KR102648658B1 - Body wash using egg yolk oil with anti-aging effect - Google Patents

Abstract

The present invention provides a body wash composition containing egg yolk oil.

Description

Body wash using egg yolk oil with anti-aging effect}

The present invention relates to a body wash using egg yolk oil, which has an anti-aging effect.

The skin is the organ in our human body that is most closely in contact with the external environment, and is a very important organ that has biochemical and physical functions to protect the inside of the human body. When active oxygen is generated in the skin, the oxygen attacks the cell membrane, destroying the cells and further causing skin aging, including the formation of wrinkles. Therefore, it always keeps the skin moist and promotes blood circulation to protect the cell membrane by scavenging free radicals generated in the body. Furthermore, by activating sweating, all toxins and waste accumulated in the body's cells are discharged, thereby improving the skin's health. In addition to delaying aging, it is necessary to proliferate cells by reactivating already damaged cells through active metabolism.

Personal care composition products such as body wash are becoming increasingly popular in the United States and globally. A desirable body wash composition must meet a number of criteria. For example, to be satisfactory to consumers, body wash compositions must exhibit good cleansing properties, exhibit good lathering characteristics, be hypoallergenic to the skin, and preferably even provide a conditioning effect to the skin.

Body wash compositions intended to provide a skin conditioning effect are known. Many of these compositions are aqueous systems containing emulsified conditioning oils or other similar substances in combination with foaming surfactants. Although these products provide both conditioning and cleansing benefits, it is often difficult to formulate a product that deposits a sufficient amount of skin conditioning agent onto the skin during use. To combat emulsification of the skin conditioning agent by the cleansing surfactant, a large amount of skin conditioning agent is added to the composition. However, this creates other problems associated with these cleaning and conditioning products. Increasing the level of skin conditioning agents to increase deposition has a negative impact on the foam performance and stability of the product. Therefore, the foam life is increased and the foaming characteristics provide improved cleansing and effects on the skin, such as silky skin feel, improved soft skin feel and improved smooth skin feel, as well as a stable, hypoallergenic and anti-aging effect. There still remains a need for body wash compositions that represent.

Patent Document 1: Republic of Korea Patent No. 10-1496624

The present invention was devised to solve the above problems, and the purpose of the present invention is to provide a body wash composition having an anti-aging effect.

The object of the present invention is not limited to the problems mentioned above, and other problems not mentioned will be clearly understood by those skilled in the art from the description below.

In order to achieve the above object, the present invention

A body wash composition containing egg yolk oil is provided.

In addition, the body wash composition includes 0.1-0.3 parts by weight of egg yolk oil, 3-7 parts by weight of a complex extract of Cranium chinensis extract, Corolla extract, and Prickly pear extract mixed in a weight ratio of 1:1:1, and sodium C14-16 olefin sulfonate. 4-5 parts by weight, disodium cocoamphodiacetate 3-5 parts by weight, sodium chloride 2-4 parts by weight, decyl glucoside 2-4 parts by weight, glycerin 0.9-1.1 parts by weight, acrylate copolymer 0.09-0.11 parts by weight , citric acid 0.09-0.11 parts by weight, hexylene glycol 0.09-0.11 parts by weight, C12-13 Alkes-9 0.09-0.11 parts by weight, coco-betaine 0.09-0.11 parts by weight, tetradecene 0.09-0.11 parts by weight. parts, 0.4-0.6 parts by weight of hydroxyacetophenone, 0.09-0.11 parts by weight of hexadecene, 0.4-0.6 parts by weight of styrene/acrylate copolymer, 0.2-0.4 parts by weight of dipropylene glycol, 0.1-0.3 parts by weight of ethylhexylglycerin. parts by weight, 1,2-hexanediol 0.1-0.3 parts by weight, disodium EDTA 0.04-0.06 parts by weight, sodium citrate 0.00009-0.00011 parts by weight, tocopherol 0.00009-0.00011 parts by weight, lemon peel oil 0.09-0.11 parts by weight parts, secretion tree oil 0.09-0.11 parts by weight, lime starch oil 0.09-0.11 parts by weight, citronella oil 0.09-0.11 parts by weight, limonene 0.3-0.5 parts by weight, geraniol 0.3-0.5 parts by weight, citronellol 0.3 -0.5 parts by weight and 80.2497-80.2499 parts by weight of purified water.

In addition, the present invention

Washing the Chinese herbaceous leaves, Chinese apricots and prickly prickly pear and drying them at a temperature of 48-52°C for 2-4 hours; Preparing a mixed powder by grinding dried Chinese herbaceous leaves, Chinese apricots, and Chinese prickly pear and mixing them at a weight ratio of 1:1:1; Mixing 8-12 parts by weight of the mixed powder and 88-92 parts by weight of purified water and performing primary hot water extraction at a temperature of 118-122°C for 5-7 hours; After primary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a primary extract; After the first hot water extraction and filtering with filter paper, 8-12 parts by weight of the remaining solids and 88-92 parts by weight of purified water were mixed, and 0.8-1.2 parts by weight of tocopherol and [BMIM][BF ₄ ](1-butyl-3- Adding 0.8-1.2 parts by weight of methylimidazolium tetrafluoroborate) and performing secondary hot water extraction at a temperature of 88-92°C for 10-14 hours while stirring; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a secondary extract; and mixing the primary extract and the secondary extract; preparing a composite extract comprising; and

Egg yolk oil 0.1-0.3 parts by weight, 3-7 parts by weight of the above complex extract, 4-5 parts by weight of sodium C14-16 olefin sulfonate, 3-5 parts by weight of disodium cocoamphodiacetate, 2-4 parts by weight of sodium chloride, decyl Glucoside 2-4 parts by weight, glycerin 0.9-1.1 parts by weight, acrylate copolymer 0.09-0.11 parts by weight, citric acid 0.09-0.11 parts by weight, hexylene glycol 0.09-0.11 parts by weight, C12-13 Alkes- 9 0.09-0.11 parts by weight, coco-betaine 0.09-0.11 parts by weight, tetradecene 0.09-0.11 parts by weight, hydroxyacetophenone 0.4-0.6 parts by weight, hexadecene 0.09-0.11 parts by weight, styrene/acrylate copolymer 0.4-0.6 parts by weight, dipropylene glycol 0.2-0.4 parts by weight, ethylhexylglycerin 0.1-0.3 parts by weight, 1,2-hexanediol 0.1-0.3 parts by weight, disodium EDTA 0.04-0.06 parts by weight, Sodium citrate 0.00009-0.00011 parts by weight, tocopherol 0.00009-0.00011 parts by weight, lemon peel oil 0.09-0.11 parts by weight, secretion tree oil 0.09-0.11 parts by weight, lime whole plant oil 0.09-0.11 parts by weight, citronella oil 0.09-0.11 parts by weight, mixing 0.3-0.5 parts by weight of limonene, 0.3-0.5 parts by weight of geraniol, 0.3-0.5 parts by weight of citronellol, and 80.2497-80.2499 parts by weight of purified water; providing a method for producing a body wash composition comprising: .

The body wash composition according to the present invention has an anti-aging effect by having antioxidant and anti-inflammatory functions. In addition, it has excellent skin moisturizing power and low irritation.

Hereinafter, various embodiments will be described in more detail. The embodiments described herein may be modified in various ways. Specific embodiments may be described in detail in the detailed description. However, the specific embodiments disclosed are only intended to facilitate understanding of the various embodiments. Accordingly, the technical idea is not limited to the specific embodiments disclosed, and should be understood to include all equivalents or substitutes included in the spirit and technical scope of the invention.

Terms containing ordinal numbers, such as primary, secondary, first, second, etc., may be used to describe various components, but these components are not limited by the above-mentioned terms. The above-mentioned terms are used only for the purpose of distinguishing one component from another.

In this specification, terms such as 'include' or 'have' are intended to designate the presence of features, numbers, steps, operations, components, parts, or combinations thereof described in the specification, but are not intended to indicate the presence of one or more other features. It should be understood that this does not exclude in advance the possibility of the existence or addition of elements, numbers, steps, operations, components, parts, or combinations thereof. When a component is said to be 'connected' or 'connected' to another component, it is understood that it may be directly connected or connected to the other component, but that other components may exist in between. It should be. On the other hand, when a component is mentioned as being 'directly connected' or 'directly connected' to another component, it should be understood that there are no other components in between.

In addition, when describing the present invention, if it is determined that a detailed description of a related known function or configuration may unnecessarily obscure the gist of the present invention, the detailed description thereof is abbreviated or omitted.

This invention

A body wash composition containing egg yolk oil is provided.

Hereinafter, the body wash composition according to the present invention will be described in detail.

The body wash composition includes 0.1-0.3 parts by weight of egg yolk oil, 3-7 parts by weight of a composite extract of 0.1-0.3 parts by weight of E. chinensis extract, Corolla extract, and Prickly pear extract mixed in a weight ratio of 1:1:1, and 4-4% sodium C14-16 olefin sulfonate. 5 parts by weight, disodium cocoamphodiacetate 3-5 parts by weight, sodium chloride 2-4 parts by weight, decyl glucoside 2-4 parts by weight, glycerin 0.9-1.1 parts by weight, acrylate copolymer 0.09-0.11 parts by weight, sheet Rick acid 0.09-0.11 parts by weight, hexylene glycol 0.09-0.11 parts by weight, C12-13alces-9 0.09-0.11 parts by weight, coco-betaine 0.09-0.11 parts by weight, tetradecene 0.09-0.11 parts by weight, Hydroxyacetophenone 0.4-0.6 parts by weight, hexadecene 0.09-0.11 parts by weight, styrene/acrylate copolymer 0.4-0.6 parts by weight, dipropylene glycol 0.2-0.4 parts by weight, ethylhexylglycerin 0.1-0.3 parts by weight , 1,2-hexanediol 0.1-0.3 parts by weight, disodium EDTA 0.04-0.06 parts by weight, sodium citrate 0.00009-0.00011 parts by weight, tocopherol 0.00009-0.00011 parts by weight, lemon peel oil 0.09-0.11 parts by weight, Secretion tree oil 0.09-0.11 parts by weight, lime starch oil 0.09-0.11 parts by weight, citronella oil 0.09-0.11 parts by weight, limonene 0.3-0.5 parts by weight, geraniol 0.3-0.5 parts by weight, citronellol 0.3-0.5 A body wash composition comprising 80.2497-80.2499 parts by weight of purified water.

The body wash composition includes 0.1-0.3 parts by weight of egg yolk oil, 4-5 parts by weight of sodium C14-16 olefin sulfonate, 3-5 parts by weight of disodium cocoamphodiacetate, 2-4 parts by weight of sodium chloride, and 2-4 parts by weight of decyl glucoside. Parts by weight, glycerin 0.9-1.1 parts by weight, acrylate copolymer 0.09-0.11 parts by weight, citric acid 0.09-0.11 parts by weight, hexylene glycol 0.09-0.11 parts by weight, C12-13Alces-9 0.09-0.11 parts by weight, coco-betaine 0.09-0.11 parts by weight, tetradecene 0.09-0.11 parts by weight, hydroxyacetophenone 0.4-0.6 parts by weight, hexadecene 0.09-0.11 parts by weight, styrene/acrylate copolymer 0.4-0.6 parts by weight parts, dipropylene glycol 0.2-0.4 parts by weight, ethylhexylglycerin 0.1-0.3 parts by weight, 1,2-hexanediol 0.1-0.3 parts by weight, disodium EDTA 0.04-0.06 parts by weight, sodium citrate 0.00009 -0.00011 parts by weight, tocopherol 0.00009-0.00011 parts by weight, lemon peel oil 0.09-0.11 parts by weight, secretion tree oil 0.09-0.11 parts by weight, lime whole plant oil 0.09-0.11 parts by weight, citronella oil 0.09-0.11 parts by weight, limonene It is preferable to include 0.3-0.5 parts by weight, 0.3-0.5 parts by weight of geraniol, 0.3-0.5 parts by weight of citronellol, and 80.2497-80.2499 parts by weight of purified water.

Egg yolk oil is an oily extract extracted from the egg yolk (yolk) of bird eggs, and is called egg yolk oil, egg oil, egg oil, etc. Egg yolk oil is known to contain lipids, vitamin A, vitamin E, and linoleic acid, and lipids are known to be composed of neutral lipids, phospholipids, and sterols. In the present invention, the egg yolk oil is applied to a body wash composition. Accordingly, the anti-aging effect is excellent.

The above sodium C14-16 olefin sulfonate, disodium cocoamphodiacetate, sodium chloride and decyl glucoside are used as surfactants, with 4-5 parts by weight of sodium C14-16 olefin sulfonate and 3-5 parts by weight of disodium cocoamphodiacetate. Part by weight, 2-4 parts by weight of sodium chloride and 2-4 parts by weight of decyl glucoside are mixed and applied. Accordingly, the body wash composition has excellent cleaning power and is hypoallergenic.

The glycerin improves moisturizing power.

The acrylate copolymer, C12-13 Alkes-9, coco-betaine, and styrene/acrylate copolymer can be general ingredients applied to cosmetics.

The lemon peel oil is an essential oil extracted from the bright yellow peel of a lemon by cold pressing, and has antioxidant, anti-inflammatory, and skin moisturizing properties.

The secretion tree oil is also called Siberian fir oil, and is known to have a fresh aroma, help relieve muscle pain, and have antioxidant, anti-inflammatory, and skin moisturizing properties.

The lime whole plant oil is an essential oil extracted from lime whole plant by cold pressing, and has antioxidant, anti-inflammatory, and skin moisturizing functions.

The citronella oil is known to have a mind-purifying and uplifting effect, relieve depression, and have a nerve stabilizing effect, and has antioxidant, anti-inflammatory, and skin moisturizing properties.

The limonene has antioxidant and anti-inflammatory properties as well as whitening properties.

The geraniol has excellent antibacterial and anti-inflammatory properties.

The citronellol is an alcohol obtained by extracting and purifying the chamomile plant. It has skin-healing ingredients, antibacterial and anti-inflammatory ingredients, and is effective in relieving skin irritation and moisturizing the skin.

In addition, the body wash composition preferably contains 3-7 parts by weight, and more preferably 4-6 parts by weight, of a composite extract in which the E. chinensis extract, Corolla extract, and Prickly prickly pear extract are mixed in a weight ratio of 1:1:1. desirable.

Geranium thunbergii Sieb. and Zucc is a perennial herb belonging to the order Geraniales, Geranium LINNE, and Geraniaceae. Approximately 250 species of plants in the Arboraceae family are distributed in temperate and tropical alpine regions, and approximately 16 species are distributed in Korea. This herbal medicine is called Hyeoncho (玄草) or Hyangyangcho (玄之草) in Oriental medicine, and refers to the whole plant harvested in the fall, trimmed, and dried. Dysentery exhibits the properties of cold, sour, and cold. It has dehumidifying and anti-diarrheal effects; it removes wind and dampness and strengthens the skeleton and muscles by communicating meridians, so it is used for quadriplegic pain, joint discomfort, bruises, etc., as well as dysentery and chronic diarrhea and abdominal pain. , it is known to be effective for enteritis.

It belongs to the green algae family, and is 10 to 50 cm long and has green, thin leaves. The base of the plant is wavy and curved, but it spreads out wider toward the top. The edges of the plant are smooth, and when viewed from the surface of the plant, the cells are paired in polygons with no edges, and the chloroplasts are on the opposite side of the paired cells. In cross section, the cell is square, and the chloroplast is usually located at the waist of the cell, but rarely is located on the surface of the plant.

Opintia humifusa (Eastern prickly pear) is a cactus of the genus Opintia (Opintia sp.) native to Korea that can overwinter inland, and is distinguished from prickly pear, a cactus native to Jeju Island. Prickly pear is also called a palm cactus because its stem has a shape similar to that of a palm. It contains various important nutrients such as phenolic substances, flavonoids, dietary fiber, vitamin C, calcium, minerals, amino acids, and complex polysaccharides.

In the present invention, a complex extract using Crayon chinensis, Longus chinensis, and Prickly pear is applied to a body wash composition, and the complex extract has excellent anti-aging effect through excellent antioxidant and anti-inflammatory functionality.

The complex extract is,

Washing the leaves of the Chinese herbaceous plant, the Chinese herbaceous plant, and the Chinese prickly pear and drying them at a temperature of 48-52°C for 2-4 hours; Preparing a mixed powder by grinding dried Chinese herbaceous leaves, Chinese apricots and prickly prickly pear and mixing them at a weight ratio of 1:1:1; Mixing 8-12 parts by weight of the mixed powder and 88-92 parts by weight of purified water and performing primary hot water extraction at a temperature of 118-122°C for 5-7 hours; After the first hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a first extract; After the first hot water extraction and filtering with filter paper, 8-12 parts by weight of the remaining solids and 88-92 parts by weight of purified water were mixed, and 0.8-1.2 parts by weight of tocopherol and [BMIM][BF ₄ ](1-butyl-3- Adding 0.8-1.2 parts by weight of methylimidazolium tetrafluoroborate) and performing secondary hot water extraction at a temperature of 88-92°C for 10-14 hours while stirring; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a secondary extract; It is preferable to use one prepared by performing the step of mixing the primary extract and the secondary extract.

In preparing the complex extract, a two-stage hot water extraction is applied, and after a pretreatment process is performed along with the preparation of the extract through the first hot water extraction, a second hot water extraction is performed, and tocopherol and ionic liquid [ The extraction performance is improved by simultaneously applying BMIM[BF ₄ ], resulting in excellent extraction efficiency of active ingredients. Accordingly, when the above complex extract is applied, the anti-aging effect is improved through superior antioxidant and anti-inflammatory functionality.

In addition, the present invention

Washing the leaves of the Chinese herbaceous plant, the Chinese herbaceous plant, and the Chinese prickly pear and drying them at a temperature of 48-52°C for 2-4 hours; Preparing a mixed powder by grinding dried Chinese herbaceous leaves, Chinese apricots and prickly prickly pear and mixing them at a weight ratio of 1:1:1; Mixing 8-12 parts by weight of the mixed powder and 88-92 parts by weight of purified water and performing primary hot water extraction at a temperature of 118-122°C for 5-7 hours; After the first hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a first extract; After the first hot water extraction and filtering with filter paper, 8-12 parts by weight of the remaining solids and 88-92 parts by weight of purified water were mixed, and 0.8-1.2 parts by weight of tocopherol and [BMIM][BF ₄ ](1-butyl-3- Adding 0.8-1.2 parts by weight of methylimidazolium tetrafluoroborate) and performing secondary hot water extraction at a temperature of 88-92°C for 10-14 hours while stirring; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a secondary extract; and mixing the primary extract and the secondary extract; preparing a composite extract comprising; and

Egg yolk oil 0.1-0.3 parts by weight, 3-7 parts by weight of the above complex extract, 4-5 parts by weight of sodium C14-16 olefin sulfonate, 3-5 parts by weight of disodium cocoamphodiacetate, 2-4 parts by weight of sodium chloride, decyl Glucoside 2-4 parts by weight, glycerin 0.9-1.1 parts by weight, acrylate copolymer 0.09-0.11 parts by weight, citric acid 0.09-0.11 parts by weight, hexylene glycol 0.09-0.11 parts by weight, C12-13 Alkes- 9 0.09-0.11 parts by weight, coco-betaine 0.09-0.11 parts by weight, tetradecene 0.09-0.11 parts by weight, hydroxyacetophenone 0.4-0.6 parts by weight, hexadecene 0.09-0.11 parts by weight, styrene/acrylate copolymer 0.4-0.6 parts by weight, dipropylene glycol 0.2-0.4 parts by weight, ethylhexylglycerin 0.1-0.3 parts by weight, 1,2-hexanediol 0.1-0.3 parts by weight, disodium EDTA 0.04-0.06 parts by weight, Sodium citrate 0.00009-0.00011 parts by weight, tocopherol 0.00009-0.00011 parts by weight, lemon peel oil 0.09-0.11 parts by weight, secretion tree oil 0.09-0.11 parts by weight, lime whole plant oil 0.09-0.11 parts by weight, citronella oil 0.09-0.11 parts by weight, mixing 0.3-0.5 parts by weight of limonene, 0.3-0.5 parts by weight of geraniol, 0.3-0.5 parts by weight of citronellol, and 80.2497-80.2499 parts by weight of purified water; providing a method for producing a body wash composition comprising: .

Hereinafter, the manufacturing method of the body wash composition according to the present invention will be described in detail in each step.

First, the method for producing a body wash composition according to the present invention includes preparing a complex extract. The step of preparing the complex extract includes washing the leaves of E. chinensis, Corolla, and Prickly pear, and drying them at a temperature of 48-52° C. for 2-4 hours; Preparing a mixed powder by grinding dried Chinese herbaceous leaves, Chinese apricots, and Chinese prickly pear and mixing them at a weight ratio of 1:1:1; Mixing 8-12 parts by weight of the mixed powder and 88-92 parts by weight of purified water and performing primary hot water extraction at a temperature of 118-122°C for 5-7 hours; After primary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a primary extract; After the first hot water extraction and filtering with filter paper, 8-12 parts by weight of the remaining solids and 88-92 parts by weight of purified water were mixed, and 0.8-1.2 parts by weight of tocopherol and [BMIM][BF ₄ ](1-butyl-3- Adding 0.8-1.2 parts by weight of methylimidazolium tetrafluoroborate) and performing secondary hot water extraction at a temperature of 88-92°C for 10-14 hours while stirring; After secondary hot water extraction, filtering through filter paper and then freeze-drying the filtrate to prepare a secondary extract; and mixing the primary extract and the secondary extract.

In preparing the complex extract, a two-stage hot water extraction is applied, and after a pretreatment process is performed along with the preparation of the extract through the first hot water extraction, a second hot water extraction is performed, and tocopherol and ionic liquid [ The extraction performance is improved by simultaneously applying BMIM[BF ₄ ], resulting in excellent extraction efficiency of active ingredients. Accordingly, when the above complex extract is applied, the anti-aging effect is improved through superior antioxidant and anti-inflammatory functionality.

Next, the method for producing the body wash composition according to the present invention is 0.1-0.3 parts by weight of egg yolk oil, 3-7 parts by weight of the complex extract, 4-5 parts by weight of sodium C14-16 olefin sulfonate, and 3 parts by weight of disodium cocoamphodiacetate. -5 parts by weight, sodium chloride 2-4 parts by weight, decyl glucoside 2-4 parts by weight, glycerin 0.9-1.1 parts by weight, acrylate copolymer 0.09-0.11 parts by weight, citric acid 0.09-0.11 parts by weight, hexylene glycol Lycol 0.09-0.11 parts by weight, C12-13 Alkes-9 0.09-0.11 parts by weight, Coco-Betaine 0.09-0.11 parts by weight, Tetradecene 0.09-0.11 parts by weight, Hydroxyacetophenone 0.4-0.6 parts by weight, Hexadecyl Decene 0.09-0.11 parts by weight, styrene/acrylate copolymer 0.4-0.6 parts by weight, dipropylene glycol 0.2-0.4 parts by weight, ethylhexylglycerin 0.1-0.3 parts by weight, 1,2-hexanediol 0.1-0.3 Parts by weight, Disodium EDTA 0.04-0.06 parts by weight, Sodium citrate 0.00009-0.00011 parts by weight, Tocopherol 0.00009-0.00011 parts by weight, Lemon peel oil 0.09-0.11 parts by weight, Secretion tree oil 0.09-0.11 parts by weight, Lime whole plant Mixing 0.09-0.11 parts by weight of oil, 0.09-0.11 parts by weight of citronella oil, 0.3-0.5 parts by weight of limonene, 0.3-0.5 parts by weight of geraniol, 0.3-0.5 parts by weight of citronellol, and 80.2497-80.2499 parts by weight of purified water. Includes steps.

Hereinafter, the present invention will be explained in more detail by the following examples.

However, the following examples only illustrate the content of the present invention and the scope of the invention is not limited by the examples and experimental examples.

<Preparation Example 1> Preparation of complex extract-1

The mixed powder was prepared by washing the leaves of dysentery, dried apricots, and prickly pear, dried at a temperature of 50°C for 3 hours, pulverized, and mixed at a weight ratio of 1:1:1. 10 parts by weight of the mixed powder and 90 parts by weight of purified water were mixed, and primary hot water extraction was performed at a temperature of 120°C for 6 hours.

After the first hot water extraction, it was filtered through filter paper and the filtrate was freeze-dried to prepare the first extract.

Mix 10 parts by weight of the remaining solids and 90 parts by weight of purified water, add 1 part by weight of tocopherol and 1 part by weight of [BMIM][BF ₄ ](1-butyl-3-methylimidazolium tetrafluoroborate), and stir at a temperature of 90°C. A second hot water extraction was performed for 12 hours.

After secondary hot water extraction, it was filtered through filter paper and the filtrate was freeze-dried to prepare a secondary extract.

A composite extract was prepared by mixing the primary and secondary extracts.

<Preparation Example 2> Preparation of complex extract-2

The mixed powder was prepared by washing the leaves of dysentery, dried apricots, and prickly pear, dried at a temperature of 50°C for 3 hours, pulverized, and mixed at a weight ratio of 1:1:1. 10 parts by weight of the mixed powder and 90 parts by weight of purified water were mixed, and primary hot water extraction was performed at a temperature of 120°C for 6 hours.

After the first hot water extraction, it was filtered through filter paper and the filtrate was freeze-dried to prepare the first extract.

10 parts by weight of the remaining solids and 90 parts by weight of purified water were mixed, and secondary hot water extraction was performed at a temperature of 90°C for 12 hours.

After secondary hot water extraction, it was filtered through filter paper and the filtrate was freeze-dried to prepare a secondary extract.

A composite extract was prepared by mixing the primary and secondary extracts.

<Preparation Example 3> Preparation of complex extract-3

The mixed powder was prepared by washing the leaves of dysentery, dried apricots, and prickly pear, dried at a temperature of 50°C for 3 hours, pulverized, and mixed at a weight ratio of 1:1:1. 10 parts by weight of the mixed powder and 90 parts by weight of purified water were mixed, and hot water extraction was performed at a temperature of 120°C for 6 hours.

After hot water extraction, it was filtered through filter paper and the filtrate was freeze-dried to prepare a composite extract.

<Example 1> Preparation of body wash composition-1

Egg yolk oil 0.2 parts by weight, sodium C14-16 olefin sulfonate 4.5 parts by weight, disodium cocoamphodiacetate 4 parts by weight, sodium chloride 3 parts by weight, decyl glucoside 3 parts by weight, glycerin 1 part by weight, acrylate copolymer 0.1 parts by weight , 0.1 part by weight of citric acid, 0.1 part by weight of hexylene glycol, 0.1 part by weight of C12-13 Alkes-9, 0.1 part by weight of coco-betaine, 0.1 part by weight of tetradecene, 0.5 part by weight of hydroxyacetophenone, 0.1 part by weight of hexadecene, 0.5 part by weight of styrene/acrylate copolymer, 0.3 part by weight of dipropylene glycol, 0.2 part by weight of ethylhexylglycerin, 0.2 part by weight of 1,2-hexanediol, 0.05 part by weight of disodium EDTA. Parts by weight, sodium citrate 0.0001 parts by weight, tocopherol 0.0001 parts by weight, lemon peel oil 0.1 parts by weight, secretion tree oil 0.1 parts by weight, lime whole plant oil 0.1 parts by weight, citronella oil 0.1 parts by weight, limonene 0.4 parts by weight, agent A body wash composition was prepared by mixing 0.4 parts by weight of raniol, 0.4 parts by weight of citronellol, and 80.2498 parts by weight of purified water.

<Example 2> Preparation of body wash composition-2

0.2 parts by weight of egg yolk oil, 5 parts by weight of the complex extract prepared in Preparation Example 1, 4.5 parts by weight of sodium C14-16 olefin sulfonate, 4 parts by weight of disodium cocoamphodiacetate, 3 parts by weight of sodium chloride, 3 parts by weight of decyl glucoside , 1 part by weight of glycerin, 0.1 part by weight of acrylate copolymer, 0.1 part by weight of citric acid, 0.1 part by weight of hexylene glycol, 0.1 part by weight of C12-13 Alkes-9, 0.1 part by weight of coco-betaine, tetra 0.1 part by weight of decene, 0.5 part by weight of hydroxyacetophenone, 0.1 part by weight of hexadecene, 0.5 part by weight of styrene/acrylate copolymer, 0.3 part by weight of dipropylene glycol, 0.2 part by weight of ethylhexylglycerin, 1,2- Hexanediol 0.2 parts by weight, Disodium EDTA 0.05 parts by weight, Sodium citrate 0.0001 parts by weight, Tocopherol 0.0001 parts by weight, Lemon peel oil 0.1 parts by weight, Secretion tree oil 0.1 parts by weight, Lime herb oil 0.1 parts by weight, sheet A body wash composition was prepared by mixing 0.1 parts by weight of ronella oil, 0.4 parts by weight of limonene, 0.4 parts by weight of geraniol, 0.4 parts by weight of citronellol, and 80.2498 parts by weight of purified water.

<Example 3> Preparation of body wash composition-3

0.2 parts by weight of egg yolk oil, 5 parts by weight of the complex extract prepared in Preparation Example 2, 4.5 parts by weight of sodium C14-16 olefin sulfonate, 4 parts by weight of disodium cocoamphodiacetate, 3 parts by weight of sodium chloride, 3 parts by weight of decyl glucoside , 1 part by weight of glycerin, 0.1 part by weight of acrylate copolymer, 0.1 part by weight of citric acid, 0.1 part by weight of hexylene glycol, 0.1 part by weight of C12-13 Alkes-9, 0.1 part by weight of coco-betaine, tetra 0.1 part by weight of decene, 0.5 part by weight of hydroxyacetophenone, 0.1 part by weight of hexadecene, 0.5 part by weight of styrene/acrylate copolymer, 0.3 part by weight of dipropylene glycol, 0.2 part by weight of ethylhexylglycerin, 1,2- Hexanediol 0.2 parts by weight, Disodium EDTA 0.05 parts by weight, Sodium citrate 0.0001 parts by weight, Tocopherol 0.0001 parts by weight, Lemon peel oil 0.1 parts by weight, Secretion tree oil 0.1 parts by weight, Lime herb oil 0.1 parts by weight, sheet A body wash composition was prepared by mixing 0.1 parts by weight of ronella oil, 0.4 parts by weight of limonene, 0.4 parts by weight of geraniol, 0.4 parts by weight of citronellol, and 80.2498 parts by weight of purified water.

<Example 4> Preparation of body wash composition-4

0.2 parts by weight of egg yolk oil, 5 parts by weight of the complex extract prepared in Preparation Example 1, 4.5 parts by weight of sodium C14-16 olefin sulfonate, 4 parts by weight of disodium cocoamphodiacetate, 3 parts by weight of sodium chloride, 3 parts by weight of decyl glucoside , 1 part by weight of glycerin, 0.1 part by weight of acrylate copolymer, 0.1 part by weight of citric acid, 0.1 part by weight of hexylene glycol, 0.1 part by weight of C12-13 Alkes-9, 0.1 part by weight of coco-betaine, tetra 0.1 part by weight of decene, 0.5 part by weight of hydroxyacetophenone, 0.1 part by weight of hexadecene, 0.5 part by weight of styrene/acrylate copolymer, 0.3 part by weight of dipropylene glycol, 0.2 part by weight of ethylhexylglycerin, 1,2- Hexanediol 0.2 parts by weight, Disodium EDTA 0.05 parts by weight, Sodium citrate 0.0001 parts by weight, Tocopherol 0.0001 parts by weight, Lemon peel oil 0.1 parts by weight, Secretion tree oil 0.1 parts by weight, Lime herb oil 0.1 parts by weight, sheet A body wash composition was prepared by mixing 0.1 parts by weight of ronella oil, 0.4 parts by weight of limonene, 0.4 parts by weight of geraniol, 0.4 parts by weight of citronellol, and 80.2498 parts by weight of purified water.

<Experimental Example 1> Analysis of antioxidant functionality, anti-inflammatory functionality, and anti-aging effect

1. Antioxidant functionality

Using the composite extract prepared in Preparation Example 1-3 as a sample, the antioxidant power was measured by DPPH (2,2-Diphenyl-1-picryl-hydrazyl) radical scavenging activity. DPPH radical scavenging ability was determined by referring to the method of Mensor et al. 80 ㎕ of 0.2mM DPPH ethanol solution was added to each sample, stirred for 1 minute, reacted in a 25°C incubator for 10 minutes, and absorbance was measured at 517 nm using an ELISA reader. DPPH radical scavenging activity was expressed as a percentage according to Equation 1 below, and the results are shown in Table 1 below.

<Equation 1>

DPPH radical scavenging activity (%) = {(1-absorbance when adding sample)/absorbance of control}×100

DPPH radical scavenging activity (%) Manufacturing Example 1 55.3 Production example 2 52.8 Production example 3 50.2

As shown in Table 1, the complex extract according to the present invention was measured to have a high DPPH radical scavenging activity value, and it can be confirmed that it has excellent antioxidant functionality.

2. Anti-inflammatory functionality

The composite extract prepared in Preparation Example 1-3 was used as a sample to confirm the effect on inhibiting NO (Nitric Oxide) production. Normal formation of NO plays an important role in killing bacteria or removing tumors, but in inflammatory conditions, NO produced by iNOS not only promotes inflammatory reactions such as vascular permeability and edema, but also promotes the biosynthesis of inflammatory mediators to reduce inflammation. It is known to worsen. Raw 264.7 cells were adjusted to ⁵ Added and cultured for 24 hours. The amount of NO produced was measured using a NO detection kit (iNtRON) and calculated according to Equation 2 below, and the NO production inhibition rate results are shown in Table 2 below.

<Equation 2>

NO production inhibition rate (%) = (NO amount of control group - NO amount of extract)/NO amount of control group

NO production inhibition rate (%) Manufacturing Example 1 77.5 Production example 2 73.4 Production example 3 70.7

As shown in Table 2 above, the complex extract according to the present invention showed a very high NO production inhibition rate and showed excellent anti-inflammatory effects.

3. Anti-aging effect

The composite extract prepared in Preparation Example 1-3 was used as a sample to confirm the effect of inhibiting aging of fibroblasts due to hydrogen peroxide treatment. Human normal fibroblast (ATCC) cells were inoculated into a 6-well microplate containing DMEM medium at approximately 1×10 ⁵ cells and incubated in a 5% CO ₂ incubator at 37°C for 24 hours. Cultured. Afterwards, the complex extract prepared in Preparation Example 1-3 and hydrogen peroxide (H ₂ O ₂ 300 μM), which can induce oxidative stress, were dissolved together in the culture medium and treated. After 72 hours, the cell culture supernatant was removed, the cells were detached by treatment with trypsin-EDTA, and the cells were fluorescently stained with Dojindo's SPiDER-ßGal for 15 minutes and flow cytometry (FACS Calibur, Becton Dickinson, San Francisco). Jose, CA), and cells were counted. Changes in cellular aging were observed by confirming the proportion of cells showing aging-related β-galactosidase activity. The resulting values were converted based on 100% of the control group, and the results are shown in Table 3 below. (-: no effect, +: weak effect, ++: medium effect, +++: strong effect, ++++: very strong effect)

Fibroblasts due to hydrogen peroxide treatment
Degree of anti-aging Manufacturing Example 1 +++ Production example 2 ++ Production example 3 ++

As shown in Table 3, the composite extract according to the present invention showed a very high degree of inhibition of fibroblast aging due to hydrogen peroxide treatment.

In this way, antioxidant functionality and anti-inflammatory functionality were secured, and it was confirmed that the anti-aging effect was excellent.

<Experimental Example 2> Analysis of skin moisturizing functionality

A skin moisturizing functionality test was performed using the body wash composition prepared in Examples 1-4 as a sample. 40 adult men and women (20 each) aged 30-40 years with sensitive skin were randomly divided into 4 groups of 5 adults each, and each was treated with the body wash composition prepared in Examples 1-4 above. The skin moisturizing functionality was confirmed immediately after taking a shower. Skin moisturizing functionality was measured using a skin moisture meter (Corneometer, CM825) of volunteers who waited indoors under constant temperature and humidity conditions (20-22°C, relative humidity 40-60%) 30 minutes before the start of the test. The measured capacitance value is expressed as arbitrary capacitance units (A.U.) between 0 and 120, and the results are shown in Table 4 below.

Moisturizing power (A.U.) Example 1 63.1 Example 2 71.2 Example 3 69.8 Example 4 68.3

As shown in Table 4, it was confirmed that the body wash composition according to the present invention exhibited very excellent skin moisturizing functionality.

Claims (3)

0.1-0.3 parts by weight of egg yolk oil, 3-7 parts by weight of a complex extract of 1:1:1 weight ratio of Elephant chinensis extract, Chinese herb extract, and Prickly pear extract, 4-5 parts by weight of sodium C14-16 olefin sulfonate, die Sodium cocoamphodiacetate 3-5 parts by weight, sodium chloride 2-4 parts by weight, decyl glucoside 2-4 parts by weight, glycerin 0.9-1.1 parts by weight, acrylate copolymer 0.09-0.11 parts by weight, citric acid 0.09-0.11 Parts by weight, hexylene glycol 0.09-0.11 parts by weight, C12-13Alces-9 0.09-0.11 parts by weight, Coco-betaine 0.09-0.11 parts by weight, tetradecene 0.09-0.11 parts by weight, hydroxyacetophenone 0.4 -0.6 parts by weight, hexadecene 0.09-0.11 parts by weight, styrene/acrylate copolymer 0.4-0.6 parts by weight, dipropylene glycol 0.2-0.4 parts by weight, ethylhexylglycerin 0.1-0.3 parts by weight, 1,2- Hexanediol 0.1-0.3 parts by weight, Disodium EDTA 0.04-0.06 parts by weight, Sodium citrate 0.00009-0.00011 parts by weight, Tocopherol 0.00009-0.00011 parts by weight, Lemon peel oil 0.09-0.11 parts by weight, Secretion tree oil 0.09- 0.11 parts by weight, lime starch oil 0.09-0.11 parts by weight, citronella oil 0.09-0.11 parts by weight, limonene 0.3-0.5 parts by weight, geraniol 0.3-0.5 parts by weight, citronellol 0.3-0.5 parts by weight, and purified water 80.2497 -A body wash composition comprising 80.2499 parts by weight. delete delete