KR102822763B1 - 이산화티탄(TiO2) 나노결정의 합성, 캡핑 및 분산 - Google Patents
이산화티탄(TiO2) 나노결정의 합성, 캡핑 및 분산 Download PDFInfo
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- KR102822763B1 KR102822763B1 KR1020217018068A KR20217018068A KR102822763B1 KR 102822763 B1 KR102822763 B1 KR 102822763B1 KR 1020217018068 A KR1020217018068 A KR 1020217018068A KR 20217018068 A KR20217018068 A KR 20217018068A KR 102822763 B1 KR102822763 B1 KR 102822763B1
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- nanocrystals
- tio
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/08—Drying; Calcining ; After treatment of titanium oxide
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
- C30B7/10—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
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- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
- C08F20/02—Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
- C08F20/10—Esters
- C08F20/26—Esters containing oxygen in addition to the carboxy oxygen
- C08F20/32—Esters containing oxygen in addition to the carboxy oxygen containing epoxy radicals
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- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/18—Manufacture of films or sheets
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/10—Metal compounds
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L33/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- C08L33/04—Homopolymers or copolymers of esters
- C08L33/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, which oxygen atoms are present only as part of the carboxyl radical
- C08L33/062—Copolymers with monomers not covered by C08L33/06
- C08L33/068—Copolymers with monomers not covered by C08L33/06 containing glycidyl groups
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
- C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09D133/08—Homopolymers or copolymers of acrylic acid esters
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/16—Oxides
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- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
- C30B7/14—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions the crystallising materials being formed by chemical reactions in the solution
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- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
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- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/84—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by UV- or VIS- data
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- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/88—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by thermal analysis data, e.g. TGA, DTA, DSC
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- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
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- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
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- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
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- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2333/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
- C08J2333/04—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters
- C08J2333/06—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters of esters containing only carbon, hydrogen, and oxygen, the oxygen atom being present only as part of the carboxyl radical
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2333/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
- C08J2333/04—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters
- C08J2333/06—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters of esters containing only carbon, hydrogen, and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C08J2333/08—Homopolymers or copolymers of acrylic acid esters
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- C—CHEMISTRY; METALLURGY
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- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2433/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
- C08J2433/04—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters
- C08J2433/06—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters of esters containing only carbon, hydrogen, and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C08J2433/08—Homopolymers or copolymers of acrylic acid esters
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
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- C08L33/04—Homopolymers or copolymers of esters
- C08L33/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, which oxygen atoms are present only as part of the carboxyl radical
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- Inorganic Chemistry (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Wood Science & Technology (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Crystallography & Structural Chemistry (AREA)
- Metallurgy (AREA)
- General Chemical & Material Sciences (AREA)
- Polymerisation Methods In General (AREA)
- Graft Or Block Polymers (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020257019922A KR20250099257A (ko) | 2018-11-20 | 2019-11-20 | 이산화티탄 나노결정의 합성, 캡핑 및 분산 |
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201862769703P | 2018-11-20 | 2018-11-20 | |
| US62/769,703 | 2018-11-20 | ||
| US201962892625P | 2019-08-28 | 2019-08-28 | |
| US62/892,625 | 2019-08-28 | ||
| PCT/US2019/062439 WO2020106860A1 (en) | 2018-11-20 | 2019-11-20 | Synthesis, capping, and dispersion of tio2 nanocrystals |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020257019922A Division KR20250099257A (ko) | 2018-11-20 | 2019-11-20 | 이산화티탄 나노결정의 합성, 캡핑 및 분산 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20210080563A KR20210080563A (ko) | 2021-06-30 |
| KR102822763B1 true KR102822763B1 (ko) | 2025-06-20 |
Family
ID=70774045
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020217018068A Active KR102822763B1 (ko) | 2018-11-20 | 2019-11-20 | 이산화티탄(TiO2) 나노결정의 합성, 캡핑 및 분산 |
| KR1020257019922A Pending KR20250099257A (ko) | 2018-11-20 | 2019-11-20 | 이산화티탄 나노결정의 합성, 캡핑 및 분산 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020257019922A Pending KR20250099257A (ko) | 2018-11-20 | 2019-11-20 | 이산화티탄 나노결정의 합성, 캡핑 및 분산 |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US12215039B2 (https=) |
| EP (1) | EP3884085A4 (https=) |
| JP (2) | JP2022507818A (https=) |
| KR (2) | KR102822763B1 (https=) |
| CN (1) | CN113227463A (https=) |
| WO (1) | WO2020106860A1 (https=) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP7605421B2 (ja) * | 2020-12-07 | 2024-12-24 | 株式会社ダイセル | チタン含有複合材料 |
| US20220204790A1 (en) * | 2020-12-31 | 2022-06-30 | Facebook Technologies, Llc | High refractive index overcoat formulation and method of use with inkjet printing |
| CN116981699A (zh) | 2021-02-24 | 2023-10-31 | 东京应化工业株式会社 | 光固性液态组合物、固化物、及固化物的制造方法 |
| EP4314146A4 (en) * | 2021-03-26 | 2025-07-09 | Pt Spe Subco Llc | ZIRCONIA AND TITANIUM DIOXIDE FORMULATIONS AND NANOCOMPOSITES FOR NANOIMPRINT LITHOGRAPHY |
| JP7691272B2 (ja) * | 2021-04-16 | 2025-06-11 | 東京応化工業株式会社 | 金属含有シリルオキシ化合物、金属含有シリルオキシ基被覆粒子、その製造方法、及び分散組成物 |
| JP2025505955A (ja) | 2022-01-25 | 2025-03-05 | アディソン クリアー ウェーブ コーティングス インコーポレーテッド | 高屈折率ナノインプリントリソグラフィー樹脂 |
| CN114524676B (zh) * | 2022-02-25 | 2023-09-01 | 广东工业大学 | 一种光固化氮化硅陶瓷浆料、氮化硅陶瓷的制备方法 |
| KR102847115B1 (ko) * | 2022-03-24 | 2025-08-18 | 한국화학연구원 | 고분자 고체전해질용 조성물, 고분자 고체전해질 및 이를 포함하는 이차전지 |
| CN115491119B (zh) * | 2022-11-22 | 2023-04-07 | 宁波惠之星新材料科技股份有限公司 | 一种防眩液、防眩膜及其制备方法、偏光片 |
| CN117363099B (zh) * | 2023-08-29 | 2025-10-28 | 西安思摩威新材料有限公司 | 一种高折射率前驱液、制备方法及其应用 |
| CN117511309A (zh) * | 2023-11-27 | 2024-02-06 | 几何智慧(常州)光伏电站运维管理有限公司 | 应用于光伏板的水性涂料的制备工艺 |
| WO2025121222A1 (ja) * | 2023-12-07 | 2025-06-12 | ナガセケムテックス株式会社 | 無機微粒子分散液 |
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| US20120088845A1 (en) * | 2010-04-23 | 2012-04-12 | Gonen Williams Zehra Serpil | Synthesis, capping and dispersion of nanocrystals |
| US20180223107A1 (en) * | 2015-07-31 | 2018-08-09 | Pixelligent Technologies Llc | Nanocomposite formulations for optical applications |
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| WO2008118422A1 (en) * | 2007-03-26 | 2008-10-02 | The Trustees Of Columbia University In The City Of New York | Metal oxide nanocrystals: preparation and uses |
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| EP3190083B1 (en) | 2010-10-27 | 2020-08-26 | Pixelligent Technologies, LLC | Synthesis, capping and dispersion of nanocrystals |
| TWI458685B (zh) | 2011-06-29 | 2014-11-01 | Univ Nat Chiao Tung | 二氧化鈦奈米粉體及其製造方法 |
| CN103387261B (zh) | 2012-05-07 | 2015-07-15 | 华中科技大学 | 一种锐钛矿型二氧化钛纳米棒及其制备方法 |
| KR102015569B1 (ko) | 2013-01-31 | 2019-08-28 | 서울대학교산학협력단 | 이차원 구조의 산화티타늄 나노입자 제조 방법 |
| US10273365B2 (en) * | 2013-03-15 | 2019-04-30 | Pixelligent Technologies Llc | High refractive index nanocomposite |
| JP6011749B1 (ja) * | 2015-02-27 | 2016-10-19 | 堺化学工業株式会社 | 酸化チタン粒子の有機溶媒分散体とその製造方法 |
| US9963355B2 (en) * | 2015-02-27 | 2018-05-08 | Sakai Chemical Industry Co., Ltd. | Method for producing organic solvent dispersion of titanium oxide particles |
| EP3277741A4 (en) | 2015-03-30 | 2018-11-14 | Pixelligent Technologies, LLC | High refractive index solvent free silicone nanocomposites |
| CN106241865B (zh) * | 2016-08-23 | 2017-10-10 | 中国科学院广州地球化学研究所 | 一种高(001)面锐钛矿型二氧化钛纳米晶的制备方法 |
| DE102016125432A1 (de) * | 2016-12-22 | 2018-06-28 | Leibniz-Institut Für Neue Materialien Gemeinnützige Gmbh | Herstellung von dotierten Nanopartikeln und ihre Verwendung |
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2019
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- 2019-11-20 CN CN201980086349.2A patent/CN113227463A/zh active Pending
- 2019-11-20 KR KR1020257019922A patent/KR20250099257A/ko active Pending
- 2019-11-20 JP JP2021527924A patent/JP2022507818A/ja active Pending
- 2019-11-20 US US17/294,261 patent/US12215039B2/en active Active
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20120088845A1 (en) * | 2010-04-23 | 2012-04-12 | Gonen Williams Zehra Serpil | Synthesis, capping and dispersion of nanocrystals |
| US20180223107A1 (en) * | 2015-07-31 | 2018-08-09 | Pixelligent Technologies Llc | Nanocomposite formulations for optical applications |
Also Published As
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| EP3884085A1 (en) | 2021-09-29 |
| US20250154020A1 (en) | 2025-05-15 |
| EP3884085A4 (en) | 2022-09-07 |
| WO2020106860A1 (en) | 2020-05-28 |
| KR20210080563A (ko) | 2021-06-30 |
| CN113227463A (zh) | 2021-08-06 |
| JP2022507818A (ja) | 2022-01-18 |
| US20220017381A1 (en) | 2022-01-20 |
| JP2025062602A (ja) | 2025-04-14 |
| KR20250099257A (ko) | 2025-07-01 |
| US12215039B2 (en) | 2025-02-04 |
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