KR102727963B1 - 기포탑 반응기 기반 분해기 및 그 사용 방법 - Google Patents
기포탑 반응기 기반 분해기 및 그 사용 방법 Download PDFInfo
- Publication number
- KR102727963B1 KR102727963B1 KR1020177029210A KR20177029210A KR102727963B1 KR 102727963 B1 KR102727963 B1 KR 102727963B1 KR 1020177029210 A KR1020177029210 A KR 1020177029210A KR 20177029210 A KR20177029210 A KR 20177029210A KR 102727963 B1 KR102727963 B1 KR 102727963B1
- Authority
- KR
- South Korea
- Prior art keywords
- slurry
- zone
- decomposition
- oxidation
- bcr
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
- B01J10/002—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/006—Baffles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2415—Tubular reactors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2415—Tubular reactors
- B01J19/242—Tubular reactors in series
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
- C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
- C07C63/14—Monocyclic dicarboxylic acids
- C07C63/15—Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
- C07C63/26—1,4 - Benzenedicarboxylic acid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00761—Details of the reactor
- B01J2219/00763—Baffles
- B01J2219/00765—Baffles attached to the reactor wall
- B01J2219/00777—Baffles attached to the reactor wall horizontal
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14/657,523 US20160264511A1 (en) | 2015-03-13 | 2015-03-13 | Bubble column reactor based digester and method for its use |
| US14/657,523 | 2015-03-13 | ||
| PCT/US2016/021912 WO2016149060A1 (en) | 2015-03-13 | 2016-03-11 | Bubble column reactor based digester andmethod for its use |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20170128462A KR20170128462A (ko) | 2017-11-22 |
| KR102727963B1 true KR102727963B1 (ko) | 2024-11-07 |
Family
ID=56887404
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020177029210A Active KR102727963B1 (ko) | 2015-03-13 | 2016-03-11 | 기포탑 반응기 기반 분해기 및 그 사용 방법 |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US20160264511A1 (enExample) |
| EP (1) | EP3268341B1 (enExample) |
| JP (1) | JP6882182B2 (enExample) |
| KR (1) | KR102727963B1 (enExample) |
| CN (1) | CN107531602B (enExample) |
| BR (1) | BR112017019452B1 (enExample) |
| CA (1) | CA2979681A1 (enExample) |
| EA (1) | EA034735B1 (enExample) |
| ES (1) | ES2880688T3 (enExample) |
| LT (1) | LT3268341T (enExample) |
| MX (1) | MX2017011729A (enExample) |
| MY (1) | MY188141A (enExample) |
| PL (1) | PL3268341T3 (enExample) |
| PT (1) | PT3268341T (enExample) |
| SG (2) | SG10201908521RA (enExample) |
| WO (1) | WO2016149060A1 (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11203769B1 (en) * | 2017-02-13 | 2021-12-21 | Solugen, Inc. | Hydrogen peroxide and gluconic acid production |
| US10000435B1 (en) * | 2017-02-28 | 2018-06-19 | Grupo Petrotemex, S.A. De C.V. | Energy and environmentally integrated method for production of aromatic dicarboxylic acids by oxidation |
| CN119056494B (zh) * | 2023-05-31 | 2025-11-14 | 中国石油化工股份有限公司 | 一种加氢催化剂及其制备方法和应用 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070293699A1 (en) | 2004-09-02 | 2007-12-20 | Eastman Chemical Company | Optimized Liquid-Phase Oxidation |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5200557A (en) * | 1991-04-12 | 1993-04-06 | Amoco Corporation | Process for preparation of crude terephthalic acid suitable for reduction to prepare purified terephthalic acid |
| DE19843573A1 (de) * | 1998-09-23 | 2000-03-30 | Degussa | Blasensäule und deren Verwendung |
| US7196215B2 (en) * | 2001-06-04 | 2007-03-27 | Eastman Chemical Company | Process for the production of purified terephthalic acid |
| US7608732B2 (en) * | 2005-03-08 | 2009-10-27 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7355068B2 (en) * | 2006-01-04 | 2008-04-08 | Eastman Chemical Company | Oxidation system with internal secondary reactor |
| US7816556B2 (en) * | 2006-03-01 | 2010-10-19 | Eastman Chemical Company | Polycarboxylic acid production system employing enhanced multistage oxidative digestion |
| US7326808B2 (en) * | 2006-03-01 | 2008-02-05 | Eastman Chemical Company | Polycarboxylic acid production system employing cooled mother liquor from oxidative digestion as feed to impurity purge system |
| US7393973B2 (en) * | 2006-03-01 | 2008-07-01 | Eastman Chemical Company | Polycarboxylic acid production system with enhanced residence time distribution for oxidative digestion |
| CN101531588B (zh) * | 2008-03-13 | 2016-02-24 | 周向进 | 一种新的精对苯二甲酸的制造方法 |
| CN202700501U (zh) | 2012-05-15 | 2013-01-30 | 中国昆仑工程公司 | 适于kpta生产的无搅拌氧化和深度氧化反应系统 |
| CN102731297B (zh) * | 2012-07-11 | 2014-06-04 | 浙江大学 | 一种逐级升温氧化制备中纯度对苯二甲酸的方法 |
-
2015
- 2015-03-13 US US14/657,523 patent/US20160264511A1/en not_active Abandoned
-
2016
- 2016-03-11 CA CA2979681A patent/CA2979681A1/en active Pending
- 2016-03-11 SG SG10201908521R patent/SG10201908521RA/en unknown
- 2016-03-11 EP EP16765474.8A patent/EP3268341B1/en active Active
- 2016-03-11 JP JP2017548128A patent/JP6882182B2/ja active Active
- 2016-03-11 BR BR112017019452-0A patent/BR112017019452B1/pt active IP Right Grant
- 2016-03-11 MX MX2017011729A patent/MX2017011729A/es unknown
- 2016-03-11 LT LTEP16765474.8T patent/LT3268341T/lt unknown
- 2016-03-11 PT PT167654748T patent/PT3268341T/pt unknown
- 2016-03-11 PL PL16765474T patent/PL3268341T3/pl unknown
- 2016-03-11 CN CN201680027722.3A patent/CN107531602B/zh active Active
- 2016-03-11 KR KR1020177029210A patent/KR102727963B1/ko active Active
- 2016-03-11 EA EA201792031A patent/EA034735B1/ru not_active IP Right Cessation
- 2016-03-11 WO PCT/US2016/021912 patent/WO2016149060A1/en not_active Ceased
- 2016-03-11 ES ES16765474T patent/ES2880688T3/es active Active
- 2016-03-11 MY MYPI2017001308A patent/MY188141A/en unknown
- 2016-03-11 SG SG11201707399XA patent/SG11201707399XA/en unknown
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070293699A1 (en) | 2004-09-02 | 2007-12-20 | Eastman Chemical Company | Optimized Liquid-Phase Oxidation |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107531602A (zh) | 2018-01-02 |
| JP2018513125A (ja) | 2018-05-24 |
| BR112017019452B1 (pt) | 2020-11-17 |
| EP3268341A1 (en) | 2018-01-17 |
| CN107531602B (zh) | 2021-02-12 |
| EA201792031A1 (ru) | 2018-02-28 |
| EP3268341A4 (en) | 2018-10-31 |
| US20160264511A1 (en) | 2016-09-15 |
| WO2016149060A1 (en) | 2016-09-22 |
| BR112017019452A2 (pt) | 2018-05-15 |
| SG11201707399XA (en) | 2017-10-30 |
| JP6882182B2 (ja) | 2021-06-02 |
| LT3268341T (lt) | 2021-07-26 |
| EP3268341B1 (en) | 2021-04-21 |
| MY188141A (en) | 2021-11-23 |
| PL3268341T3 (pl) | 2021-11-02 |
| ES2880688T3 (es) | 2021-11-25 |
| SG10201908521RA (en) | 2019-11-28 |
| KR20170128462A (ko) | 2017-11-22 |
| CA2979681A1 (en) | 2016-09-22 |
| PT3268341T (pt) | 2021-06-30 |
| EA034735B1 (ru) | 2020-03-13 |
| MX2017011729A (es) | 2017-11-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0105 | International application |
Patent event date: 20171012 Patent event code: PA01051R01D Comment text: International Patent Application |
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| PG1501 | Laying open of application | ||
| A201 | Request for examination | ||
| PA0201 | Request for examination |
Patent event code: PA02012R01D Patent event date: 20210309 Comment text: Request for Examination of Application |
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| E902 | Notification of reason for refusal | ||
| PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 20221230 Patent event code: PE09021S01D |
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| E902 | Notification of reason for refusal | ||
| PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 20230730 Patent event code: PE09021S01D |
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| E701 | Decision to grant or registration of patent right | ||
| PE0701 | Decision of registration |
Patent event code: PE07011S01D Comment text: Decision to Grant Registration Patent event date: 20240829 |
|
| GRNT | Written decision to grant | ||
| PR0701 | Registration of establishment |
Comment text: Registration of Establishment Patent event date: 20241105 Patent event code: PR07011E01D |
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| PR1002 | Payment of registration fee |
Payment date: 20241105 End annual number: 3 Start annual number: 1 |
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| PG1601 | Publication of registration |