KR19980702396A - 고 중합성 n-비닐카복실산 아미드 및 이의 제조방법 - Google Patents

고 중합성 n-비닐카복실산 아미드 및 이의 제조방법 Download PDF

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Publication number
KR19980702396A
KR19980702396A KR1019970705795A KR19970705795A KR19980702396A KR 19980702396 A KR19980702396 A KR 19980702396A KR 1019970705795 A KR1019970705795 A KR 1019970705795A KR 19970705795 A KR19970705795 A KR 19970705795A KR 19980702396 A KR19980702396 A KR 19980702396A
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KR
South Korea
Prior art keywords
acid amide
vinylcarboxylic acid
highly polymerizable
preparation
vinylcarboxylic
Prior art date
Application number
KR1019970705795A
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English (en)
Inventor
도시유키 아이자와
히토시 나카무라
구니토시 와카바야시
데츠오 구도
겐지 시마무라
순이치 나가마츠
Original Assignee
오하시 미츠오
쇼와 덴코 가부시키가이샤
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Application filed by 오하시 미츠오, 쇼와 덴코 가부시키가이샤 filed Critical 오하시 미츠오
Priority claimed from PCT/JP1995/002757 external-priority patent/WO1997024315A1/en
Publication of KR19980702396A publication Critical patent/KR19980702396A/ko

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/02—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C233/03—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to hydrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/22—Separation; Purification; Stabilisation; Use of additives
    • C07C231/24—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/02—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C233/04—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/02—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C233/04—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C233/05—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton having the nitrogen atoms of the carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F126/00—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen
    • C08F126/02—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen by a single or double bond to nitrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F26/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen
    • C08F26/02—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen by a single or double bond to nitrogen

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

본 발명은 N-1, 3-부타디에닐카복실산 아미드 함량이 30ppm 이하인 고중합성 N-비닐카복실산 아미드, 이의 제조방법 및 이를 이용한 N-비닐카복실산 아미드 단독중합체 또는 이와 공중합가능한 다른 단량체와의 공중합체의 제조방법에 관한 것이다. 또한, 고 중합성 N-비닐카복실산 아미드는 N-(1-알콕시에틸)카복실산 아미드 또는 에틸리덴비스카복실산 아미드의 열분해 또는 촉매 분해에 의해 생성되며, N-(1-알콕시에틸) 카복실산 아미드 또는 에틸리덴비스카복실산 아미드 중의 N-비닐카복실산 아미드 함량은 10 중량% 이하이다.
KR1019970705795A 1995-12-28 1995-12-28 고 중합성 n-비닐카복실산 아미드 및 이의 제조방법 KR19980702396A (ko)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/JP1995/002757 WO1997024315A1 (en) 1995-07-13 1995-12-28 Highly polymerizable n-vinylcarboxylic acid amide and production process thereof

Publications (1)

Publication Number Publication Date
KR19980702396A true KR19980702396A (ko) 1998-07-15

Family

ID=14126599

Family Applications (2)

Application Number Title Priority Date Filing Date
KR1019970705795A KR19980702396A (ko) 1995-12-28 1995-12-28 고 중합성 n-비닐카복실산 아미드 및 이의 제조방법
KR1019970705795A KR100389242B1 (ko) 1995-12-28 1995-12-28 고중합성n-비닐카복실산아미드및이의제조방법

Family Applications After (1)

Application Number Title Priority Date Filing Date
KR1019970705795A KR100389242B1 (ko) 1995-12-28 1995-12-28 고중합성n-비닐카복실산아미드및이의제조방법

Country Status (6)

Country Link
KR (2) KR19980702396A (ko)
CN (1) CN1082943C (ko)
AT (1) ATE214690T1 (ko)
AU (1) AU716698B2 (ko)
CA (1) CA2213119C (ko)
DE (1) DE69525974T2 (ko)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090287020A1 (en) * 2005-08-11 2009-11-19 Hiroshi Uchida Process for producing high-purity n-vinylcarboxamides
JP5357780B2 (ja) * 2007-12-27 2013-12-04 昭和電工株式会社 安定性及び重合性の改善されたｎ−メチル−ｎ−ビニルアセトアミドの製造方法
CN113227043B (zh) * 2018-12-27 2024-05-07 株式会社力森诺科 N-乙烯基羧酸酰胺制造用组合物
WO2021132366A1 (ja) * 2019-12-26 2021-07-01 昭和電工株式会社 高重合性ｎ－ビニルカルボン酸アミド単量体の製造方法
US20220220063A1 (en) * 2019-12-26 2022-07-14 Showa Denko K.K. Method for producing highly polymerizable n-vinyl carboxylic acid amide monomer
CN113874347A (zh) * 2019-12-26 2021-12-31 昭和电工株式会社 高聚合性n-乙烯基羧酸酰胺单体的制造方法
US20220220064A1 (en) * 2019-12-26 2022-07-14 Showa Denko K.K. Method for producing highly polymerizable n-vinyl carboxylic acid amide monomer
CN113939497A (zh) * 2019-12-26 2022-01-14 昭和电工株式会社 高聚合性n-乙烯基羧酸酰胺单体的制造方法
CN112047854B (zh) * 2020-10-20 2021-07-02 中国科学院长春应用化学研究所 一种n-乙烯基烷基酰胺的制备方法

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4018826A (en) * 1974-11-04 1977-04-19 Dynapol Corporation Process for preparing polyvinylamine and salts thereof
US4554377A (en) * 1984-07-16 1985-11-19 Celanese Corporation Production of N-vinyl carboxylic acid amides

Also Published As

Publication number Publication date
CA2213119C (en) 2007-03-06
AU4356596A (en) 1997-07-28
AU716698B2 (en) 2000-03-02
CA2213119A1 (en) 1997-07-10
KR19987002396A (en) 1998-07-15
KR100389242B1 (ko) 2003-09-26
ATE214690T1 (de) 2002-04-15
CN1082943C (zh) 2002-04-17
DE69525974D1 (de) 2002-04-25
CN1193959A (zh) 1998-09-23
DE69525974T2 (de) 2002-11-28

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