KR102727963B1 - 기포탑 반응기 기반 분해기 및 그 사용 방법 - Google Patents

기포탑 반응기 기반 분해기 및 그 사용 방법 Download PDF

Info

Publication number
KR102727963B1
KR102727963B1 KR1020177029210A KR20177029210A KR102727963B1 KR 102727963 B1 KR102727963 B1 KR 102727963B1 KR 1020177029210 A KR1020177029210 A KR 1020177029210A KR 20177029210 A KR20177029210 A KR 20177029210A KR 102727963 B1 KR102727963 B1 KR 102727963B1
Authority
KR
South Korea
Prior art keywords
slurry
zone
decomposition
oxidation
bcr
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
KR1020177029210A
Other languages
English (en)
Korean (ko)
Other versions
KR20170128462A (ko
Inventor
앨런 지 원더스
Original Assignee
알펙 폴리에스테르, 에스.에이. 데 씨.브이.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 알펙 폴리에스테르, 에스.에이. 데 씨.브이. filed Critical 알펙 폴리에스테르, 에스.에이. 데 씨.브이.
Publication of KR20170128462A publication Critical patent/KR20170128462A/ko
Application granted granted Critical
Publication of KR102727963B1 publication Critical patent/KR102727963B1/ko
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/002Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2415Tubular reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2415Tubular reactors
    • B01J19/242Tubular reactors in series
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/487Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C63/00Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
    • C07C63/14Monocyclic dicarboxylic acids
    • C07C63/15Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
    • C07C63/261,4 - Benzenedicarboxylic acid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00777Baffles attached to the reactor wall horizontal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020177029210A 2015-03-13 2016-03-11 기포탑 반응기 기반 분해기 및 그 사용 방법 Active KR102727963B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US14/657,523 US20160264511A1 (en) 2015-03-13 2015-03-13 Bubble column reactor based digester and method for its use
US14/657,523 2015-03-13
PCT/US2016/021912 WO2016149060A1 (en) 2015-03-13 2016-03-11 Bubble column reactor based digester andmethod for its use

Publications (2)

Publication Number Publication Date
KR20170128462A KR20170128462A (ko) 2017-11-22
KR102727963B1 true KR102727963B1 (ko) 2024-11-07

Family

ID=56887404

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020177029210A Active KR102727963B1 (ko) 2015-03-13 2016-03-11 기포탑 반응기 기반 분해기 및 그 사용 방법

Country Status (16)

Country Link
US (1) US20160264511A1 (enExample)
EP (1) EP3268341B1 (enExample)
JP (1) JP6882182B2 (enExample)
KR (1) KR102727963B1 (enExample)
CN (1) CN107531602B (enExample)
BR (1) BR112017019452B1 (enExample)
CA (1) CA2979681A1 (enExample)
EA (1) EA034735B1 (enExample)
ES (1) ES2880688T3 (enExample)
LT (1) LT3268341T (enExample)
MX (1) MX2017011729A (enExample)
MY (1) MY188141A (enExample)
PL (1) PL3268341T3 (enExample)
PT (1) PT3268341T (enExample)
SG (2) SG10201908521RA (enExample)
WO (1) WO2016149060A1 (enExample)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11203769B1 (en) * 2017-02-13 2021-12-21 Solugen, Inc. Hydrogen peroxide and gluconic acid production
US10000435B1 (en) * 2017-02-28 2018-06-19 Grupo Petrotemex, S.A. De C.V. Energy and environmentally integrated method for production of aromatic dicarboxylic acids by oxidation
CN119056494B (zh) * 2023-05-31 2025-11-14 中国石油化工股份有限公司 一种加氢催化剂及其制备方法和应用

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070293699A1 (en) 2004-09-02 2007-12-20 Eastman Chemical Company Optimized Liquid-Phase Oxidation

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5200557A (en) * 1991-04-12 1993-04-06 Amoco Corporation Process for preparation of crude terephthalic acid suitable for reduction to prepare purified terephthalic acid
DE19843573A1 (de) * 1998-09-23 2000-03-30 Degussa Blasensäule und deren Verwendung
US7196215B2 (en) * 2001-06-04 2007-03-27 Eastman Chemical Company Process for the production of purified terephthalic acid
US7608732B2 (en) * 2005-03-08 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7355068B2 (en) * 2006-01-04 2008-04-08 Eastman Chemical Company Oxidation system with internal secondary reactor
US7816556B2 (en) * 2006-03-01 2010-10-19 Eastman Chemical Company Polycarboxylic acid production system employing enhanced multistage oxidative digestion
US7326808B2 (en) * 2006-03-01 2008-02-05 Eastman Chemical Company Polycarboxylic acid production system employing cooled mother liquor from oxidative digestion as feed to impurity purge system
US7393973B2 (en) * 2006-03-01 2008-07-01 Eastman Chemical Company Polycarboxylic acid production system with enhanced residence time distribution for oxidative digestion
CN101531588B (zh) * 2008-03-13 2016-02-24 周向进 一种新的精对苯二甲酸的制造方法
CN202700501U (zh) 2012-05-15 2013-01-30 中国昆仑工程公司 适于kpta生产的无搅拌氧化和深度氧化反应系统
CN102731297B (zh) * 2012-07-11 2014-06-04 浙江大学 一种逐级升温氧化制备中纯度对苯二甲酸的方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070293699A1 (en) 2004-09-02 2007-12-20 Eastman Chemical Company Optimized Liquid-Phase Oxidation

Also Published As

Publication number Publication date
CN107531602A (zh) 2018-01-02
JP2018513125A (ja) 2018-05-24
BR112017019452B1 (pt) 2020-11-17
EP3268341A1 (en) 2018-01-17
CN107531602B (zh) 2021-02-12
EA201792031A1 (ru) 2018-02-28
EP3268341A4 (en) 2018-10-31
US20160264511A1 (en) 2016-09-15
WO2016149060A1 (en) 2016-09-22
BR112017019452A2 (pt) 2018-05-15
SG11201707399XA (en) 2017-10-30
JP6882182B2 (ja) 2021-06-02
LT3268341T (lt) 2021-07-26
EP3268341B1 (en) 2021-04-21
MY188141A (en) 2021-11-23
PL3268341T3 (pl) 2021-11-02
ES2880688T3 (es) 2021-11-25
SG10201908521RA (en) 2019-11-28
KR20170128462A (ko) 2017-11-22
CA2979681A1 (en) 2016-09-22
PT3268341T (pt) 2021-06-30
EA034735B1 (ru) 2020-03-13
MX2017011729A (es) 2017-11-13

Similar Documents

Publication Publication Date Title
KR101281378B1 (ko) 최적화된 액상 산화 방법
KR20080103984A (ko) 퍼지 시스템으로의 공급물로서 산화적 분해로부터의 냉각된모액을 사용하는 폴리카복실산 제조 시스템
KR102727963B1 (ko) 기포탑 반응기 기반 분해기 및 그 사용 방법
CA2787899C (en) Oxidation system with sidedraw secondary reactor
JP6329117B2 (ja) 側方取り出し式の第2の反応器を備える酸化システム
JP2018513125A5 (enExample)
JP6538528B2 (ja) 側方取り出し式の第2の反応器を備える酸化システム
KR20070054696A (ko) 최적화된 액상 산화 방법

Legal Events

Date Code Title Description
PA0105 International application

Patent event date: 20171012

Patent event code: PA01051R01D

Comment text: International Patent Application

PG1501 Laying open of application
A201 Request for examination
PA0201 Request for examination

Patent event code: PA02012R01D

Patent event date: 20210309

Comment text: Request for Examination of Application

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

Comment text: Notification of reason for refusal

Patent event date: 20221230

Patent event code: PE09021S01D

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

Comment text: Notification of reason for refusal

Patent event date: 20230730

Patent event code: PE09021S01D

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

Patent event code: PE07011S01D

Comment text: Decision to Grant Registration

Patent event date: 20240829

GRNT Written decision to grant
PR0701 Registration of establishment

Comment text: Registration of Establishment

Patent event date: 20241105

Patent event code: PR07011E01D

PR1002 Payment of registration fee

Payment date: 20241105

End annual number: 3

Start annual number: 1

PG1601 Publication of registration