KR102364274B1 - 2-메틸알릴 알코올의 연속 제조 방법 - Google Patents

2-메틸알릴 알코올의 연속 제조 방법 Download PDF

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KR102364274B1
KR102364274B1 KR1020207010732A KR20207010732A KR102364274B1 KR 102364274 B1 KR102364274 B1 KR 102364274B1 KR 1020207010732 A KR1020207010732 A KR 1020207010732A KR 20207010732 A KR20207010732 A KR 20207010732A KR 102364274 B1 KR102364274 B1 KR 102364274B1
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South Korea
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reaction
sodium acetate
methylallyl
sodium
solution
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KR1020207010732A
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English (en)
Korean (ko)
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KR20200047716A (ko
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홍 인
즈롱 천
웨이송 왕
신롱 왕
성리 왕
이펑 진
난 동
홍쥔 가오
딩리엔 마
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저지앙 대학
저지앙 황마 테크놀로지 컴퍼니 리미티드
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Publication of KR20200047716A publication Critical patent/KR20200047716A/ko
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
    • C07C29/12—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of esters of mineral acids
    • C07C29/124—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of esters of mineral acids of halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C33/00—Unsaturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C33/02—Acyclic alcohols with carbon-to-carbon double bonds
    • C07C33/025—Acyclic alcohols with carbon-to-carbon double bonds with only one double bond
    • C07C33/03—Acyclic alcohols with carbon-to-carbon double bonds with only one double bond in beta-position, e.g. allyl alcohol, methallyl alcohol

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020207010732A 2017-12-22 2018-10-10 2-메틸알릴 알코올의 연속 제조 방법 KR102364274B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN201711400139.5A CN108191604B (zh) 2017-12-22 2017-12-22 一种连续制备2-甲基烯丙醇的方法
CN201711400139.5 2017-12-22
PCT/CN2018/109595 WO2019119934A1 (zh) 2017-12-22 2018-10-10 一种连续制备2-甲基烯丙醇的方法

Publications (2)

Publication Number Publication Date
KR20200047716A KR20200047716A (ko) 2020-05-07
KR102364274B1 true KR102364274B1 (ko) 2022-02-17

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JP (1) JP7029740B2 (ru)
KR (1) KR102364274B1 (ru)
CN (1) CN108191604B (ru)
RU (1) RU2734548C1 (ru)
WO (1) WO2019119934A1 (ru)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108191604B (zh) * 2017-12-22 2020-03-27 浙江大学 一种连续制备2-甲基烯丙醇的方法
CN111099990B (zh) * 2019-12-31 2023-12-26 山东广通新材料有限公司 长碳链二元羧酸精制结晶母液的回收利用方法
CN111170828B (zh) * 2020-01-17 2023-01-03 浙江大学宁波理工学院 利用原位生成Cu(I)催化剂制备甲基烯丙醇的方法
CN111499515A (zh) * 2020-04-28 2020-08-07 南京简迪环境工程有限公司 硝基氯苯连续水解合成硝基酚钠工艺
CN112546658A (zh) * 2020-11-13 2021-03-26 南通百川新材料有限公司 一种新型的2-甲氧基-1-丙醇乙酸酯脱酯精馏提纯方法
CN114015034A (zh) * 2021-12-08 2022-02-08 江苏奥克化学有限公司 用于合成减水剂聚醚的醇钠催化剂的制备方法与应用
CN114560752A (zh) * 2022-02-24 2022-05-31 浙江皇马科技股份有限公司 一种2-甲基烯丙醇的合成方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009107949A (ja) 2007-10-29 2009-05-21 Nippon Shokubai Co Ltd アリルアルコール化合物の製造方法
CN103242139B (zh) 2013-05-22 2015-07-01 南京工业大学 酯化水解两步法制备2-甲基烯丙基醇的方法
CN105037097A (zh) 2015-06-23 2015-11-11 浙江绿科安化学有限公司 一种2-甲基烯丙醇的合成方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4810765B1 (ru) * 1969-08-14 1973-04-07
JPS5210296A (en) * 1975-07-15 1977-01-26 Kohjin Co Ltd A process for preparing 6,2'-cyclo-5- substituted isocytidines
KR100676304B1 (ko) * 2004-12-24 2007-01-30 주식회사 엘지화학 네오펜틸글리콜의 제조방법
CN104341255B (zh) * 2014-09-19 2016-08-24 江苏苏博特新材料股份有限公司 一种不饱和醇的制备方法
CN108191604B (zh) * 2017-12-22 2020-03-27 浙江大学 一种连续制备2-甲基烯丙醇的方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009107949A (ja) 2007-10-29 2009-05-21 Nippon Shokubai Co Ltd アリルアルコール化合物の製造方法
CN103242139B (zh) 2013-05-22 2015-07-01 南京工业大学 酯化水解两步法制备2-甲基烯丙基醇的方法
CN105037097A (zh) 2015-06-23 2015-11-11 浙江绿科安化学有限公司 一种2-甲基烯丙醇的合成方法

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Publication number Publication date
CN108191604B (zh) 2020-03-27
KR20200047716A (ko) 2020-05-07
RU2734548C1 (ru) 2020-10-20
CN108191604A (zh) 2018-06-22
JP7029740B2 (ja) 2022-03-04
JP2021506981A (ja) 2021-02-22
WO2019119934A1 (zh) 2019-06-27

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