 호르몬 형성에 좋은 것으로 알려져 있다.As the main ingredient in kelp, alginic acid prevents arteriosclerosis by lowering cholesterol, prevents high blood pressure from salt, prevents poisoning by excretion of heavy metals, and fucoidan prevents arteriosclerosis by lowering cholesterol, prevents blood clots, and laminarin prevents hypertension. Fucosterol lowers blood cholesterol, prevents arteriosclerosis, and chlorophyll removes bad breath. EPA is a platelet coagulant. Blood clots are prevented. Magnesium and magnesium are known to help prevent heart disease, iron to prevent anemia, and iodine to form thyroid hormones.

다시마차는 일본 등지에서 다시마를 건조하여 분쇄한 후 물에 타서 마시는데 수불용성 물질이 많아서 완전히 녹지 않고 하부로 침전하기 때문에 마시기에 불편하고 잔유물이 거부감을 준다. 또한 다시마 퓨레나 농축물을 약용으로 사용하기도 하지만 음료로 상품화된 사례는 없다.Kelp tea is dried and crushed in Japan and dried, and then consumed in water to drink. It is inconvenient to drink because the water insoluble substance is not completely dissolved and settles to the bottom. They also use kelp purena concentrate for medicinal purposes, but there are no commercialized beverages.

본 발명은 다시마에 함유된 유용성분을 효율적으로 추출하고자 많은 연구를 거듭한 끝에 중성역에서 열수로 1차 추출하고, 그 잔사를 산성용액으로 부분적인 가수분해를 하여 수용성의 유용성분을 최대한 추출하는 방법을 개발하여 본 발명을 완성하였다. 이때 과도한 산분해를 하게 되면 유용한 생리활성물질이 산가수분해되어 소실되므로 부분적인 가수분해조건을 확립하는 것이 아주 중요하다. 본 발명자는 다시마에 함유된 전술한 성분을 추출하기 위하여 마쇄, 자숙 등의 방법으로 수많은 실험을 통하여 확인해 보았으나 미량의 유효성분만이 유리된다는 것을 알게 되었다. 이러한 문제점을 개선하고자 연구한 끝에 특정의 산성영역에서 추출효율이 높다는 것을 알고 본원발명을 완성하게 되었다.The present invention is to extract the useful components contained in the kelp efficiently after a lot of research to the primary extraction with hot water in the neutral zone, the residue is partially hydrolyzed with an acidic solution to extract the water-soluble useful components to the maximum The method was developed to complete the present invention. At this time, it is very important to establish partial hydrolysis conditions because excessive biodegradation results in acid hydrolysis and loss of useful bioactive substances. The present inventors have confirmed through numerous experiments by grinding, cooking, etc. in order to extract the above-mentioned ingredients contained in kelp, but found that only a small amount of active ingredient is released. After researching to improve these problems, the present invention was completed, knowing that the extraction efficiency is high in a specific acidic region.

소건품 다시마의 일반적인 성분은 수분 12.1%, 단백질 7.2%, 지방 1.1%, 탄수화물 45.9%, 회분 33.7%, 칼슘 712mg, 인 182mg, 철 7.2mg, 비타민 325 IU 함유되어 있다. 생리활성물질로 알려진 알긴산, 푸코이단, 라미나린, 푸코스테롤, 클로로필, EPA 등은 상기의 성분들 중에 미량으로 함유되어 있는 것을 알려져 있다.Common constituents of dried kelp are water 12.1%, protein 7.2%, fat 1.1%, carbohydrate 45.9%, ash 33.7%, calcium 712mg, phosphorus 182mg, iron 7.2mg, vitamin 325 IU. Alginic acid, fucoidan, laminarin, fucosterol, chlorophyll, EPA, and the like, which are known as bioactive substances, are known to be contained in trace amounts in the above components.

제 1 도는 다시마 음료의 제조공정도이다.1 is a manufacturing process of kelp beverages.

* 제 1 공정* 1st process

다시마 원료는 완도의 원근해역에서 양식된 다시마로 염처리하여 저온으로 보존된 것을 다시마의 5배의 수돗물로 3회 세척한다. 마쇄기를 이용하여 세포막이 파괴되도록 마쇄하고 10-30배의 물로 90℃에서 30-60분간 추출한 후 상등액을 분리하여 다시마 추출액을 얻는다.The kelp raw material is salted with kelp farmed in the near sea of Wando and washed three times with tap water of 5 times that of kelp. Using a grinding machine, the cell membrane is crushed to break, extracted with 10-30 times of water at 90 ° C. for 30-60 minutes, and the supernatant is separated to obtain a kelp extract.

* 제 2 공정2nd process

잔사를 재차 마쇄한 후에 구연산을 첨가하여 pH 2.5-4.0으로 조절하여 60-80℃에서 30-60분간 추출한 후 탄산소다로 중화하고 원심분리하여 다시마추출액을 얻는다.After the residue was triturated again, citric acid was added to adjust the pH to 2.5-4.0, extracted at 60-80 ° C. for 30-60 minutes, neutralized with sodium carbonate and centrifuged to obtain a kelp extract.

* 제 3 공정3rd process

제 1 공정과 제 2 공정에서 얻은 다시마추출액을 합하여 20배의 물로 희석하여 올리고당과 포도당 그리고 구연산을 첨가하여 다시마음료를 제조한 후 여과, 살균, 포장한다.The kelp extracts obtained in the first and second processes are combined and diluted with 20 times water. Oligosaccharides, glucose and citric acid are added to prepare kelp beverages, followed by filtration, sterilization and packaging.

[실시예 1]Example 1

다시마 1kg에 물 5ℓ를 가하여 수돗물로 3회에 걸쳐 세척한다. 다시마를 1-2 mm 크기로 미세하게 마쇄하여 물 30ℓ를 가하여 90℃에서 1시간 동안 교반하면서 추출하여 원심분리한 후 열수에 의한 다시마 추출물을 얻었다.5 kg of water is added to 1 kg of kelp and washed three times with tap water. The kelp was finely pulverized to a size of 1-2 mm, 30 L of water was added thereto, extracted with stirring at 90 ° C. for 1 hour, and centrifuged to obtain kelp extracts by hot water.

[실시예 2]Example 2

잔사를 재차 미세하게 마쇄하여 구연산을 사용하여 pH 3.0으로 조절하고 60℃에서 30분간 추출한 후 탄산소다로 pH 6.5로 조절하여 원심분리하고 산가수분해에 의한 다시마추출물을 얻었다.The residue was finely ground again, adjusted to pH 3.0 using citric acid, extracted at 60 ° C. for 30 minutes, adjusted to pH 6.5 with sodium carbonate, and centrifuged to obtain kelp extract by acid hydrolysis.

[실시예 3]Example 3

제 1 공정과 제 2 공정에서 얻은 추출물을 합하여 96.5중량부를 넣고 20배의 물로 희석하여 포도당 1.5중량부와 올리고당 2.0중량부를 혼합하고 구연산으로 pH 6.5로 조절한 후 여과, 살균, 포장하여 다시마음료를 제조하였다.96.5 parts by weight of the extract obtained in the first and second steps were combined, diluted with 20 times of water, 1.5 parts by weight of glucose and 2.0 parts by weight of oligosaccharide were mixed, adjusted to pH 6.5 with citric acid, filtered, sterilized and packaged. Prepared.

[비교예][Comparative Example]

다시마 1kg에 수돗물 5ℓ를 가하여 3회에 걸쳐 세척하고, 다시마를 1-2 mm 크기로 미세하게 마쇄하여 물 30ℓ를 가하여 90℃에서 1시간 동안 교반하면서 추출하여 원심분리한 후 열수에 의한 다시마 추출물을 얻었다. 추출물을 여과하여 물 20배로 희석하여 추출물 96.5중량부에 포도당 1.5중량부와 올리고당 2.0중량부를 혼합하여 구연산으로 pH 6.5로 한 후 여과, 살균, 포장하여 다시마음료를 제조하였다.5 kg of tap water was added to 1 kg of kelp and washed three times. The kelp was finely pulverized to a size of 1-2 mm, 30 L of water was added thereto, stirred at 90 ° C. for 1 hour, centrifuged, and the kelp extract by hot water was extracted. Got it. The extract was filtered and diluted with 20 times of water, 96.5 parts by weight of the extract was mixed with 1.5 parts by weight of glucose and 2.0 parts by weight of oligosaccharides to pH 6.5 with citric acid, and then filtered, sterilized and packaged to prepare a kelp beverage.

[관능검사][Sensory test]

이상의 실시예에서 제조된 다시마음료와 단순히 열수추출하여 얻은 비교예의 추출물을 대조군으로 하여 남녀 각각 5명(계10명)에게 맛 12점, 향 4점, 색도 4점 만점으로 하여 다시마음료 음용후의 종합적인 맛과 피로 회복효과를 관능검사하였다.Using tangle extract prepared in the above example and the extract of the comparative example obtained by simply extracting hot water as a control group, five men and women (10 persons) each had 12 points of taste, 4 points of flavor, and 4 points of chromaticity. Sensory evaluation was conducted to evaluate taste and fatigue recovery.

[표 1]TABLE 1

다시마음료의 관능검사 결과Sensory test result of kelp drink

[표 2]TABLE 2

피로회복에 대한 다시마음료의 관능검사 결과Sensory Test Results of Kelp Beverage for Fatigue Recovery

상기의 표 1 및 표 2 의 결과로부터 알 수 있듯이 본 발명의 음료는 맛, 향 및 색도 등이 기호성이 우수하며 뛰어난 피로회복 효과를 지니는 것을 알 수 있었다.As can be seen from the results of Table 1 and Table 2, the beverage of the present invention was found to have excellent palatability and excellent fatigue recovery effect in taste, aroma and color.

이상의 실시예는 본 발명을 설명하기 위한 것으로, 이들 실시예에 의하여 본 발명의 기술적 범위가 한정되는 것은 아니다.The above embodiments are for explaining the present invention, and the technical scope of the present invention is not limited by these examples.

다시마의 주성분인 알긴산, 푸코이산, 라미나린, 푸코스테롤, 클로로필, EPA, 식이섬유, 미네랄, 당, 아미노산 등의 성분을 추출하여 농축한 다시마추출물과 포도당, 올리고당, 구연산 등을 혼합한 다시마음료는 생리활성물질과 영양소가 골고루 혼합되어 있어 맛과 영양면에서 뿐만 아니라 현대인의 피로회복에도 효과가 있는 다시마음료를 제공하므로서 소비자의 건강증진과 어민의 소득증대에 기여할 수 있다.The kelp beverage is a mixture of concentrated kelp extract, glucose, oligosaccharide, citric acid, etc., extracted from alginic acid, fucoic acid, laminarin, fucosterol, chlorophyll, EPA, dietary fiber, minerals, sugars and amino acids. Bio-active substances and nutrients are evenly mixed to provide kelp beverages that are effective not only in terms of taste and nutrition, but also in modern people's fatigue recovery, thereby contributing to the health of consumers and the income increase of fishermen.

Claims (2)

다시마를 마쇄하여 세포막이 파괴된 것을 80-95℃에서 30-60분간 추출하여 추출물을 얻고, 잔사를 재차 마쇄하여 산성용액하에서 60-80℃로 30-60분간 추출한 후, 알칼리용액으로 중화하여 분리한 추출물을 혼합하고 포도당, 올리고당, 구연산을 첨가하는 것을 특징으로 하는 다시마추출물을 주성분으로 하는 다시마음료의 제조방법.Grind the kelp to extract the cell membrane was broken for 30-60 minutes at 80-95 ℃, the residue was again milled and extracted for 30-60 minutes at 60-80 ℃ under acidic solution, neutralized with alkaline solution and separated A method for preparing kelp beverages containing kelp extract as a main component, which comprises mixing one extract and adding glucose, oligosaccharide and citric acid. 제 1 항에 있어서, 산성용액은 염산, 구연산, 사과산 또는 주석산 중에서 선택된 1종 이상으로 pH 2.5-3.5로 하여 추출하고, 알칼리용액은 가성소다, 탄산소다, 탄산칼슘 또는 소석회 중에서 선택된 1종 이상으로 pH 5.5-6.5로 중화하는 것을 특징으로 하는 다시마 추출물을 주성분으로 하는 다시마음료의 제조방법.The acidic solution is extracted at pH 2.5-3.5 with at least one selected from hydrochloric acid, citric acid, malic acid or tartaric acid, and the alkaline solution is at least one selected from caustic soda, sodium carbonate, calcium carbonate or slaked lime. A method for producing kelp beverages containing the kelp extract as a main ingredient, which is neutralized to pH 5.5-6.5.
KR1019970038084A 1997-08-09 1997-08-09 Method for preparing kelp beverages containing kelp extract as a main ingredient KR19990015782A (en)

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Cited By (11)

* Cited by examiner, † Cited by third party
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KR20000059703A (en) * 1999-03-08 2000-10-05 김재윤 Composition for beverage containing sea-tangle extract solution and chito-oligosaccharide
KR100367716B1 (en) * 2000-03-29 2003-01-14 윤의구 Manufacture of water soluble low-molecular alginate by autoclaving pretreatment and hot water extraction
KR20030018126A (en) * 2001-08-27 2003-03-06 한국수산주식회사 making method and composition for brown seaweed
KR100403423B1 (en) * 2000-10-17 2003-10-30 바램제약주식회사 Preparing method of beverage using seatangle powder and beverage prepared by the method
KR100405133B1 (en) * 2001-05-23 2003-11-12 대한민국 Beverage containing oligosaccharides of laminaria religiosa and process for the preparation thereof
KR100411508B1 (en) * 2001-02-23 2003-12-18 대한민국 Seaweed beverage mixed brown algae mold of green color and its processing knowhow
KR100441111B1 (en) * 2000-10-09 2004-07-21 전라남도 Drinks comprising glasswort extracts
KR100466248B1 (en) * 2002-04-26 2005-01-13 강원도 Beverage Composition Containing The Extracts of Laminaria and Manufacturing Method thereof
KR100584664B1 (en) * 2006-02-20 2006-05-29 주식회사 대영엔지니어링 Assembly type breakwater for weak pondside
KR101374617B1 (en) * 2012-11-12 2014-03-19 강원친환경 영농조합법인 Method for manufacturing grape extract from grape skin and seed, and grape extract produced thereby
KR20150134123A (en) 2014-05-21 2015-12-01 김윤규 Bread including seaweeds and method for producing thereof

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20000059703A (en) * 1999-03-08 2000-10-05 김재윤 Composition for beverage containing sea-tangle extract solution and chito-oligosaccharide
KR100367716B1 (en) * 2000-03-29 2003-01-14 윤의구 Manufacture of water soluble low-molecular alginate by autoclaving pretreatment and hot water extraction
KR100441111B1 (en) * 2000-10-09 2004-07-21 전라남도 Drinks comprising glasswort extracts
KR100403423B1 (en) * 2000-10-17 2003-10-30 바램제약주식회사 Preparing method of beverage using seatangle powder and beverage prepared by the method
KR100411508B1 (en) * 2001-02-23 2003-12-18 대한민국 Seaweed beverage mixed brown algae mold of green color and its processing knowhow
KR100405133B1 (en) * 2001-05-23 2003-11-12 대한민국 Beverage containing oligosaccharides of laminaria religiosa and process for the preparation thereof
KR20030018126A (en) * 2001-08-27 2003-03-06 한국수산주식회사 making method and composition for brown seaweed
KR100466248B1 (en) * 2002-04-26 2005-01-13 강원도 Beverage Composition Containing The Extracts of Laminaria and Manufacturing Method thereof
KR100584664B1 (en) * 2006-02-20 2006-05-29 주식회사 대영엔지니어링 Assembly type breakwater for weak pondside
KR101374617B1 (en) * 2012-11-12 2014-03-19 강원친환경 영농조합법인 Method for manufacturing grape extract from grape skin and seed, and grape extract produced thereby
KR20150134123A (en) 2014-05-21 2015-12-01 김윤규 Bread including seaweeds and method for producing thereof

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