KR102265426B1 - Manufacturing Method of Cosmetic Composition Comprising Hot Spring Water and Cosmetic Composition Comprising thereof - Google Patents

Abstract

The present invention relates to a method for manufacturing a cosmetic composition comprising hot spring water, and the cosmetic composition comprising hot spring water. The cosmetic composition comprises 60 to 70 wt% of purified water, 3 to 7 wt% of butylene glycol, 3 to 7 wt% of glycerin, 0.01 to 0.1 wt% of disodium EDTA, 0.1 to 0.5 wt% of citric acid, 0.1 to 0.5 wt% of sodium citrate, 1 to 5 wt% of a Centella asiatica leaf extract, 1 to 5 wt% of a Hamamelis virginiana extract, 1 to 5 wt% of a green tea extract, 0.01 to 0.1 wt% of arginine, 0.01 to 0.1 wt% of hydroxyacetophenone, 1 to 5 wt% of 1,2-hexanediol, and 15 to 25 wt% of hot spring water. The cosmetic composition not only has an excellent skin moisturizing effect by including hot spring water, but also has an excellent skin trouble reducing effect by including the Centella asiatica leaf extract, the Hamamelis virginiana extract, and the green tea extract.

Description

The manufacturing method of a cosmetic composition comprising hot spring water and a cosmetic composition comprising hot spring water {Manufacturing Method of Cosmetic Composition Comprising Hot Spring Water and Cosmetic Composition Comprising thereof}

The present invention relates to a method for producing a cosmetic composition comprising hot spring water and a cosmetic composition comprising hot spring water, and more particularly, to a cosmetic composition comprising hot spring water having excellent skin moisturizing effect and whitening effect as well as skin trouble improvement effect It relates to a cosmetic composition comprising a method and hot spring water.

Hot springs are springs in which groundwater is heated to above average temperature by geothermal heat and leached to the surface. In Korea, hot springs are defined as hot springs that are not harmful to the human body at 25℃ or higher. 1981.6.18, Presidential Decree No. 10354)]. Hot spring, in the broad sense of hot springs, is defined as water that comes out from the ground to the surface of natural water, which is physically and chemically different from normal water. A spring that is lower than the water temperature of the groundwater is called a cold spring, and a spring that contains a large amount of inorganic substances or gas components regardless of the water temperature is called a mineral spring. According to this definition, the threshold temperature of a hot spring varies from region to region. In Korea, based on 25℃, cold spring below 25℃, mild hot spring at 25~34℃, hot spring at 34~42℃, and hot spring above 42℃. The classification of hot springs differs according to scholars and countries, but in general, they are divided according to temperature, the type of elution of the hot spring, liquid ion concentration, the solubility of minerals, and the development status of the hot spring.

In Korea, there are about 200 hot springs, and most of them are developed for hot spring baths, and although the development of products using hot springs is insufficient, currently 8 domestic hot springs have been designated as health care hot springs, and bio-products using them are being developed steadily.

Korean Patent Publication No. 10-1854409 (May 13, 2018) discloses a cosmetic composition for moisturizing the skin containing hot spring water.

The cosmetic composition for moisturizing the skin contains a lysate of hot spring water powder prepared by freeze-drying hot spring water, and has an excellent skin moisturizing effect, but has a disadvantage in that the skin trouble improvement effect is poor.

KR 10-1854409 B1 2018.05.13.

An object of the present invention is to provide a method for preparing a cosmetic composition containing hot spring water having excellent moisturizing effect on the skin and a cosmetic composition containing hot spring water.

Another object of the present invention is to provide a method for preparing a cosmetic composition comprising hot spring water having excellent skin whitening effect and skin trouble improvement effect, and a cosmetic composition comprising hot spring water.

In order to achieve the above object, the present invention provides the following means.

The present invention comprises the steps of preparing a Centella asiatica leaf extract, a Virginia fungus extract and a green tea extract (step 1); and 60 to 70 wt% of purified water, 3 to 7 wt% of Butylene Glycol, 3 to 7 wt% of Glycerin, 0.01 to 0.1 wt% of Disodium EDTA, and citric acid (Citric Acid) 0.1 to 0.5% by weight, Sodium Citrate 0.1 to 0.5% by weight, the Centella asiatica extract 1 to 5% by weight, the Virginia Peony extract 1 to 5% by weight, the green tea extract 1 to 5% by weight %, Arginine 0.01~0.1 wt%, Hydroxyacetophenone 0.01~0.1 wt%, 1,2-hexanediol (1,2-Hexanediol) 1~5 wt%, and hot spring water 15~25 preparing a cosmetic composition containing hot spring water by stirring the wt% at 20 rpm for 10 to 40 minutes (step 2); It provides a method for producing a cosmetic composition comprising hot spring water, including.

In step 1, the Centella asiatica extract is added to 100 parts by weight of Centella asiatica leaves by weight 600 to 700 parts by weight of magnetized water, extracted at 100 to 105° C. for 5 to 6 hours, and then filtered, and the Virginia Peony extract is bio 600~700 parts by weight of purified ceramic stone water is added, extracted at 95~100° C. for 1~2 hours, and filtered, and the purified bioceramic stone water is 6~10 parts by weight of bioceramic stone added to 100 parts by weight of water and left for 6~8 hours The bioceramic stone is prepared by adding a mixture containing 60 to 70% by weight of pearlite, 15 to 25% by weight of sericite, and 10 to 20% by weight of ocher in water, kneading it, and then aging it at 1,100 to 1,200 ° C. It is calcined at a temperature for 3 to 4 hours, and the green tea extract is filtered after adding 600 to 700 parts by weight of plasma treated water to 100 parts by weight of green tea and extracting it at 105 to 110° C. for 8 to 9 hours.

In addition, the present invention, purified water 60 to 70% by weight, butylene glycol (Butylene Glycol) 3 to 7% by weight, glycerin (Glycerin) 3 to 7% by weight, disodium EDTA (Disodium EDTA) 0.01 to 0.1 weight %, Citric Acid 0.1 to 0.5% by weight, Sodium Citrate 0.1 to 0.5% by weight, The Centella asiatica extract 1 to 5% by weight, The Virginia Peony extract 1 to 5% by weight, The green tea Extract 1-5 wt%, Arginine 0.01-0.1 wt%, Hydroxyacetophenone 0.01-0.1 wt%, 1,2-Hexanediol 1-5 wt% And it provides a cosmetic composition comprising hot spring water, including 15 to 25% by weight of hot spring water.

1 to 5 parts by weight of a skin trouble improvement improver is additionally included in 100 parts by weight of the cosmetic composition containing the hot spring water, and the epithelial skin trouble improvement enhancer includes 55 to 65 wt% of fermented oleracea extract, 20 to 30 wt% of fermented extract and Contains 10 to 20% by weight of mung bean extract and fermented product, and the fermented mung bean extract is put 600-700 parts by weight of purified water in 100 parts by weight of oleracea, extracted at 100-105° C. for 8-10 hours, and 100 parts by weight of extract Add 2-4 parts by weight of the first mixed bacteria and ferment for 24 to 25 hours at 25-30 ℃, the first mixed bacteria is Bacillus natto in 60-70% by weight, yeast 20-30% by weight, and yeast 5-15 Including weight %, the fermented jeoryeong extract is put into 100 parts by weight of jeoryeong 70% (v/v) ethanol 600-700 parts by weight and extracted at 65-70° C. for 24-25 hours, and 100 parts by weight of jeoryeong extract. Add 1-3 parts by weight of the second mixed bacteria and ferment for 14-15 hours at 15-20 ° C. The second mixed bacteria is 60-70% by weight of lactic acid bacteria, 20-30% by weight of Hongguk bacteria and 5-15% by weight of Bacillus subtilis. Including, the fermented mung bean extract is added 300-400 parts by weight of 80% (v/v) ethanol to 100 parts by weight of mung bean, followed by ultrasonic extraction for 14 to 16 hours, and 1-3 parts by weight of Hwangguk-gyun to 100 parts by weight of the mung bean extract and fermented at 15-20°C for 30-32 hours.

1 to 5 parts by weight of a whitening effect enhancer is additionally included in 100 parts by weight of the cosmetic composition containing the hot spring water, wherein the whitening effect enhancer is 55 to 65% by weight of fermented rice bran extract, 20 to 30% by weight of fermented bamboo shoot extract, and 300% by weight extract It contains 10 to 20% by weight, and the fermented rice bran extract is refluxed by adding 700 to 800 parts by weight of 90% (v/v) ethanol to 100 parts by weight of rice bran, and 1-3 parts by weight of white chrysanthemum to 100 parts by weight of rice bran extract. It is prepared by adding parts and fermenting at 26-30 ° C. for 24 to 25 hours, and the fermented bamboo shoot extract is put into 100 parts by weight of bamboo shoots 500 to 600 parts by weight of purified water and hot water extraction at 105 to 110 ° C. for 3-4 hours, It is prepared by adding 1 to 3 parts by weight of photosynthetic bacteria to 100 parts by weight of the bamboo shoot extract and fermenting it for 14 to 15 hours at 20 to 25 ° C. The extract is made by adding 400 to 500 parts by weight of propylene glycol to 100 parts by weight of 300 seconds and 50 to 55 It is prepared by extraction at ℃ for 4~5 hours, filtering, and aging at 31~33℃ for 2-3 days.

The cosmetic composition containing the hot spring water according to the present invention has the effect of preventing roughness of the skin and refining the texture, has an effect of providing moisture and softening the skin by supplying and controlling moisture to the skin, protecting the skin and helping to improve the skin tone It has the effect of helping to whiten the skin.

The cosmetic composition comprising hot spring water according to the present invention has excellent skin moisturizing effect by including hot spring water, as well as excellent skin trouble improvement effect by including Centella asiatica leaf extract, Hamamelis virginiana extract, and green tea extract.

The cosmetic composition comprising the hot spring water according to the present invention has an advantage in improving skin troubles by using magnetized water, bioceramic stone purified water, and plasma treated water when preparing Centella asiatica leaf extract, Hamamelis virginiana extract and green tea extract. .

Hereinafter, the present invention will be described in detail.

First, a method for preparing a cosmetic composition containing hot spring water according to the present invention will be described.

The manufacturing method of the cosmetic composition comprising the hot spring water of the present invention,

A step of preparing a Centella asiatica leaf extract, a Virginia Peony extract and a green tea extract (step 1); and

Purified water 60-70% by weight, Butylene Glycol 3-7% by weight, Glycerin 3-7% by weight, Disodium EDTA 0.01-0.1% by weight, citric acid ( Citric Acid) 0.1 to 0.5% by weight, Sodium Citrate 0.1 to 0.5% by weight, the Centella asiatica extract 1 to 5% by weight, the Virginia Peony extract 1 to 5% by weight, The green tea extract 1 to 5% by weight , Arginine 0.01 to 0.1% by weight, Hydroxyacetophenone 0.01 to 0.1% by weight, 1,2-Hexanediol 1 to 5% by weight, and hot spring water 15 to 25% by weight % was stirred at 20 rpm for 10 to 40 minutes to prepare a cosmetic composition containing hot spring water (step 2);

includes

The present invention has an advantage in that it has excellent skin moisturizing effect by including hot spring water, as well as excellent skin trouble improvement effect by including Centella asiatica leaf extract, Hamamelis virginiana extract, and green tea extract.

In step 1, the Centella asiatica leaf extract is filtered after adding 600 to 700 parts by weight of magnetized water to 100 parts by weight of Centella asiatica leaf and extracting it at 100 to 105° C. for 5 to 6 hours.

The magnetized water refers to water obtained by converting a pentagonal number, which is a typical structure of water, into a hexagonal number form by using a strong magnet such as a neodymium magnet.

The molecular structure of water consists of one oxygen atom of a - ion and two hydrogen atoms of a + ion bonded to each other. volume increases

In the hexagonal structured magnetized water, no bacteria can absorb the oxygen in the water molecule, and 6 times more hydrogen atoms of + ions and oxygen atoms of - ions are inevitably held in the process of bonding with each other compared to normal water. Because of the magnetic energy of about 0.5 Gauss, it is difficult for bacteria to survive due to various restrictions, and even if they do survive, they cannot reproduce and eventually disappear.

The centella asiatica is [scientific name] Centella asiatica [INCI name] Centella Asiatica Leaf Extract, originating in the tropics of the Indian Ocean, and growing ideally at an altitude of 600 meters in a humid and shady area. It is a perennial plant commonly found in the mountains and fields of the southern islands of the Korean Peninsula. it is grass The main stem extends laterally, and there are two degenerated scaly leaves near the root node. Leaves are dense at nodes, elongate, 2-5cm in diameter, glossy on the surface, with dull serrated edges, and the length of petiole is 4-20cm. Flowers are reddish-purple, hung in umbels by 3-4 in leaf axils, and are shaped like a head. The style is bifurcated, and the fruit is a segmental oblong shape. Centella asiatica is also called Gotu Kola, Indian Pennywort or Tiger Grass (which Bengal tigers used to roll and eat on the grass to heal their wounds). Although it was only listed in the French Codex in 1884, it has been used as a traditional medicine since 3,000 years ago in eastern India, American Indians, China, and Indonesia. Since Dry Extract was first produced in 1941, its efficacy against diseases such as skin damage and wounds, burns, ulcers, leprosy, seborrheic dermatitis of the scalp, hypertrophic scars, and cellulitis has been revealed through numerous studies. The ingredients of the folding screen include asiatic acid, madecassic acid, and asiaticoside. Centella asiatica contains antioxidants, suppresses inflammation, promotes collagen synthesis in the skin, and inhibits cellulite production, so it has the effect of alleviating stretch marks.

In step 1, Virginia perennial plant extract is filtered after adding 600 to 700 parts by weight of purified bioceramic stone water to 100 parts by weight of Virginia perennial plant and extracting it at 95 to 100° C. for 1 to 2 hours.

The bioceramic stone purified water is prepared by adding 6-10 parts by weight of bioceramic stone to 100 parts by weight of water and leaving it for 6-8 hours.

The bioceramic stone is a mixture containing 60 to 70% by weight of pearlite, 15 to 25% by weight of sericite, and 10 to 20% by weight of loess in water, kneaded and aged, and then 3 to at a temperature of 1,100 to 1,200 ° C. Firing for 4 hours.

The Virginia perennial flower ( Hamamelis virginiana ) contains a large amount of tannins with drying and astringent effects. The Virginia perennial plant ( Hamamelis virginiana ) forms a protective layer that enhances the anti-inflammatory function and promotes the recovery of damaged skin by strengthening the skin and converging proteins on the damaged surface of the skin.

In step 1, the green tea extract is filtered after adding 600 to 700 parts by weight of plasma treated water to 100 parts by weight of green tea and extracting it at 105 to 110° C. for 8 to 9 hours.

The plasma-treated water is prepared by irradiating plasma directly to purified water.

Plasma contains various ions, electrons, free radicals, neutral particles, photons, etc., and is effective in the treatment of wounds, blood clots, sterilization, and oral diseases.

Plasma discharge unit is disposed at a point spaced apart from the surface of purified water, and plasma is irradiated to the purified water by electric discharge, and at this time, it is preferable to provide a means for preventing evaporation of purified water. Plasma treatment time may be 35 to 40 minutes.

The green tea uses the leaves of the tea tree ( Camellia sinensis ), and the tea tree is one of 82 species classified in the genus Camellia and is currently cultivated in more than 50 countries, such as Africa, South America, and Oceania, mainly in Asia. As one of the plants with proven excellent antioxidant power among natural functional substances, it contains a number of active ingredients including catechin, a polyphenolic compound. It is known to have the ability to remove free radicals.

The present invention has the advantage that the skin trouble improvement effect is more excellent by using magnetized water, bioceramic stone purified water and plasma treated water in the preparation of Centella asiatica leaf extract, Virginia Peony ( Hamamelis virginiana ) extract and green tea extract.

Next, a cosmetic composition comprising hot spring water according to the present invention will be described.

A cosmetic composition comprising hot spring water according to the present invention,

Purified water 60-70% by weight, Butylene Glycol 3-7% by weight, Glycerin 3-7% by weight, Disodium EDTA 0.01-0.1% by weight, citric acid ( Citric Acid) 0.1 to 0.5% by weight, Sodium Citrate 0.1 to 0.5% by weight, the Centella asiatica extract 1 to 5% by weight, the Virginia Peony extract 1 to 5% by weight, The green tea extract 1 to 5% by weight , Arginine 0.01 to 0.1% by weight, Hydroxyacetophenone 0.01 to 0.1% by weight, 1,2-Hexanediol 1 to 5% by weight, and hot spring water 15 to 25% by weight Including %.

When the content of each component satisfies the above numerical range, the cosmetic composition is effective in preventing roughness of the skin and refining the texture, providing moisture and suppleness by supplying and controlling moisture to the skin, protecting the skin and improving skin tone It is excellent in helping effect and helping to whiten skin.

The butylene glycol is used as an organic solvent.

The glycerin is a humectant containing an oil and fat component, and serves to supply moisture to the skin by absorbing moisture in the air, and is added to moisturize dry skin to make it shiny. In addition, the glycerin has a skin conditioning effect that enhances the vitality of the skin, suppresses the growth of anaerobic bacteria, and exhibits a deodorizing effect.

The disodium EDTA serves as a stabilizer for each component to perform its role, and in particular, also serves as a purifying agent to prevent the propagation of microorganisms or the generation of lead or heavy metals.

The citric acid is used as a pH adjuster.

The sodium citrate is used as a pH adjuster.

The arginine (Arginine) is an alkaline essential amino acid present in nature, and it can improve the regeneration effect of skin aging prevention and wound healing, etc., and act on the skin to promote collagen synthesis.

The hydroxyacetophenone is included as a preservative.

The 1,2-hexanediol is included as a preservative.

The cosmetic composition containing the hot spring water of the present invention is not particularly limited in its formulation, and may be, for example, a lotion formulation, but is not limited thereto.

The cosmetic composition containing the hot spring water according to the present invention has the effect of preventing roughness of the skin and refining the texture, has an effect of providing moisture and softening the skin by supplying and controlling moisture to the skin, protecting the skin and helping to improve the skin tone It has the effect of helping to whiten the skin.

The cosmetic composition comprising hot spring water according to the present invention has excellent skin moisturizing effect by including hot spring water, as well as excellent skin trouble improvement effect by including Centella asiatica leaf extract, Hamamelis virginiana extract, and green tea extract.

The cosmetic composition comprising the hot spring water according to the present invention has an advantage in improving skin troubles by using magnetized water, bioceramic stone purified water, and plasma treated water when preparing Centella asiatica leaf extract, Hamamelis virginiana extract and green tea extract. .

In the present invention, 1 to 5 parts by weight of a skin trouble improving agent may be additionally included in 100 parts by weight of the cosmetic composition including the hot spring water.

The skin trouble improving agent includes 55 to 65% by weight of fermented extract of oleracea extract, 20 to 30% by weight of fermented extract of jeolin, and 10 to 20% by weight of fermented green bean extract.

The ogapi is an herbal remedy, analgesic and antispasmodic, heals pungsaengjeung, energizes, and strengthens tendons and bones. In the ogapi, eleutheroside B inhibits inflammatory COX, and drug molecules of the diterpene system also act in this way. Also, just as steroid hormones _{inhibit PLA 2} , steroidal substances such as β-citosterol also have this function to protect the release of acachidonic acid from cell membrane phospholipids.

The extract and fermented sagebrush extract is put 600-700 parts by weight of purified water into 100 parts by weight of scorpion spp., extracted at 100-105° C. for 8-10 hours, and 2-4 parts by weight of the first mixed bacteria is added to 100 parts by weight of sorghum extract, and 25- Fermentation at 30°C for 24 to 25 hours.

The first mixed bacteria includes 60 to 70% by weight of Bacillus natto, 20 to 30% by weight of yeast, and 5 to 15% by weight of yeast.

The bacilli present in natto straw bacteria (Bacillus natto) is attached to the approximately 10 million at a straw bundle, and the size of the bacteria has a length 2.33 microns, a width of 1 micron and has a property to form spores for the preservation of the species .

Wherein the yeast is made to my process Lucy (Saccharomyces rouxii), three Levy cyano as Saccharomyces My process as Saccharomyces (Saccharomyces cereviciae), my process Ob pole miss in Saccharomyces (Saccharomyces oviformis) and My process stay Neri (Saccharomyces steineri) in Saccharomyces Any one selected from the group may be used.

The yeast may use any one selected from the group consisting of Aspergillus oryzae (Aspergillus oryzae) and Aspergillus sojae (Aspergillus sojae).

The jeoryeong ( Polyporus umbellatus ) is also called by other names such as juryeong, siryung, jeosiryeong, jiodo, huiryeong, and gajeoshi, and is a mushroom belonging to the basidiomycete Minus umbellatus family, especially in broadleaf forests in autumn. It is parasitic on the mountain roots of alder, oak, maple, or oak tree, and its temper is sweet and bitter. It is mainly distributed in Korea, Japan, Europe, China, and the United States. The stem is split several times at the base, and the cap blooms at the end of each branch. The height is 10-20 cm and the diameter is 10-30 cm. The sclerotia are irregular masses, many of which are similar to ginger, and the surface has an unusual shape and is yellowish white or weasel color. It resembles pig feces, hence the name 'Joryeong'. The fruiting body consists of a complicatedly branched stalk and cap. It is an irregular long mass or a mass that is close to round, and the size is not uniform. The long ones are usually curved or cracked like ginger and are 5~25cm long. The surface is black or blackish-brown, and there is a protrusion of a lump. It is light and tough, and the cross section is milky white or yellowish white. Jeolyeong has the effect of facilitating water metabolism. It is used when you cannot urinate well or there is edema in the body. It is good for symptoms such as swelling of the legs due to difficulty urinating during pregnancy, and diarrhea due to weak digestion. .

The fermented extract of jeolyeong is put into 100 parts by weight of jeoryeong 70% (v/v) ethanol 600-700 parts by weight and extracted at 65-70° C. for 24-25 hours, and the second mixed bacteria 1 to 100 parts by weight of jeoryeong extract. Add 3 parts by weight and ferment at 15-20° C. for 14-15 hours.

The second mixed bacteria includes 60 to 70% by weight of lactic acid bacteria, 20 to 30% by weight of Hongguk bacteria and 5 to 15% by weight of Bacillus subtilis.

The lactic acid bacteria are Lactobacillus delbrueckii ( Lactobacillus delbrueckii ), Lactobacillus bulgaricus ( Lactobacillus bulgaricus ), Lactobacillus casei ( Lactobacillus casei ), Lactobacillus acidophil ( Lactobacillus brevis ), Lactobacillus acidophilus ( Lactobacillus brevis ), Lactobacillus brevis ) Ococcus pentosaceus ( Pediococcus pentosaceus ), Pediococcus cerevisiae ), Lactococcus lactis ( Lactococcus lactis ), Leuconostoc citreum ( Leuconostoc citreum ), Leuconostoc mesenteroid ( Leuconostoc mesenteroid ) Bifidobacterium bifidum ( Bifidobacterium bifidum ) and Lactobacillus rhamnosus ( Lactobacillus rhamnosus ) Any one selected from the group consisting of may be used.

The Hong Guk-gyun is a red filamentous fungus belonging to the genus Ascomycetes Monascus, and produces dark red pigment and monacolin K as various beneficial metabolites in the process of fermenting grains such as rice. This fungus has been used for a long time as a natural food coloring agent or processed product, as well as a material for promoting digestion and improving blood flow in various regions of East Asia, including China. Mebinoline, a secondary metabolite produced by Hong Guk-gyun, strongly inhibits HMG-CoA (3-hydroxy-methyl-3-glutaryl-coenzyme) reductase, a cholesterol biosynthetic enzyme, thereby reducing blood lipid concentration and inhibiting cholesterol synthesis. It has various functions such as antifungal, suppression of blood sugar rise, blood pressure control, anti-obesity, and anti-cancer. In addition, Hong Guk-gyun produces red pigments (rubropuntain, monascorubin), yellow pigments (monascin, ankaflavin), purple pigments (rubropunctamine, monascorubramine), and the like, and these pigment substances have antibacterial and anticancer effects.

The Hong Guk-gyun is Monascus pilosus ( Monascus pilosus ), Monascus rubber ( Monascus ruber ), Monascus purpureus ), Monascus kaoliang ( Monascus kaoliang ), Monascus barykery ) Any one selected from the group consisting of Monascus anka may be used.

The Bacillus subtilis ( B. subtilis ), Bacillus lichneformis ( B. lichneformis ), Bacillus megaterium ( B. megaterium ), Bacillus amyloliquefaciens ( B. amyloliquefaciens ), Bacillus natto ( B . natto), Bacillus la Alliance system (B.antharcis), Bacillus alkylene tooth (B.lentus), Bacillus mirror's buffer (B.pumilus), Bacillus rendering if N-Sys (B.thuringiensis), Bacillus al bay (B.alvei ), Bacillus azo topic Sans (B.azotofixans), Bacillus maese lance (B.macerans), Bacillus Poly miksa (B.polymyxa), Bacillus papil Rie (B.popilliae), Bacillus core posts lance (B.coagulans), Bacillus Stearothermophilus ( B. stearothermophilus ), Bacillus pasteurii ( B.pasteurii ), Bacillus paricus ( B.sphaericus ) and Bacillus pastidiosus ( B.fastidiosus ) Any one selected from the group consisting of may be used.

The mung bean ( Phaseolous radiatus , Mung bean) is also called andu or gildu, and is a seed of mung bean of the legume family. It grows well in loam (black soil with a suitable mixture of sand and clay) in a warm climate, and the height is 30-80 cm. . The stem is thin and has vertical veins, has about 10 nodes, and branches. A pair of cotyledons and newly formed leaves come out, followed by a compound leaf consisting of three small leaves. These mung beans have been used in oriental medicine as a skin disease treatment, antipyretic and antidote, and in Donguibogam, it has been known that mung bean powder can be used to obtain cosmetic effects when applied to the face.

The mung bean extract and fermented product is obtained by adding 300 to 400 parts by weight of 80% (v/v) ethanol to 100 parts by weight of mung bean, followed by ultrasonic extraction for 14 to 16 hours, and adding 1 to 3 parts by weight of Hwangguk bacteria to 100 parts by weight of the mung bean extract and 15 to 20 parts by weight. Fermented at ℃ for 30-32 hours.

The Hwanggukgyun is a kind of bacteria that have been attached to some native bacteria during the manufacture of Korean traditional soybean, but has been isolated and purely used for the manufacture of high-fat materials such as soybean paste, soy sauce, and Cheongju in Japan since early days.

In the present invention, 1 to 5 parts by weight of a whitening effect enhancer may be additionally included in 100 parts by weight of the cosmetic composition including the hot spring water.

The whitening effect enhancer includes 55 to 65% by weight of fermented rice bran extract, 20 to 30% by weight of fermented bamboo shoot extract, and 10 to 20% by weight of extract of ginseng plant.

The rice bran refers to the inner hull powder consisting of rice bran and rice bran generated in the process of polishing from brown rice to white rice. When the nutritional content of rice is analyzed, it contains 29% of the rice bran, 66% of the rice bran, and 5% of the rice called white rice. Because of this distribution, 95% of the nutrients of rice are in the rice bran composed of rice bran and rice bran. Rice bran is known to have several functions, and it has various functions, such as removing sukbun by activating peristaltic movement of the intestines, reducing cholesterol and triglycerides, healing high blood pressure, arteriosclerosis, and improving concentration and memory by activating brain cell functions. It has an effect on the human body.

The rice bran extract and fermented product is extracted by refluxing 700 to 800 parts by weight of 90% (v/v) ethanol to 100 parts by weight of rice bran, and 1-3 parts by weight of white chrysanthemum bacteria are added to 100 parts by weight of rice bran extract, and 24 at 26-30 ° C. It is prepared by fermentation for ~25 hours.

The Baekgukgyun is a strain in which the conidia of Heukgukgyun, which is a strain that produces a large amount of citric acid, oxalic acid, glucolic acid, and the like, from sugar are changed from black to white.

The bamboo shoot (Phyllostachys spp.) is a plant belonging to the bamboo family (bambuseae) of the Grape family, and is a young and tender shoot of bamboo surrounded by bamboo skin. Generally, when it grows to a height of 20-30cm, it is harvested and used for food. Bamboo shoots are low in fat and cholesterol, but high in protein, carbohydrate, and fiber, as well as vitamins A, B1, B2, C, fructose, glucose, and other sugars, essential amino acids, fiber, potassium, calcium, iron, phosphorus and It contains many of the same minerals. Carbohydrates of bamboo shoots are decomposed into hemicellulose to produce enzymes that promote metabolism, and choline is the main component of lecithin, which removes toxicity, prevents fatty liver, asparagine, lysine ( lysine), methionine, glutamine, glycine, etc. play an important role in nutrition and flavor. Fiber relieves hypertension and constipation diuresis, promotes intestinal motility and suppresses cholesterol levels, bamboo shoots of minerals are known to be effective in preventing adult diseases. According to Donguibogam, bamboo shoots are reported to be effective in preventing constipation, clearing heat, blood cleansing, hangover relief, and diuresis, and are also used as herbal ingredients, and pharmacological effects such as antioxidant, anticancer, diabetes, and obesity have been reported. In addition, the anti-inflammatory effect of bamboo shoots has recently been reported.

The fermented bamboo shoot extract is put into 100 parts by weight of bamboo shoots, 500 to 600 parts by weight of purified water, hot water extraction at 105 to 110° C. for 3 to 4 hours, and 1 to 3 parts by weight of photosynthetic bacteria are added to 100 parts by weight of the bamboo shoot extract and 20 to 25 It is prepared by fermentation at ℃ for 14 to 15 hours.

The photosynthetic bacteria are important microorganisms that form group 1 in the plant circulation circuit of the natural world. The photosynthetic bacteria exist at a level of 1,000 to 10,000 individuals/cc in the ocean, soil, rivers, lakes, etc., and play an important role in the purification of the natural world. Microorganisms that contain chlorophyll and can assimilate themselves.

The photosynthetic bacteria may use any one selected from the group consisting of Rhodopseudomonas capsulata, Rhodopseudomonas sphaeroides, and Rhodospirillum rubrum.

The triticale ( Saururus chinensis ) is a kind of dicotyledonous perennial herb of the order Pepperaceae tricotyl. The rhizome is white and extends laterally in the mud. The height of the stem is 50~100cm, and white flowers bloom in June~August. It grows mainly in wetlands, and is called trifolieae because its roots, leaves, and flowers are white. It is known to be effective for beriberi, jaundice, and hepatitis, and is distributed in Korea, Japan, and China.

The 300 seconds extract is prepared by adding 400 to 500 parts by weight of propylene glycol to 100 parts by weight of 300 seconds, extracting at 50 to 55° C. for 4 to 5 hours, filtering, and then aging at 31 to 33° C. for 2-3 days.

Hereinafter, the configuration and effects of the present invention will be described in more detail through examples. These examples are only for illustrating the present invention, and the scope of the present invention is not limited by these examples.

Purified water 64.66 wt%, Butylene Glycol 5 wt%, Glycerin 5 wt%, Disodium EDTA 0.04 wt%, Citric Acid 0.1 wt%, Sodium Citrate (Sodium Citrate) 0.1% by weight, Centella asiatica leaf extract 1% by weight, Virginia chrysanthemum extract 1% by weight, green tea extract 1% by weight, Arginine 0.05% by weight, Hydroxyacetophenone 0.05% by weight, A cosmetic composition containing hot spring water was prepared by stirring 2 wt% of 1,2-hexanediol (1,2-Hexanediol) and 20 wt% of hot spring water at 20 rpm for 40 minutes. The Centella asiatica leaf extract was prepared by adding 700 parts by weight of magnetized water to 100 parts by weight of Centella asiatica leaf, extracting at 100° C. for 6 hours, and then filtration. The Virginia perennial flower extract was prepared by adding 700 parts by weight of purified bioceramic stone water to 100 parts by weight of Virginia perennial flower, extracting at 95° C. for 2 hours, and then filtering. The bioceramic stone purified water was prepared by adding 10 parts by weight of bioceramic stone to 100 parts by weight of water and leaving it to stand for 8 hours. The bioceramic stone was prepared by mixing a mixture containing 65% by weight of pearlite, 20% by weight of sericite, and 15% by weight of loess in water, kneading it, and then calcining at a temperature of 1,200° C. for 4 hours. The green tea extract was prepared by adding 700 parts by weight of plasma-treated water to 100 parts by weight of green tea, extracting at 105° C. for 9 hours, and then filtering.

In Example 1, 5 parts by weight of a skin trouble improving agent was additionally included in 100 parts by weight of the cosmetic composition including the hot spring water. The epithelial skin trouble improvement agent was prepared by mixing 60% by weight of fermented oleracea extract, 25% by weight of fermented extract of jeolyeong, and 15% by weight of fermented mung bean extract. The fermented sagebrush extract was prepared by adding 700 parts by weight of purified water to 100 parts by weight of scorpion aphids, and adding 4 parts by weight of the first mixed bacteria to 100 parts by weight of the scorpion extract extracted at 105° C. for 10 hours, and fermenting at 25° C. for 24 hours. The first mixed bacteria was prepared by mixing 65% by weight of Bacillus natto, 25% by weight of yeast, and 10% by weight of yeast. The yeast Saccharomyces rouxii was used, and the yeast was used as the Aspergillus oryzae (Aspergillus oryzae). The fermented extract of jeolyeong is added 3 parts by weight of the second mixed bacteria to 100 parts by weight of 70% (v/v) ethanol and 700 parts by weight of 70% (v/v) ethanol to 100 parts by weight of jeoryeong, and 3 parts by weight of the second mixed bacteria is added to 100 parts by weight of the jeoryeong extract extracted for 24 hours at 70 ℃ It was prepared by fermentation. The second mixed bacteria was prepared by mixing 65% by weight of lactic acid bacteria, 25% by weight of Hongguk bacteria and 10% by weight of Bacillus subtilis. The lactic acid bacteria was Lactobacillus delbrueckii ( Lactobacillus delbrueckii ) was used, the Hong Guk bacteria was Monascus pilosus ( Monascus pilosus ) was used, the Bacillus subtilis ( B. subtilis ) was used. The fermented mung bean extract was prepared by adding 400 parts by weight of 80% (v/v) ethanol to 100 parts by weight of mung bean, adding 3 parts by weight of Hwangguk bacterium to 100 parts by weight of the mung bean extract ultrasonically extracted for 16 hours, and fermenting at 20° C. for 30 hours.

[Comparative Example 1]

A cosmetic composition containing hot spring water was prepared in the same manner as in Example 1, except that purified water was used instead of magnetized water, bioceramic stone purified water, and plasma treated water when preparing the Centella asiatica leaf extract, Virginia Peony extract and green tea extract.

[Comparative Example 2]

A cosmetic composition was prepared in the same manner as in Example 1, except that distilled water was used instead of hot spring water.

[Experimental Example 1]

Forty women were divided into 4 groups of 10 each, and skin irritation was induced through tape stripping. The cosmetic compositions containing the hot spring water of Examples 1 and 2 and the cosmetic compositions of Comparative Examples 1 and 2 were applied twice daily in the morning and in the afternoon, and the degree of recovery of skin damage was observed. The results are shown in Table 1 below.

skin damage recovery time Example 1 3.9 days Example 2 3.1 days Comparative Example 1 4.9 days Comparative Example 2 6.2 days

Referring to Table 1, it can be seen that the cosmetic composition containing the hot spring water of Examples 1 and 2 significantly shortens the recovery time of skin damage compared to the cosmetic compositions of Comparative Examples 1 and 2.

[Experimental Example 2]

For the cosmetic compositions containing the hot spring water of Examples 1 and 2 and the cosmetic compositions of Comparative Examples 1 and 2, a sensory test on a 9-point scale was performed to confirm moisturizing satisfaction and skin stability. The panel consisted of 30 women in their 20s and 50s. The test results are shown in Table 2 below.

Moisture satisfaction skin stability Example 1 7.5 7.4 Example 2 7.9 7.5 Comparative Example 1 5.3 6.1 Comparative Example 2 3.7 3.8

According to Table 2, it can be confirmed that the cosmetic composition containing the hot spring water of Examples 1 and 2 has excellent moisturizing satisfaction and skin stability compared to the cosmetic compositions of Comparative Examples 1 and 2.

[Experimental Example 3]

In order to confirm the sebum inhibitory effect on the cosmetic composition containing the hot spring water of Examples 1 and 2 and the cosmetic composition of Comparative Examples 1 and 2, after 4 weeks of 10 subjects, the skin oil using a skin oil meter (Sebum meter SM810) of sebum secretion was measured. Experiments were conducted at 22±2°C and 40±5% humidity. For oily skin, the measured value is 220㎍/㎠ or more, and for normal skin, it is 100-220㎍/㎠. The test results are shown in Table 3 below.

sebum inhibitory effect 0 days (before use) 28 days (after use) Example 1 240 173 Example 2 241 161 Comparative Example 1 240 195 Comparative Example 2 240 201

According to Table 3, it can be confirmed that the cosmetic composition containing the hot spring water of Examples 1 and 2 is superior to the cosmetic composition of Comparative Examples 1 and 2 to have an excellent sebum inhibitory effect.

[Experimental Example 4]

For the cosmetic compositions containing the hot spring water of Examples 1 and 2 and the cosmetic compositions of Comparative Examples 1 and 2, a skin irritation test was performed as follows to examine the skin trouble improvement effect.

After dividing 40 subjects into four groups of 10 each, using a steam generator to sweat enough for 15 minutes, the cosmetic compositions of Examples 1 and 2 and the cosmetic compositions of Comparative Examples 1 and 2 Apply vigorously around the nose and around the cheeks. Stinging grade, depending on the time the stimulus response appears after application, is intense stinging if it occurs within 30 seconds, mild stinging within 2.5 minutes, moderate stinging within 5 minutes, 8 Within minutes, it was classified as unstimulated (delayed stinging) and evaluated. The determination is made by observing the skin reactions (itchiness, stinging, soreness, redness, swelling, etc.) that appear after applying the sample to the face for 8 minutes and dividing the stimulus score by the number of subjects (n). %)) to evaluate the stimulus. The degree of skin irritation according to the stimulus positive rate (Response rate (%)) was determined according to Table 4 below, and the results are shown in Table 5.

rank Stimulus positivity (%) Judgment One 0.00-0.75 non-irritant 2 0.76-1.50 unstimulated 3 1.51-2.50 mild stimulation 4 2.51-4.00 central stimulus 5 4.01 or higher strong stimulus

Stimulus positivity (%) Judgment rank Example 1 0.59 non-irritant One Example 2 0.52 non-irritant One Comparative Example 1 1.12 unstimulated 2 Comparative Example 2 1.58 mild stimulation 3

As shown in Table 5, as a result of the skin trouble improvement test according to the skin irritation test, the cosmetic composition containing the hot spring water of Examples 1 and 2 was non-irritating, the cosmetic composition of Comparative Example 1 was non-irritating, and the cosmetic composition of Comparative Example 2 The composition appeared to be mild irritation.

In Example 1, 5 parts by weight of a whitening effect enhancer was additionally included in 100 parts by weight of the cosmetic composition including the hot spring water. The whitening effect enhancer was prepared by mixing 60% by weight of fermented rice bran extract, 25% by weight of fermented bamboo shoot extract and 15% by weight of extract of ginseng plant. The fermented rice bran extract was prepared by adding 800 parts by weight of 90% (v/v) ethanol to 100 parts by weight of rice bran, and adding 3 parts by weight of white chrysanthemum to 100 parts by weight of the rice bran extract extracted under reflux and fermenting at 30° C. for 24 hours. The fermented bamboo shoot extract was prepared by adding 600 parts by weight of purified water to 100 parts by weight of bamboo shoots, hot water extraction at 105° C. for 4 hours, adding 3 parts by weight of photosynthetic bacteria to 100 parts by weight of bamboo shoot extract, and fermentation at 25° C. for 14 hours. As the photosynthetic bacteria, Rhodopseudomonas capsulata was used. The extract was prepared by adding 500 parts by weight of propylene glycol to 100 parts by weight of 300 seconds, extracting at 55° C. for 5 hours, filtration, and aging at 31° C. for 2 days.

[Experimental Example 5]

In order to test the persistence of the skin whitening effect for the cosmetic compositions containing the hot spring water of Examples 1 and 3 and the cosmetic compositions of Comparative Examples 1 and 2, 3 times a day 10 After daily cleansing, 2 g of cosmetic lotion was applied to the face, and the degree of skin whitening improvement was measured on the 10th day. After that, the cosmetic lotion was not applied for 5 days from the 11th day, and the skin whitening degree was measured every day, and the results are shown in Table 6. For skin whitening measurement, the average value of skin tone measured after washing 20 adult women immediately before the start of the experiment was set as 100, and the lightening degree of skin tone was converted into a numerical value and displayed.

before the experiment Day 10 Day 11 Day 12 Day 13 Day 14 Day 15 Example 1 100 150 149 148 145 140 138 Example 3 100 160 158 154 152 151 148 Comparative Example 1 100 131 124 121 115 109 104 Comparative Example 2 100 115 108 105 102 100 100

According to Table 6, it can be seen that the cosmetic compositions containing the hot spring water of Examples 1 and 3 have excellent skin whitening effect, and the skin whitening lasting effect is also very excellent compared to the cosmetic compositions of Comparative Examples 1 and 2.

Claims (5)

delete delete Purified water 60-70 wt%, Butylene Glycol 3-7 wt%, Glycerin 3-7 wt%, Disodium EDTA 0.01-0.1 wt%, Citric Acid ( Citric Acid) 0.1 to 0.5% by weight, Sodium Citrate 0.1 to 0.5% by weight, Centella asiatica extract 1 to 5% by weight, Virginia Peony extract 1 to 5% by weight, Green tea extract 1 to 5% by weight, Arginine (Arginine) 0.01 ~ 0.1% by weight, Hydroxyacetophenone (Hydroxyacetophenone) 0.01 ~ 0.1% by weight, 1,2-Hexanediol (1,2-Hexanediol) 1 ~ 5% by weight and 15 ~ 25% by weight of hot spring water 1 to 5 parts by weight of a skin trouble improving agent additionally included in 100 parts by weight of the mixture,
The improvement agent for improving epithelial skin troubles contains 55 to 65% by weight of fermented oleracea extract, 20 to 30% by weight of fermented extract of sageum, and 10 to 20% by weight of fermented mung bean extract,
The extract and fermented sagebrush extract is put 600-700 parts by weight of purified water in 100 parts by weight of scorpion spp., extracted at 100-105° C. for 8-10 hours, and 2-4 parts by weight of the first mixed bacteria is added to 100 parts by weight of scorpion asiatica, and 25- Fermented at 30°C for 24 to 25 hours,
The first mixed bacteria comprises 60 to 70% by weight of Bacillus natto, 20 to 30% by weight of yeast, and 5 to 15% by weight of yeast,
The fermented extract of jeolyeong is put into 100 parts by weight of jeolyeong 70% (v/v) ethanol 600-700 parts by weight and extracted at 65-70° C. for 24-25 hours, and the second mixed bacteria 1 to 100 parts by weight of jeoryeong extract. Add 3 parts by weight and ferment for 14-15 hours at 15-20 ℃,
The second mixed bacteria comprises 60 to 70% by weight of lactic acid bacteria, 20 to 30% by weight of Hongkukbacillus and 5 to 15% by weight of Bacillus subtilis,
The mung bean extract and fermented product is obtained by adding 300 to 400 parts by weight of 80% (v/v) ethanol to 100 parts by weight of mung bean, followed by ultrasonic extraction for 14 to 16 hours, and adding 1 to 3 parts by weight of Hwangguk bacteria to 100 parts by weight of the mung bean extract and 15 to 20 parts by weight. Fermented at ℃ for 30-32 hours,
A cosmetic composition comprising hot spring water.
delete 4. The method of claim 3,
1 to 5 parts by weight of a whitening effect enhancing agent is additionally included in 100 parts by weight of the mixture,
The whitening effect enhancer includes 55 to 65% by weight of fermented rice bran extract, 20 to 30% by weight of fermented bamboo shoot extract, and 10 to 20% by weight of extract of ginseng plant,
The rice bran extract and fermented product is extracted by refluxing 700 to 800 parts by weight of 90% (v/v) ethanol to 100 parts by weight of rice bran, and 1-3 parts by weight of white chrysanthemum bacteria are added to 100 parts by weight of rice bran extract, and 24 at 26-30 ° C. It is prepared by fermentation for ~25 hours,
The fermented bamboo shoot extract is put into 100 parts by weight of bamboo shoots, 500 to 600 parts by weight of purified water, hot water extraction at 105 to 110° C. for 3 to 4 hours, and 1 to 3 parts by weight of photosynthetic bacteria are added to 100 parts by weight of the bamboo shoot extract and 20 to 25 It is produced by fermentation at ℃ for 14 to 15 hours,
The 300 seconds extract is prepared by adding 400 to 500 parts by weight of propylene glycol to 100 parts by weight of 300 seconds, extracting at 50 to 55 ° C. for 4 to 5 hours, filtering, and then aging at 31 to 33 ° C. for 2-3 days,
A cosmetic composition comprising hot spring water.