KR102411330B1 - Method for manufacturing gondree powder with high content of pectinarin - Google Patents
Method for manufacturing gondree powder with high content of pectinarin Download PDFInfo
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- KR102411330B1 KR102411330B1 KR1020200182991A KR20200182991A KR102411330B1 KR 102411330 B1 KR102411330 B1 KR 102411330B1 KR 1020200182991 A KR1020200182991 A KR 1020200182991A KR 20200182991 A KR20200182991 A KR 20200182991A KR 102411330 B1 KR102411330 B1 KR 102411330B1
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- 239000000843 powder Substances 0.000 title claims abstract description 53
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 17
- 238000000034 method Methods 0.000 title description 3
- 238000000227 grinding Methods 0.000 claims abstract description 27
- 239000002245 particle Substances 0.000 claims abstract description 21
- 238000009826 distribution Methods 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 238000010298 pulverizing process Methods 0.000 claims abstract description 10
- 238000001035 drying Methods 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims abstract description 5
- 238000002360 preparation method Methods 0.000 claims abstract description 4
- DUXQKCCELUKXOE-UHFFFAOYSA-N Pectolinarigenin-Biosid Natural products C1=CC(OC)=CC=C1C(OC1=C2)=CC(=O)C1=C(O)C(OC)=C2OC1C(O)C(O)C(O)C(COC2C(C(O)C(O)C(C)O2)O)O1 DUXQKCCELUKXOE-UHFFFAOYSA-N 0.000 abstract description 23
- SEXCCMQJDXQBOE-UHFFFAOYSA-N Pectolinarin Natural products C1=CC(OC)=CC=C1C(OC1=C2)=CC(=O)C1=C(O)C(OC)=C2OC1C(O)C(O)C(OC2C(C(O)C(O)C(C)O2)O)C(CO)O1 SEXCCMQJDXQBOE-UHFFFAOYSA-N 0.000 abstract description 23
- DUXQKCCELUKXOE-CBBZIXHGSA-N pectolinarin Chemical compound C1=CC(OC)=CC=C1C(OC1=C2)=CC(=O)C1=C(O)C(OC)=C2O[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@H]2[C@@H]([C@H](O)[C@@H](O)[C@H](C)O2)O)O1 DUXQKCCELUKXOE-CBBZIXHGSA-N 0.000 abstract description 23
- 238000000605 extraction Methods 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 description 8
- 238000010586 diagram Methods 0.000 description 4
- 238000003921 particle size analysis Methods 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 238000004128 high performance liquid chromatography Methods 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 239000002270 dispersing agent Substances 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 230000037303 wrinkles Effects 0.000 description 2
- 241000132536 Cirsium Species 0.000 description 1
- 102000000380 Matrix Metalloproteinase 1 Human genes 0.000 description 1
- 108010016113 Matrix Metalloproteinase 1 Proteins 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000005445 natural material Substances 0.000 description 1
- 230000009759 skin aging Effects 0.000 description 1
- 239000010421 standard material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/01—Instant products; Powders; Flakes; Granules
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/22—Agglomeration or granulation with pulverisation of solid particles, e.g. in a free-falling curtain
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/10—Drying, dehydrating
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/31—Mechanical treatment
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- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Disintegrating Or Milling (AREA)
Abstract
곤드레의 지표성분이면서, 주요 기능 성분인 pectolinarin(펙토리나린)의 추출 조건이 구명되지 않아, 곤드레 분말로부터 펙토리나린의 추출량에 차이가 있고, 곤드레 분말로부터 가능한 많은 양의 펙토리나린을 추출하지 못하여 원료의 이용률이 낮은 문제가 있다.
본 발명은 상기와 같은 문제를 해결하기 위하여, 곤드레 원료를 준비하는 원료준비(S1); 및 상기 곤드레 원료를 조분쇄하는 조분쇄단계(S2); 및 상기 조분쇄단계에서 조분쇄한 곤드레를 열풍 건조기로 60℃에서 8시간 건조하는 조분쇄 후 건조단계(S3); 및 상기 조분쇄 후 건조단계에서 건조한 건조물을 2,500 ~ 3,800 RPM으로 미세분쇄하여 입도분포 X90이 139 ~ 150㎛ 인 것을 특징으로 하는 펙토리나린 고함유 곤드레 분말 제조방법을 제공한다.
상기와 같은 구성에 의하여 곤드레 분말로부터 최대의 펙토리나린을 추출하여 사용함으로써 원료의 이용효율을 높이고 이에 따라 생산원가를 낮출 수 있는 효과가 있다.As the extraction conditions for pectolinarin, which is an index component and main functional component of Gondree, are not determined, there is a difference in the amount of pectolinarin extracted from Gondree powder. There is a problem with the low utilization rate.
In order to solve the above problems, the present invention provides a raw material preparation (S1) for preparing a gondre raw material; and a coarse grinding step (S2) of coarsely grinding the gondre raw material; and a drying step (S3) of coarsely pulverizing the gondree, which was coarsely pulverized in the coarse pulverization step, at 60° C. for 8 hours with a hot air dryer; and finely pulverizing the dried material in the drying step after the coarse pulverization at 2,500 to 3,800 RPM to provide a method for producing pectinarin-rich gondre powder, characterized in that the particle size distribution X90 is 139 to 150 μm.
By extracting and using the maximum pectinarin from the gondre powder according to the above configuration, there is an effect of increasing the utilization efficiency of raw materials and thereby lowering the production cost.
Description
본 출원 발명은 고려엉겅퀴 또는 곤드레라 불리는 천연물질로부터 펙토리나린(pectolinarin) 성분을 이용하는 기술에 관한 것이다. 더욱 자세하게는 상기 곤드레의 가공과정에서 상기 펙토리나린의 함량을 높이는 기술에 관한 것이다.The present invention relates to a technology using a pectolinarin component from a natural material called Korean thistle or gondre. More particularly, it relates to a technique for increasing the content of the pectinarin during the processing of the gondre.
본 발명의 출원 이전의 선행기술로 펙토리나린을 유효성분으로 함유하는 대피부 주름 개선 및 피부 노화 방지용 화장료 조성물에 관한 기술이 개시되어 있다. 이 기술에서는 펙토리나린은 MMP-1을 억제하여 뛰어난 피부 주름 개선 및 노화 방지 효과가 있는 기술을 개시하고 있다.As a prior art prior to the filing of the present invention, there is disclosed a technology related to a cosmetic composition for improving skin wrinkles and preventing skin aging containing pectinarin as an active ingredient. In this technology, pectinarin inhibits MMP-1 and discloses a technology that has excellent skin wrinkle improvement and anti-aging effects.
또 다른 선행기술로 곤드레추출물을 함유하는 레트로트형 누룽지에 관한 기술이다. 이 기술에서는 곤드레추출물의 추출조건을 개시하고 있다.Another prior art is a technology related to a retro-type nurungji containing a gondre extract. In this technology, the extraction conditions of the Gondree extract are disclosed.
곤드레의 지표성분이면서, 주요 기능 성분인 pectolinarin(펙토리나린)의 추출 조건이 구명되지 않아, 곤드레 분말로부터 펙토리나린의 추출량에 차이가 있고, 곤드레 분말로부터 가능한 많은 양의 펙토리나린을 추출하지 못하여 원료의 이용률이 낮은 문제가 있다. 본 발명은 상기 곤드레 분말로부터 상기 펙토리나린을 추출하는 최적의 추출조건을 찾아 곤드레 분말로부터 최대량의 펙토리나린을 추출하여 이용하고자 한다.As the extraction conditions for pectolinarin, which is an index component and main functional component of gondae, are not known, there is a difference in the amount of pectolinarin extracted from gondre powder. There is a problem with the low utilization rate. The present invention is to find the optimal extraction conditions for extracting the pectinarin from the gondree powder, and to extract and use the maximum amount of pectinarin from the gondre powder.
삭제delete
본 발명은 상기와 같은 문제를 해결하기 위하여 아래의 과제해결 수단을 제공한다.
곤드레 원료를 준비하는 원료준비(S1); 및The present invention provides the following problem solving means in order to solve the above problems.
Raw material preparation (S1) for preparing gondre raw materials; and
상기 곤드레 원료를 조분쇄하는 조분쇄단계(S2); 및a coarse grinding step of coarsely grinding the gondre raw material (S2); and
상기 조분쇄단계에서 조분쇄한 곤드레를 열풍 건조기로 60℃에서 8시간 건조하는 조분쇄 후 건조단계(S3); 및Drying step (S3) after coarse grinding of coarsely pulverized gondree in the coarse pulverization step and dried at 60° C. for 8 hours with a hot air dryer; and
상기 조분쇄 후 건조단계에서 건조한 건조물을 2,500 ~ 3,800 RPM으로 미세분쇄하여 입도분포 X90이 139 ~ 150㎛ 인 것을 특징으로 하는 펙토리나린 고함유 곤드레 분말 제조방법을 제공한다.After the coarse grinding, the dried material is finely pulverized at 2,500 to 3,800 RPM in the drying step to provide a method for producing pectinarin-rich gondre powder, characterized in that the particle size distribution X90 is 139 to 150 μm.
또한, 상기 펙토리나린 고함유 곤드레 분말 제조방법으로 제조된 곤드레분말 1g 당 펙토리나린이 10.24 ~ 11.07mg 함유된 것을 특징으로 하는 펙토리나린 고함유 곤드레 분말 제조방법을 제공한다.In addition, there is provided a method for producing a gondre powder with a high pectorinarin content, characterized in that 10.24 to 11.07 mg of pectorinarin is contained per 1 g of the gondre powder prepared by the method for producing a gondre powder with a high pectinarine content.
상기와 같은 구성에 의하여 곤드레 분말로부터 최대의 펙토리나린을 추출하여 사용함으로써 원료의 이용효율을 높이고 이에 따라 생산원가를 낮출 수 있는 효과가 있다.By extracting and using the maximum pectinarin from the gondre powder according to the above configuration, there is an effect of increasing the utilization efficiency of raw materials and thereby lowering the production cost.
도 1은 본 발명의 곤드레 분말의 미세분쇄/공기분급 조건
도 2는 본 발명의 미세분쇄/분급 장비
도 3은 본 발명의 HPLC 펙토리나린 분석조건
도 4는 본 발명의 분쇄 조건별 곤드레 분말의 입도분포
도 5는 본 발명의 분쇄 조건별 펙토리나린 함량조건
도 6은 본 발명의 입도분포에 따른 곤드레 분말의 펙토리나린 함량
도 7은 본 발명의 분쇄 조건 S-1 에 따른 곤드레 분말의 입자분포도 이다.
도 8은 본 발명의 분쇄 조건 S-2 에 따른 곤드레 분말의 입자분포도 이다.
도 9는 본 발명의 분쇄 조건 S-3 에 따른 곤드레 분말의 입자분포도 이다.
도 10은 본 발명의 분쇄 조건 S-4 에 따른 곤드레 분말의 입자분포도 이다.1 is a condition of fine grinding/air classification of gondre powder of the present invention;
Figure 2 is a fine grinding / classification equipment of the present invention
Figure 3 is HPLC Factorinarin analysis conditions of the present invention
4 is a particle size distribution of gondre powder according to grinding conditions of the present invention;
5 is a pectinarin content condition for each grinding condition of the present invention.
6 is a pectinarin content of gondre powder according to the particle size distribution of the present invention;
7 is a particle distribution diagram of gondre powder according to the grinding condition S-1 of the present invention.
8 is a particle distribution diagram of gondre powder according to the grinding condition S-2 of the present invention.
9 is a particle distribution diagram of gondre powder according to the grinding condition S-3 of the present invention.
10 is a particle distribution diagram of gondre powder according to the grinding condition S-4 of the present invention.
본 발명은 곤드레 분말의 분쇄 조건에 따른 곤드레 분말로부터의 펙토리나린 추출량을 최적화하는 것이다. 기존에는 이러한 펙토리나린 추출량과 곤드레 분말의 분쇄 조건의 구명이 없어 적당히 분쇄한 또는 가지고 있는 장비로 분쇄한 곤드레 분말로부터 펙토리나린을 추출하여 사용하여왔다. 그렇기 때문에 원료인 곤드레 분말로부터 가능한 양의 펙토리나린을 추출하지 못하여 생산수율이 낮아, 생산원가가 증가하는 문제가 있었다.The present invention optimizes the amount of pectinarin extracted from gondree powder according to the grinding conditions of gondre powder. In the past, there was no clarification of the pectinarin extraction amount and the pulverization conditions of the gondre powder, so it has been used by extracting pectinarin from the gondre powder that has been properly pulverized or pulverized with the equipment it has. Therefore, it was not possible to extract the possible amount of pectinarin from the raw gondre powder, so there was a problem in that the production yield was low, and the production cost increased.
본 발명은 동일한 원료의 곤드레 분말로부터 가능한 많은 양의 펙토리나린을 추출하여 생산원가를 낮추고, 낮은 가격의 펙토리나린을 생산함으로써 펙토리나린을 대량으로 저가로 공급하여 그 사용성을 높이고자 하는데 그 목적이 있다.The present invention is to reduce the production cost by extracting as much pectinarin as possible from the gondre powder of the same raw material, and to increase the usability by supplying pectinarin at a low price in large quantities by producing pectinarin at a low price. .
이를 위하여 하기의 곤드레 분쇄방법과 펙토리나린 추출방법을 사용하였다.For this purpose, the following gondre grinding method and pectinarin extraction method were used.
1. Pectolinarin 고함유 곤드레 분말화 1. Powdered Gondree with high Pectolinarin content
<실시예 1 실험방법><Example 1 Experimental Method>
1) 미세분쇄/분급 기술을 이용한 곤드레 분말 제조 1) Manufacture of gondre powder using fine grinding/classification technology
본 발명에서 사용한 건조 곤드레 원료는 ㈜정선약초백화점(Jeongseon, Korea)로부터 구입하였다. 건조 곤드레를 미세분쇄/분급 처리하기 전, 분쇄 효율을 높이고자 MS-200 분쇄기(Myeongseong Co. Ltd, Chengju, Korea)를 사용하여 조분쇄(S-1) 한 후 열풍건조기로 60℃에서 8시간 재건조를 실시하였다. 건조된 조분쇄물(S-1)은 Soro-100N (도 2 참조) 미세분쇄/분급기(Sorobio Co. Ltd, Jeonju, Korea)를 이용하여 각각 2,500~2,800 RPM(S-2), 3,500 RPM(S-3), 3500~3,800 RPM(S-4)으로 곤드레 미세분쇄/분급을 실시하여 pectolinarin 고함유 곤드레 분말을 제조하였다. 조분쇄된 곤드레 시료 투입량(각 7.5 Kg) 대비 S-2, S-3, S-4 조건에서 곤드레 분말의 회수량은 각각, 1.6 Kg(21.3%), 1.6 Kg(21.3%), 1.7 Kg(22.7%)으로 나타났다. 미세분쇄/분급된 곤드레 분말의 입도가 지표성분(pectolinarin) 함량에 미치는 영향을 살펴보고자 500 mesh 이하(25 μm 이하), 270~500 mesh(25~53 μm), 170~270 mesh (53~90 μm) 및 100~170 mesh (90~150 μm) 입도별로 pectolinarin 함량을 분석하였다(도 1 참조)The dried gondre raw materials used in the present invention were purchased from Jeongseon Herbal Medicine Department Store (Jeongseon, Korea). Before fine pulverizing/classifying dried gondae, coarsely pulverize (S-1) using an MS-200 pulverizer (Myeongseong Co. Ltd, Chengju, Korea) to increase pulverization efficiency, and then use a hot air dryer at 60℃ for 8 hours. Re-drying was performed. The dried coarsely pulverized product (S-1) was 2,500 to 2,800 RPM (S-2) and 3,500 RPM, respectively, using a Soro-100N (see FIG. 2) fine pulverizer/classifier (Sorbio Co. Ltd, Jeonju, Korea). (S-3), 3500~3,800 RPM (S-4) was performed to finely pulverize/classify gondree to prepare a gondre powder with a high pectolinarin content. Compared to the amount of coarsely pulverized Gondree sample input (7.5 Kg each), the recovery amount of Gondree powder under S-2, S-3, and S-4 conditions was 1.6 Kg (21.3%), 1.6 Kg (21.3%), and 1.7 Kg ( 22.7%). 500 mesh or less (25 μm or less), 270-500 mesh (25-53 μm), 170-270 mesh (53-90 μm) and 100-170 mesh (90-150 μm) pectolinarin content was analyzed for each particle size (see Fig. 1).
2) Pectolinarin 분석 2) Pectolinarin Assay
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곤드레 pectolinarin 함량을 분석은 HPLC로 분석하였다(도 3참조). 표준물질 pectolinarin 및 시료를 HPLC로 분석하여 얻은 chromatogram을 비교하여 pectolinarin의 머무름 시간을 확인하였으며 photodiode- array (PDA) spectrum을 확인하여 동일한 spectrum을 나타내는지 확인하여 곤드레에 함유된 pectolinarin의 함량을 분석하였다. The pectolinarin content of Gondree was analyzed by HPLC (see Fig. 3). The retention time of pectolinarin was confirmed by comparing the chromatogram obtained by analyzing the standard material pectolinarin and the sample by HPLC, and the photodiode-array (PDA) spectrum was checked to confirm that the same spectrum was displayed, and the content of pectolinarin contained in gondae was analyzed.
3) 입도분석 3) Particle size analysis
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곤드레 분말 소재의 입도분석은 분산제로 증류수를 사용하였고 1g의 시료를 분취하고 동량의 분산제를 첨가하고 1분간 분산시킨 후, 이를 5회 반복하여 측정하였다. 입도분석은 particle size analyzer(Model Mastersizer 3000, Malvern Panalytical Ltd, Malvern, United Kingdom)를 사용하였다. For particle size analysis of the gondre powder material, distilled water was used as a dispersing agent, and 1 g of a sample was aliquoted, the same amount of a dispersing agent was added and dispersed for 1 minute, and this was repeated 5 times. For particle size analysis, a particle size analyzer (Model Mastersizer 3000, Malvern Panalytical Ltd, Malvern, United Kingdom) was used.
<실시예 2 실험결과><Example 2 Experimental Results>
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1) Pectolinarin 고함유 곤드레 분말의 입도분포1) Particle size distribution of gondre powder with high Pectolinarin content
미세분쇄/분급 기술을 활용한 pectolinarin 고함유 곤드레 분말을 제조한 후, 곤드레 분말의 입도분석을 실시한 결과 먼저 조분쇄 된 곤드레 분말의 입도분포는 X10, X50, X90에서 각각 113, 252, 587 ㎛의 입도분포를 나타내었다(도 7 내지 10). 조분쇄된 곤드레 분말을 2,500~2,800 RPM으로 처리하였을 때 S-2시료의 입도분포는 X10, X50, X90에서 각각 9.42, 63.3, 150 ㎛이었으나, RPM 속도를 조절하여 3,500 RPM으로 처리하였을 때, S-3시료의 입도분포는 X10, X50, X90에서 각각 7.31, 57.9, 147 ㎛로 보다 더 미세분쇄 되었으며, 3500~3,800 RPM으로 처리한 S-4시료의 입도분포는 X10, X50, X90에서 각각 6.64, 49.9, 139 ㎛로 나타나 가장 미분화 된 분말로 나타났다(도 4 참조).After manufacturing gondre powder with high pectolinarin content using fine grinding/classification technology, particle size analysis of the gondre powder was performed. The particle size distribution was shown ( FIGS. 7 to 10 ). The particle size distribution of the S-2 sample was 9.42, 63.3, and 150 μm in X10, X50, and X90, respectively, when the coarsely pulverized gondre powder was treated at 2,500-2,800 RPM. The particle size distribution of the -3 sample was 7.31, 57.9, and 147 ㎛ in X10, X50, and X90, respectively, and the particle size distribution of the S-4 sample treated at 3500~3,800 RPM was 6.64 in X10, X50, and X90, respectively. , 49.9, and 139 μm, indicating the most pulverized powder (see Fig. 4).
이상의 결과로 보았을 때, 조분쇄된 곤드레 분말을 RPM과 처리용량을 각각 달리하여 미세분쇄 곤드레 분말을 제조하였을 때, 회수량을 기준으로 회수율을 21.3~22.7%의 수준으로 나타났으며 이때의 입도분포는 X10은 6.64~9.42 ㎛이었고, X50은 49.9~63.3 ㎛, X90은 139~150 ㎛의 입도분포를 나타내었다. 조건별 곤드레 분말의 입도분포가 펙토리나린 함량 및 효능에 미치는 영향을 조사하였고 이들 분석결과를 토대로 미세분쇄/분급의 최적조건을 설정하였다. Judging from the above results, when finely pulverized Gondre powder was prepared by varying the RPM and processing capacity of the coarsely pulverized Gondree powder, the recovery rate was 21.3~22.7% based on the recovery amount, and the particle size distribution at this time The particle size distribution of X10 was 6.64~9.42 μm, X50 was 49.9~63.3 μm, and X90 was 139~150 μm. The effect of the particle size distribution of Gondree powder for each condition on the content and efficacy of pectinarin was investigated, and the optimal conditions for fine grinding/classification were established based on these analysis results.
2) 곤드레 분말의 pectolinarin 함량 분석 2) Analysis of pectolinarin content of gondae powder
HPLC-PDA를 이용하여 곤드레 분말 샘플의 pectolinarin 함량을 분석한 결과는 도 5와 같다. 조건별 곤드레 분말의 지표성분 함량은 S-3와 S-4 분말에서 각각 11.07±0.05 및 10.95±0.15 mg/g으로 가장 높은 함량을 보였으며 조분쇄된 곤드레 S-1 분말(4.24±0.02 mg/g)에 비해 pectolinarin의 함량은 2.58~3.83배 증가한 것으로 나타났다. The results of analyzing the pectolinarin content of the gondre powder sample using HPLC-PDA are shown in FIG. 5 . The index component content of Gondree powder by condition showed the highest content of 11.07±0.05 and 10.95±0.15 mg/g in S-3 and S-4 powder, respectively, and coarsely pulverized Gondre S-1 powder (4.24±0.02 mg/g/g) g), the content of pectolinarin increased 2.58 to 3.83 times.
곤드레 pectolinarin 함량에 미치는 분말의 주요 입도분포를 확인하고자 500 mesh 이하(25 μm 이하), 270~500 mesh(25~53 μm), 170~270 mesh (53~90 μm) 및 100~170 mesh (90~150 μm) 입도별로 pectolinarin 함량을 분석한 결과, Table 5와 같이 500 mesh 이하(25 μm 이하)에서 pectolinarin이 가장 고함유(11.33±0.01 mg/Kg)되어 있었으며 270~500 mesh(25~53 μm)에서도 9.60±0.02 mg/Kg으로 나타나 조분쇄(S-1) 곤드레 분말에 비해 약 2배 정도의 pectolinarin 함량이 고함유되어 입도분포를 53 μm 이하로 곤드레 분말을 제조하면 pectolinarin 함량이 고함유 된 곤드레 분말을 제조가능 한 것으로 나타났다. 500 mesh or less (25 μm or less), 270-500 mesh (25-53 μm), 170-270 mesh (53-90 μm), and 100-170 mesh (90 As a result of analyzing the pectolinarin content by particle size (~150 μm), as shown in Table 5, the highest pectolinarin content (11.33±0.01 mg/Kg) was found at 500 mesh or less (25 μm or less), and 270~500 mesh (25~53 μm). ) also showed 9.60±0.02 mg/Kg, so the pectolinarin content was about twice as high as that of the coarsely ground (S-1) gondre powder. It was found that gondre powder could be prepared.
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이상의 결과로 고려해 볼 때, pectolinarin 고함유 곤드레 분말 제조조건은 S-3(3500 rpm 이상)으로 처리량은 10 Kg/hr의 조건으로 곤드레 미세분쇄/분급을 실시하면 조분쇄된 곤드레 분말에 비해 pectolinarin의 함량이 3.83배 이상 높은 곤드레 분말화가 가능하였다. Considering the above results, when the pectolinarin-rich gondre powder manufacturing condition was S-3 (3500 rpm or higher) and the treatment amount was 10 Kg/hr, the pectolinarin was reduced compared to the coarsely pulverized gondre powder. It was possible to powder gondre with a content of 3.83 times or more.
상기와 같은 실험결과로부터 아래와 같은 과제해결 수단이 제공된다.From the above experimental results, the following problem solving means are provided.
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곤드레 원료를 준비하는 원료준비(S1); 및Raw material preparation (S1) for preparing gondre raw materials; and
상기 곤드레 원료를 조분쇄하는 조분쇄단계(S2); 및a coarse grinding step of coarsely grinding the gondre raw material (S2); and
상기 조분쇄단계에서 조분쇄한 곤드레를 열풍 건조기로 60℃에서 8시간 건조하는 조분쇄 후 건조단계(S3); 및Drying step (S3) after coarse grinding of coarsely pulverized gondree in the coarse pulverization step and dried at 60° C. for 8 hours with a hot air dryer; and
상기 조분쇄 후 건조단계에서 건조한 건조물을 2,500 ~ 3,800 RPM으로 미세분쇄하여 입도분포 X90이 139 ~ 150㎛ 인 것을 특징으로 하는 펙토리나린 고함유 곤드레 분말 제조방법을 제공한다.After the coarse grinding, the dried material is finely pulverized at 2,500 to 3,800 RPM in the drying step to provide a method for producing pectinarin-rich gondre powder, characterized in that the particle size distribution X90 is 139 to 150 μm.
또한, 상기 펙토리나린 고함유 곤드레 분말 제조방법으로 제조된 곤드레분말 1g 당 펙토리나린이 10.24 ~ 11.07mg 함유된 것을 특징으로 하는 펙토리나린 고함유 곤드레 분말 제조방법을 제공한다.In addition, there is provided a method for producing a gondre powder with a high pectorinarin content, characterized in that 10.24 to 11.07 mg of pectorinarin is contained per 1 g of the gondre powder prepared by the method for producing a gondre powder with a high pectinarine content.
Claims (2)
상기 곤드레 원료를 조분쇄하는 조분쇄단계(S2); 및
상기 조분쇄단계에서 조분쇄한 곤드레를 열풍 건조기로 60℃에서 8시간 건조하는 조분쇄 후 건조단계(S3); 및
상기 조분쇄 후 건조단계에서 건조한 건조물을 3,500 ~ 3,800 RPM으로 미세분쇄하여 입도분포 X90이 139 ~ 150㎛ 이며,
상기 미세분쇄된 곤드레 분말은 1g 당 펙토리나린이 10.24 ~ 11.07 mg 함유된 것을 특징으로 하는 펙토리나린 고함유 곤드레 분말 제조방법.
Raw material preparation (S1) for preparing gondre raw materials; and
a coarse grinding step of coarsely grinding the gondre raw material (S2); and
Drying step (S3) after coarse grinding of coarsely pulverized gondree in the coarse pulverization step and dried at 60° C. for 8 hours with a hot air dryer; and
After the coarse grinding, the dried material in the drying step is finely pulverized at 3,500 to 3,800 RPM so that the particle size distribution X90 is 139 to 150㎛,
The method for producing a gondre powder with a high content of pectinarin, wherein the finely pulverized gondre powder contains 10.24 to 11.07 mg of pectorinarin per 1 g.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR20170087190A (en) * | 2016-01-20 | 2017-07-28 | 최근종 | SUNDAE Sausage Manufacturing Method |
| KR101894539B1 (en) | 2016-06-22 | 2018-09-05 | 주식회사 코씨드바이오팜 | Cosmetic composition with pectolinarin for skin anti-wrinkle and anti aging |
| KR20190005479A (en) * | 2017-07-07 | 2019-01-16 | 박대롱 | Cirsium setidens Nakai sheet and manufactring method thereof |
| KR20200035751A (en) | 2018-09-27 | 2020-04-06 | (주)세준에프앤비 | Retort Type Scorched Rice Having cirsium setidens extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR20170087190A (en) * | 2016-01-20 | 2017-07-28 | 최근종 | SUNDAE Sausage Manufacturing Method |
| KR101894539B1 (en) | 2016-06-22 | 2018-09-05 | 주식회사 코씨드바이오팜 | Cosmetic composition with pectolinarin for skin anti-wrinkle and anti aging |
| KR20190005479A (en) * | 2017-07-07 | 2019-01-16 | 박대롱 | Cirsium setidens Nakai sheet and manufactring method thereof |
| KR20200035751A (en) | 2018-09-27 | 2020-04-06 | (주)세준에프앤비 | Retort Type Scorched Rice Having cirsium setidens extract |
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