KR102244147B1 - Cosmetic composition for relieving and preventing fatigue of skin and muscles containing spicule extract and manufacturing thereof - Google Patents

Abstract

Disclosed are a functional cosmetic composition for relieving and preventing fatigue of skin and muscles containing a spicule extract in order to improve the penetration of active ingredients by containing the spongy-processed needle-shaped spicule and giving the skin a feeling of cooling and muscle warmth at the same time, and a manufacturing method thereof. The functional cosmetic composition for relieving and preventing fatigue of skin and muscles according to an embodiment of the present invention may comprise the spicule extract.

Description

TECHNICAL FIELD A functional cosmetic composition for relieving and preventing fatigue of skin and muscles containing spicule extract and manufacturing thereof comprising spicule extract

The present invention relates to a functional cosmetic composition and a manufacturing method for skin and muscle fatigue relief and prevention comprising spicule extract (hydrolides sponge), and more particularly, to a needle-shaped spicule processed with sponge The present invention relates to a functional cosmetic composition and a manufacturing method for preventing and relieving skin and muscle fatigue, including spicule extract, which can improve the penetration of active ingredients by doing so, and can give a feeling of coolness and warmth of muscles to the skin at the same time.

Many modern people suffer from muscle fatigue and blood circulation disorders. Although the method of solving it through professional treatment and prescription is effective, many people generally solve it with anti-inflammatory analgesics, drugs, and herbal acupuncture.

These universal solutions require more time and money to be invested than expected, and have many side effects. First, anti-inflammatory analgesics and drugs cause toxicity depending on the dose, and there is a risk of side effects and addiction to the body. Second, there is oriental acupuncture treatment, which cannot be done alone without basic knowledge and expert help, and the metal impregnated directly into the human body causes pain and there is a risk of damage to the skin tissue.

Therefore, there are fewer side effects than currently used anti-inflammatory analgesics and drugs, and while direct contact with the human body has less pain and damage, it is required to quickly relieve muscle and skin fatigue, and to develop research and technology that sustain the effects. to be. However, in the case of most drugs for skin, it is only applied to the surface of the skin, so that the drug effects reach the epidermis and the dermal layer has a limit.

The skin is composed of the epidermis, the dermis, and the subcutaneous tissue, and the uppermost layer of the epidermis, which is the outermost layer, is called the stratum corneum. This stratum corneum is formed when the basal cell layer of the epidermis constantly divides and rises upward, and it can be said to be the last stage of skin production. Normal skin creates new cells by repeating the process of producing and removing dead skin cells every 28 days.

These dead skin cells act as a barrier to prevent harmful foreign substances from penetrating from the outermost part of the skin, and even function to protect oil and moisture. However, such a defense mechanism of keratin is known to interfere with the penetration of active ingredients in cosmetics, so many attempts have been made to overcome this. In particular, studies of penetrating active ingredients into the stratum corneum using a microstructure such as a microneedle have been conducted. It's going on.

Sponge animals (Porifera) is a generic term for sponges. Spongy animals are metazoans with simple structures, and there are currently about 1,000 species known as animals that do not have differentiation in the embryonic design of the muscular nervous system and digestive system.

The skeleton of these sponges is supported by small bone fragments (骨片, spicule), and is made of calcareous or siliceous material, and is divided into skeletal bones and microbones. The soft and tough skeleton of keratin sponges and keratin sponges has been used since ancient times for cleaning, bathing, and painting. In the Middle Ages, burned sponges were used to treat various diseases. Wild sponges have been used to make pottery jewelery or paint, and recently, freshwater sponges such as Spongilla lacustris L., Spongilla fragilis Leidy, and Epidatia flu. It is used as a cosmetic or surgical drug by separating a needle-shaped spicule, a skeletal tissue, from the skeleton of Ephydatia fluviatilis.

These spicules are divided into two types: Megascleres and Microscleres, and Megascleres are 60-2,000㎛ in size and can be distinguished with the naked eye. Microscleres are observed using a microscope with a size of 10 to 60 μm.

In addition, spicules are formed in the form of stars, spheres, shovels, citations, half-moons, needles, etc., depending on the shape of Anisochelas, Chelae, Euasters, and Forceps. ), Isochelas, Microstrongyles, Oxeas, and style. Of these, Oxeas has a needle shape on both sides and a tube that crosses the center (lumen , 內腔) is found.

In particular, spicule's acicular structure has a structure capable of penetrating the stratum corneum and has porosity, which is being studied as a major means of supplying the active ingredients of cosmetics into the stratum corneum. However, the existing spicule is manufactured using chemicals including hydrochloric acid, and the active ingredients used together are also limited to external skin preparations, so efforts to improve them are needed.

(0001) Korean Patent Application Publication No. 10-2019-0070556 (0002) Korean Patent Registration No. 10-1678621

The present invention has been conceived to solve the above problems, and an object of the present invention is to simultaneously protect the skin and sedate the stiff muscle bath by including a component capable of simultaneously giving a feeling of coolness to the skin and a feeling of warmth of muscles. It is to provide cosmetic products that can be used and their manufacturing methods.

In addition, another object of the present invention is to provide a cosmetic product containing a natural substance with less side effects and capable of minimizing skin damage and enhancing the permeability of an active ingredient to give a high fatigue-relieving effect of muscles and a method for manufacturing the same.

In addition, another object of the present invention is to provide a cosmetic product having a high muscle and skin soothing effect compared to conventional cosmetic products by permeating active ingredients under the stratum corneum of the skin as it contains spicule, and a method for manufacturing the same.

The subject of the present invention is not limited to the problems mentioned above, and other problems that are not mentioned will be clearly understood by those skilled in the art from the following basis.

The functional cosmetic composition for relieving and preventing skin and muscle fatigue according to an embodiment of the present invention for solving the above problems may include spicule extract.

In one embodiment, the cosmetic composition, (a) hydrolyzed sponge; (b) extracts derived from nature, including white oyster mushroom extract and olive leaf extract; (c) aromatic oils; And (d) containing a solvent, wherein the hydrolyzed sponge includes the steps of: (i) washing the collected sponge and then drying it so that the moisture content is less than 10% by weight; (ii) heating the dried sponge by immersing it in water at 90 to 100° C. for 10 to 40 minutes; (iii) immersing the heated sponge in an acidic solution having a pH of 2 to 4 for 10 to 20 days; (iv) separating the acidic solution from the solid content of the sponge, and then washing the solid content with water by repeating 2 to 5 times; (v) immersing the washed solids in water and then washing them using ultrasonic waves; (vi) after the ultrasonic cleaning is completed, immersing the sponge in a basic solution having a pH of 8 to 10 for 1 to 5 days; (vii) separating the basic solution from the solid and then washing the solid with water by repeating 2 to 5 times; And (viii) immersing the washed solids in water and then washing them using ultrasonic waves, and the acidic solution comprises lemon juice, citron juice, sugar citron juice, orange juice and vinegar. It is a mixture of one or more selected from the group containing, the basic solution is a step of separating and then washing the shellfish shells; Sintering the washed clam shells at a temperature of 800 to 1200°C; Crushing the sintered shellfish shell; Mixing the crushed clam shells with 1000 to 5000 parts by weight of water relative to 100 parts by weight of clam shells, and then leaving them for 2 to 10 days; And separating the solid content of the shellfish shell. It is a solution prepared by a method including, the ultrasonic wave has a frequency of 20 to 130 kHz, the hydrolyzed sponge contains 0.005 to 0.1 parts by weight based on 100 parts by weight of the solvent, and the natural extract is 100 parts by weight of the solvent Contrasting white tree mushroom extract 0.1 to 5.0 parts by weight and olive leaf extract 0.01 to 5.0 parts by weight, the natural extract further comprises an extract of Sangbaekpi, Eoseongcho, Mokdanpi, or a mixture thereof, and the aromatic oil is lavender, rosemary , Eucalyptus, Cypress, Bergamot, Sandalwood, Rose, and a mixture of one or more extracts selected from the group of lemon and menthol, the cosmetic composition further comprises a thickener, preservatives, pH regulators, antioxidants, emulsifiers, emulsifying aids It may include a spicule extract, characterized in that.

In addition, the present invention is a water-soluble dissolving step to obtain a water-soluble mixture by mixing and then dissolving the hydrolyzed sponge in a water-soluble component including a natural extract including a white wood mushroom extract and an olive leaf extract, a thickener, a preservative, and a moisturizing agent; A fat-soluble dissolving step of dissolving aroma oil and fat-soluble components including menthol in silicone oil to obtain a fat-soluble mixture; Emulsifying step of mixing the water-soluble mixture, the oil-soluble mixture, and an emulsifier to obtain an O/W-type gel; And a packaging step of injecting the O/W-type gel into an aluminum container, wherein the hydrolyzed sponge comprises the steps of: (i) washing the collected sponge and drying it so that the moisture content is less than 10% by weight; (ii) heating the dried sponge by immersing it in water at 90 to 100° C. for 10 to 40 minutes; (iii) immersing the heated sponge in an acidic solution having a pH of 2 to 4 for 10 to 20 days; (iv) separating the acidic solution from the solid content of the sponge, and then washing the solid content with water by repeating 2 to 5 times; (v) immersing the washed solids in water and then washing them using ultrasonic waves; (vi) after the ultrasonic cleaning is completed, immersing the sponge in a basic solution having a pH of 8 to 10 for 1 to 5 days; (vii) separating the basic solution from the solid and then washing the solid with water by repeating 2 to 5 times; And (viii) immersing the washed solids in water and then washing them using ultrasonic waves, and the acidic solution comprises lemon juice, citron juice, sugar citron juice, orange juice and vinegar. It is a mixture of one or more selected from the group containing, the basic solution is a step of separating and then washing the shellfish shells; Sintering the washed clam shells at a temperature of 800 to 1200°C; Crushing the sintered shellfish shell; Mixing the crushed clam shells with 1000 to 5000 parts by weight of water relative to 100 parts by weight of clam shells, and then leaving them for 2 to 10 days; And it is a solution prepared by a method comprising the step of separating the solid content of the shell, the ultrasonic wave has a frequency of 20 to 130 kHz, the hydrolyzed sponge contains 0.005 to 0.1 parts by weight relative to 100 parts by weight of the solvent, , The natural-derived extract comprises 0.1 to 5.0 parts by weight of white oyster mushroom extract and 0.01 to 5.0 parts by weight of olive leaf extract relative to 100 parts by weight of a solvent, and the natural extract further comprises extracts of Sangbaekpi, Eoseongcho, Mokdanpi, or a mixture thereof. The aromatic oil is a mixture of one or more extracts selected from the group of lavender, rosemary, eucalyptus, cypress, bergamot, sandalwood, rose and lemon, and menthol, and after the emulsification step is completed, a thickener, preservative, and pH adjuster It provides a method for producing a cosmetic composition comprising a spicule extract, characterized in that it further comprises the step of mixing an antioxidant, an emulsifying agent, and an emulsifying aid.

According to the exemplary embodiment of the present invention, it is possible to provide a feeling of cooling of the skin and a feeling of warming of the muscles at the same time, thereby having an excellent effect on the recovery of the skin and muscles.

In addition, according to the present invention, since the active ingredient contained in the cosmetic can be effectively delivered to the layer below the stratum corneum by including spicule, it is possible to manufacture a cosmetic product having a higher effective ingredient delivery power compared to the existing cosmetic product.

In addition, the present invention provides a cosmetic composition capable of effectively relieving muscle and skin fatigue by providing beneficial effects such as pain relief or damage recovery by directly acting on the affected area and having fewer side effects than commonly used analgesic anti-inflammatory drugs. Can provide.

The effects according to the present invention are not limited by the contents exemplified above, and more various effects are included in the present invention.

Hereinafter, various embodiments will be described in more detail with reference to the accompanying drawings. The embodiments described herein may be variously modified. Certain embodiments may be depicted in the drawings and described in detail in the detailed description. However, specific embodiments disclosed in the accompanying drawings are only intended to facilitate understanding of various embodiments. Therefore, the technical idea is not limited by the specific embodiments disclosed in the accompanying drawings, and it should be understood to include all equivalents or substitutes included in the spirit and scope of the invention.

Terms including ordinal numbers such as first and second may be used to describe various elements, but these elements are not limited by the above-described terms. The above-described terms are used only for the purpose of distinguishing one component from other components.

In the present specification, terms such as "comprises" or "have" are intended to designate the presence of features, numbers, steps, actions, components, parts, or combinations thereof described in the specification, but one or more other features. It is to be understood that the presence or addition of elements or numbers, steps, actions, components, parts, or combinations thereof does not preclude in advance. When a component is referred to as being "connected" or "connected" to another component, it is understood that it may be directly connected or connected to the other component, but other components may exist in the middle. It should be. On the other hand, when a component is referred to as being "directly connected" or "directly connected" to another component, it should be understood that there is no other component in the middle.

Meanwhile, a "module" or "unit" for a component used in the present specification performs at least one function or operation. In addition, the "module" or "unit" may perform a function or operation by hardware, software, or a combination of hardware and software. In addition, a plurality of "modules" or a plurality of "units" excluding "module" or "unit" to be performed in specific hardware or performed by at least one processor may be integrated into at least one module. Singular expressions include plural expressions unless the context clearly indicates otherwise.

In addition, in describing the present invention, when it is determined that a detailed description of a related known function or configuration may unnecessarily obscure the subject matter of the present invention, the detailed description thereof will be abbreviated or omitted.

The present invention relates to a functional cosmetic composition comprising spicule extract for relieving and preventing fatigue of skin and muscles.

It is called the spiculne hydrolyzed sponge and is a component manufactured by separating and purifying only the incupuncture of the sponge. Since this spicule not only has a needle-shaped structure but also has many pores on its surface, it can be used as a carrier for an active ingredient in cosmetics by using these pores.

In addition, the spicules are divided into two types, Megascleres and Microscleres, depending on their size, and Megascleres can be distinguished with the naked eye in a size of 60-2,000㎛. And, Microscleres (Microscleres) can be observed using a microscope with a size of 10 to 60㎛. In the present invention, it is preferable to use a micro class spicule having a size of 30 to 50 μm. At this time, if the size of the spicule is less than 30 μm, the porosity may decrease, so that the delivery ability of the active ingredient may decrease, and if it exceeds 50 μm, it may irritate the skin.

Existing spicule separates organic parts except incisors using strong acids and strong bases such as hydrochloric acid, but in this case, it has a disadvantage that it can irritate the skin due to strong acids and strong bases remaining in the porous area while having high productivity. . Therefore, in the present invention, it is preferable to separate the spicules using acids and bases obtained from natural substances instead of the strong acids and bases.

To this end, the spicules (hydrolyzed sponges) include (i) washing the collected sponges, and then drying them so that the moisture content is less than 10% by weight; (ii) heating the dried sponge by immersing it in water at 90 to 100° C. for 10 to 40 minutes; (iii) immersing the heated sponge in an acidic solution having a pH of 2 to 4 for 10 to 20 days; (iv) separating the acidic solution from the solid content of the sponge, and then washing the solid content with water by repeating 2 to 5 times; (v) immersing the washed solids in water and then washing them using ultrasonic waves; (vi) after the ultrasonic cleaning is completed, immersing the sponge in a basic solution having a pH of 8 to 10 for 1 to 5 days; (vii) separating the basic solution from the solid and then washing the solid with water by repeating 2 to 5 times; And (viii) immersing the washed solid content in water and then washing using ultrasonic waves.

The step (i) is a step of washing the collected sponge and then drying it so that the moisture content is less than 10% by weight. After washing the foreign matter present on the surface of the clarification, it is dried. At this time, the sponge may be dried so that the moisture content is less than 10% by weight, preferably less than 7% by weight. Through this drying, the mucous components that always exist on the surface of the sea surface can be more easily removed, and the organic components contained in the sea surface are decomposed during the drying process as described above and the tissue is destroyed, so that subsequent processes can be more easily performed. I can.

The step (ii) is a step of immersing the dried sponge in water at 90 to 100°C for 10 to 40 minutes to heat the dried sponge to promote the denaturation of the protein component. This is a step that facilitates. In general, animals are composed mostly of proteins except for the mineral skeleton. In the case of this protein, since it plays the role of connecting the skeleton, it is composed of a very hard tissue, but when it is heated, the protein is denatured and may be easily separated from the skeleton. Using this, in the case of the present invention, the dried sponge is immersed in water at 90 to 100° C., that is, boiling water, thereby causing the denaturation of the protein, thereby facilitating the separation of the protein. In this case, if the immersion time is less than 10 minutes, it may be difficult to separate the protein, and if the immersion time is longer than 40 minutes, the degraded protein may be adsorbed to the pores of the incus.

The step (iii) is a step of immersing the heated sponge in an acidic solution having a pH of 2 to 4 for 10 to 20 days, and removing organic substances present on the heated sponge using an acid. In general, organic matter can be removed by accelerating its decomposition rate when it comes into contact with an acid. However, in the conventional spicule manufacturing method, hydrochloric acid is used to remove it, but this may have a problem in that hydrochloric acid remains in the porous portion of the spicule and may cause skin irritation. Therefore, in the present invention, it is preferable to prepare the spicules using natural acidic substances such as lemon juice, citron juice, sugar citron juice, orange juice and vinegar. That is, the heated sponge may be immersed in the lemon juice, citron juice, sugar citron juice, orange juice, or vinegar. At this time, if the immersion period is less than 10 days, it may be difficult to remove the organic matter, and if it exceeds 20 days, the incupuncture may be decomposed by acid. In addition, when organic matter is removed using an acid as described above, a part of the incupuncture may be dissolved and the porosity of the incupuncture may be further increased. In addition, when the acidic solution is less than pH2, the incupuncture may be decomposed due to strong acidity or irritation to the skin due to the residual acidic solution, and when the acidic solution exceeds pH4, it may be difficult to decompose such organic matter.

After the (iii) step is completed, (iv) the acidic solution and the solid content of the sponge may be separated, and then the solid content may be washed by repeating 2 to 5 times with water. By the acidic solution, the incus and the organic component can be separated, and most of the organic component can be changed into a state dissolved in the acidic solution. Therefore, in the case of separating the solids as described above, most of the solids may be composed of the incupuncture, which may be washed several times to perform the next step.

The step (v) is a step of (v) immersing the washed solids in water and then washing them using ultrasonic waves, and removing foreign matters including organic substances adhering to the incupuncture bone using ultrasonic waves.

At this time, since the ultrasonic waves are better transmitted in water, the solid content may be immersed in water for smooth transmission of the ultrasonic waves. In addition, the ultrasonic wave may have a frequency of 20 to 130 kHz, and the above-described cleaning can be performed only in the frequency range.

The step (vi) is a step of immersing the sponge in a basic solution having a pH of 8 to 10 for 1 to 5 days after the ultrasonic cleaning is completed, and is a step of washing by immersing the solid content on which the ultrasonic cleaning has been completed in a basic solution. Although most of the organic matter can be removed through the acidic solution immersion process, it is preferable to use a basic solution in order to finally remove the organic matter. In particular, in the case of a basic solution, not only has the property of easily decomposing the protein of the sponge, but also can neutralize the acidic solution present in the porous portion of the spicule.

At this time, in the case of the existing basic solution, a strong base, that is, sodium hydroxide or potassium hydroxide was used for convenience of use, but in this case, the residual basic solution may irritate the skin. Therefore, in the case of the present invention, it is preferable to prepare and use a basic solution using calcium carbonate. In particular, in the case of the spicule of the present invention, since it can be used in contact with the skin, the calcium carbonate may also be prepared using a shell shell, not an industrially synthesized product.

Looking at this in detail, the basic solution comprises the steps of separating and then washing the shellfish; Sintering the washed clam shells at a temperature of 800 to 1200°C; Crushing the sintered shellfish shell; Mixing the crushed clam shells with 1000 to 5000 parts by weight of water relative to 100 parts by weight of clam shells, and then leaving them for 2 to 10 days; And it may be a solution prepared by a method comprising the step of separating the solid content of the shellfish shell.

The shells of the shellfish are mainly composed of a large amount of calcium carbonate, and most of them are treated as waste. Therefore, when calcium carbonate is extracted and used from such shells, it can contribute to resource recycling and environmental protection while exhibiting the desired effect. The shellfish shell may be washed and organic matter removed, and then calcined at a temperature of 800 to 1200°C. Through this, organic matter present in the shellfish shell may be removed by oxidation of other impurities, and only calcium carbonate may remain. At this time, if the firing temperature is less than 800°C, smooth firing may not be performed. If the firing temperature exceeds 1200°C, energy usage increases and calcium carbonate is decomposed by firing, resulting in a decrease in yield.

After the firing is completed as described above, it can be pulverized, mixed with 1000 to 5000 parts by weight of water relative to 100 parts by weight, and then left to stand for 2 to 10 days to prepare an aqueous calcium carbonate solution. At this time, if less than 1000 parts by weight of water is used, the amount of the aqueous solution to be prepared may be reduced and the efficiency may be reduced, and if more than 5000 parts by weight of water is used, the concentration of calcium carbonate is lowered, so that the effect of calcium carbonate cannot be expected. .

In the basic solution prepared as described above, the ultrasonically cleaned solid component may be added and immersed for 1 to 5 days. At this time, when immersed for less than 1 day, it is difficult to expect the effect due to the basic solution, and when added for more than 5 days, there is no further effect and the manufacturing efficiency decreases.

When washing with the basic solution is completed as described above, it is possible to manufacture spicules (hydrolyzed sponges) through ultrasonic washing and washing in the same manner as in the steps after washing with acidic acidic solution.

The spicule prepared as described above may be mixed with a naturally derived extract, an aromatic oil, and a solvent to be prepared into a cosmetic composition. In other words, Hydrolyzed Sponge (Spicul) is a microneedle (fine needle) that allows the active ingredients of the natural extract and aroma oil to penetrate the skin quickly and deeply into the dermis, and aroma due to rapid volatilization like alcohol. It prevents the oil from evaporating into the air to maintain the persistence of the active ingredients of the aromatic oil. In addition, the relaxation and activation, moisturizing and soothing effects of stiff muscle skin can be further maximized.

The natural-derived extract is for supplying moisture and nutrition without irritation to the skin, and for imparting elasticity, and may include a white tree mushroom extract and an olive leaf extract.

The white tree mushroom extract has excellent moisturizing effect and, unlike conventional hyaluronic acid, when dried, it forms a protective film on the skin to maintain moisture. This white tree mushroom extract is used in an amount of 0.01 to 5.0 parts by weight based on 100 parts by weight of the solvent. When the white ear mushroom extract is used in an amount of less than 0.01 parts by weight, it is difficult to expect the effect of the white ear mushroom extract, and when it is used in an amount exceeding 5.0 parts by weight, the formulation of the cosmetic may become too sticky and it may be difficult to apply it to the skin.

The olive leaf extract not only keeps the skin young by promoting collagen production, but is also effective in skin whitening by inhibiting the production of melanin. These olive leaf extracts are used in an amount of 0.01 to 5.0 parts by weight based on 100 parts by weight of the solvent. When the olive leaf extract is used in an amount of less than 0.01 parts by weight, it is difficult to expect the effect of the olive leaf extract, and when it is used in excess of 5.0 parts by weight, the cost used for manufacturing a cosmetic composition may increase.

In addition, as the naturally derived extract, only white oyster mushroom extract and olive leaf extract may be used, but in order to further add useful functions to the skin, Sangbaekpi, Eoseongcho, Mokdanpi, or a mixture thereof may be further used.

Sangbaekpi extract has the function of soothing the skin and imparting elasticity. Eoseongcho extract helps relieve skin irritation and is effective in soothing the skin. Mokdanpi extract gives elasticity to the skin and soothes the skin. These Sangbaekpi, Eoseongcho, Mokdanpi extracts may be used in each of 0.01 to 5.0 parts by weight based on 100 parts by weight of the solvent.

The aromatic oil (aroma herb extract) is selected from the group of lavender, rosemary, eucalyptus, cypress, bergamot, sandalwood, rose, and lemon as for relieving muscle tension and spasm and soothing and relaxing the skin and nerves caused by fragrance. A mixture of one or more extracts and menthol to be used may be used.

For example, lavender oil has the ability to improve skin, relieve muscle tension and stress, and also serves as a solubilizer.

In addition, eucalyptus oil improves skin absorption, promotes blood circulation, and has a moisturizing function. These eucalyptus oils are nonionic thickeners and have a function of controlling the viscosity when dissolving in oil-soluble substances.

Cypress oil is effective in relaxing muscles, and bergamot oil has the ability to improve and calm the skin. Sandalwood oil replenishes the skin with moisture and soothes the skin, while rose oil provides elasticity to the skin, supplies moisture and nutrition, and has the effect of relaxing and soothing muscle tension. The sandalwood and rose oil also play a role in adjusting the pH when dissolving in a fat-soluble manner.

In this way, according to the purpose or use required by the user, a composition containing one selected from the aromatic oils or a mixture thereof as a main component may be prepared. These aromatic oils may be used in an amount of 0.01 to 5.0 parts by weight based on 100 parts by weight of the solvent. If the aroma oil is mixed in less than 0.01 parts by weight, it is difficult to expect the effect of the aroma oil, and if it is included in more than 5.0 parts by weight, the oil content in the formulation increases, so that when applied, it is difficult to separate the oil component or greasy. Can happen.

In addition, the aromatic oil may contain menthol (oil). The menthol is intended to release the stiff skin muscles and give the skin a refreshing sensation, and is mixed in a large amount compared to the aromatic oil, but when used excessively, it may irritate the skin, so 0.1 to 20 parts by weight per 100 parts by weight of the solvent Is used. If the menthol is contained in an amount of less than 0.1 parts by weight, it is difficult to expect the effect of menthol, and if it is contained in an amount exceeding 20 parts by weight, it may irritate the skin and cause side effects such as erythema.

Purified water, ethanol, or a mixture thereof may be used as the solvent, or a mixture thereof may be used. In particular, such a solvent is a factor that determines the formulation of the cosmetic composition, and when the content of the solvent is lowered, the viscosity of the cosmetic composition is increased to have a cream or ointment type formulation. Since the viscosity of the cosmetic composition is lowered, it can have a liquid formulation.

Components constituting the massage cosmetic composition according to the present invention include natural extracts, aromatic oils and hydrolyzed sponges (spicules), as well as thickeners, preservatives, pH regulators, antioxidants, emulsifiers, emulsifiers commonly used in the manufacture of cosmetic compositions. Additives including adjuvants may be used.

The thickener is for making the gel-type formulation stable by increasing the viscosity, and carbomer and sodium chloride may be used. Carbomer is a water-soluble viscosity modifier synthesized from acrylic acid, and is added to increase the viscosity or concentration of raw materials to maintain a stable shape. Sodium Chloride (Sodium Chloride) A water-soluble thickener that increases the viscosity and calms the skin. The thickener may be used in an amount of 0.1 to 5.0 parts by weight based on 100 parts by weight of the solvent. When the thickener is used in an amount of less than 0.1 parts by weight, it is difficult for the cosmetic composition to maintain an appropriate formulation, and when it is used in an amount exceeding 5.0 parts by weight, it may be difficult to apply the composition to the fibo due to the increased viscosity.

The preservative has antibacterial activity and is for preventing spoilage of natural extracts and aromatic oils, and caprylyl glycol, 1,2-hexanediol may be used. Caprylyl Glycol is a substance obtained in the process of decomposition of vegetable oils. It has antibacterial action against bacteria, increases product stability, extends lifespan, and maintains moisture in the skin. 1,2-Hexanediol (1,2-Hexanediol) has a good moisturizing power and antibacterial properties, plays a role in preserving natural extracts, has no irritation, and has excellent compatibility with water. In addition, methylparaben and propylparaben may be additionally used. However, since parabens such as methyl paraben or propyl paramen are recently known as hormone-disrupting substances, it is desirable to minimize their content when using them. Since the preservative may irritate the skin when used excessively, 0.01 to 2.0 parts by weight may be used based on 100 parts by weight of the solvent. When the preservative is used in an amount of less than 0.01 parts by weight, the cosmetic composition may be deteriorated by pathogens, and when it is included in an amount exceeding 2.0 parts by weight, it may irritate the skin, resulting in side effects.

The pH adjuster is for appropriately adjusting or stabilizing the pH to reduce irritation to the skin, and the pH adjusting agent is triethanolamine, tromethamine, potassium hydroxide, sodium hydroxide, arginine, etc. I can. At this time, the amount of the pH adjusting agent used may be 0.001 to 0.1 parts by weight based on 100 parts by weight of the solvent. When the pH adjuster is used in an amount of less than 0.001 part by weight, it may irritate the skin, and even when it is used in an amount exceeding 0.1 part by weight, the skin may be irritated due to the increased content.

The antioxidant is for inhibiting the reaction by oxygen to prevent oxidation and decay, and to prevent the occurrence of precipitates, disodium EDTA, ethylenediaminetetraacetic acid disodium salt, EDTA 2Na) can be used. The antioxidant may be included in an amount of 0.01 to 0.5 parts by weight based on 100 parts by weight of the solvent. If the antioxidant is contained in an amount of less than 0.01 parts by weight, the cosmetic composition may be oxidized to generate a precipitate, and if it exceeds 0.5 parts by weight, it may irritate the skin.

The moisturizer is to retain moisture so that moisture does not evaporate from the skin, and glycerin, dipropylene glycol, butylene glycol, or polyhydric alcohols are used, and excessive use of such moisturizer may cause stickiness. It is preferable to use 0.1 to 5.0 parts by weight based on 100 parts by weight of the solvent because there is a risk of irritation.

The emulsifier is to ensure that the water-soluble component for supplying moisture and the oil-soluble component for retaining it are not separated and mixed well, and the polysorbate series (polysorbate 80), dimethicone series (cetyl PG/PP-10) are not separated. /Dimethicone), etc. are used selectively. The polysorbate series (Polysorbate 80; product name Tween 80) is a water-soluble nonionic surfactant that easily dissolves poorly soluble components and helps stabilize the emulsion of other components. The emulsifier of dimethicone (Cetyl PEG/PPG-10/1 Dimethicone) is an oil emulsifier and can be used to easily emulsify the oily component of silicone-based oil with an aqueous phase. When the emulsifier is used excessively, the viscosity of the gel-type massage cosmetic product obtained according to the present invention increases, and the contents do not flow out well when used inside a container, so the spreadability to the skin decreases, and the cooling sensation expressed from the water-soluble part (water-soluble component) Since it becomes difficult to deliver to the skin, 0.01 to 1.0 parts by weight may be used based on 100 parts by weight of the solvent.

The emulsion stabilizer (emulsification aid) is for maintaining the stability and life of the gel formulation without separating the emulsion, and polyacrylates and polyacrylamides are used. It is preferably used in an amount of 0.1 to 1.0 parts by weight based on 100 parts by weight of the solvent because it is elevated and the contents do not flow out well from the container, making it difficult to apply to the skin. In addition, sodium chloride is used as the emulsification stabilizer, that is, sodium chloride acts as a stabilizer so that the phase separation of the silicone oil to be described later with the water-soluble component does not occur.

As other sub-materials, silicone oil may be used to give a cool feeling when applied to the skin and soften the skin because it is volatile. Such silicone oil is selectively used from cyclopentasiloxane and hexamethyldisiloxane.

Cyclopentasiloxane softens the skin and gives it a cool feeling, and hexamethyl disiloxane not only softens the skin, but also keeps the skin moisturized, and also adjusts the viscosity to apply the composition. It also plays a role in adjusting the thickness. If too much of such silicone oil is used, the emulsion stability with the water-soluble component may be lost. Therefore, 0.01 to 30 parts by weight of the solvent is preferably used.

In addition, 0.01 to 1.0 parts by weight of fragrance may be additionally used based on 100 parts by weight of the solvent. As described above, the present invention is made of natural extracts and aromatic oils as main components, but in order to quickly and deeply penetrate the skin with the active ingredients they have, and to maintain the duration of the feeling of coolness and warmth felt in the skin, hydrolyzed sponge (Spicul ) Is added appropriately, and other raw materials are properly blended.

Hereinafter, the present invention will be described in detail through a method of manufacturing a cosmetic composition.

[1] water-soluble dissolution

This is the step of dissolving water-soluble ingredients.

Naturally derived extracts including white oyster mushroom extract and olive leaf extract, and water-soluble ingredients including thickeners, preservatives, moisturizers, and antioxidants are added to the main tank and dissolved while mixing and stirring at room temperature.

[2] fat-soluble dissolution

This is the step of dissolving the fat-soluble ingredients.

Aroma oil consisting of one selected from lavender, rosemary, eucalyptus, cypress, bergamot, sandalwood, rose, and lemon oil, or a mixture thereof, and fat-soluble components including menthol are dissolved in silicone oil while stirring. At this time, since the oil-soluble components may be volatilized due to vaporization, stirring is performed at room temperature. At this time, the stirring speed is not to exceed 1000 rpm to prevent the viscosity from increasing so that the cosmetic according to the present invention flows out smoothly out of the roll-on-ball container.

[3] oil paintings

This is a step of mixing a fat-soluble mixture with an aqueous mixture.

The oil-soluble mixture obtained in step [2] was added to the main tank in step [1], and an emulsifier such as Tween 80 or Cetyl Pig/P PEG-10/Dimethicone was added to make the oil-soluble mixture uniform in the aqueous mixture. Mixing and stirring so as to be dispersed to obtain an O/W type gel.

At this time, stirring is performed at room temperature to minimize vaporization of components such as aroma oil and menthol.

The gel thus obtained is in a state in which the effective nutrients, fragrance, and hydrogen of natural extracts and aroma oils are embedded inside the hydrogen bubbles, and thus, when the user applies them to the skin, they can be absorbed deeply into the skin. At this time, the stirring speed is prevented from increasing the viscosity so that the formulation according to the present invention does not exceed 1000 rpm to smoothly flow out of the roll-on-ball container.

[4] packaging

This is the step of injecting the gel-formed composition (final cosmetic product) into the container.

The gel composition obtained in step [3] is injected into a container of a predetermined shape after passing through a filtration process. Gel-type massage cosmetics that have been injected into the container as described above are hydrolyzed sponges (spicules) when applied evenly to the skin area desired by the user using a roller ball coupled to the open part of the container, and extracts derived from nature and The skin penetration power of the active ingredient of the aroma oil can be increased by 25 times.

Hereinafter, preferred embodiments of the present invention will be described with reference to the accompanying drawings so that those of ordinary skill in the art can easily implement them. In addition, in describing the present invention, when it is determined that a detailed description of a related known function or a known configuration may unnecessarily obscure the subject matter of the present invention, a detailed description thereof will be omitted. In addition, certain features shown in the drawings are enlarged or reduced or simplified for ease of description, and the drawings and their components are not necessarily drawn to scale. However, those skilled in the art will readily understand these details.

Example

It is to measure the efficacy of the initial cool feeling, the duration of the feeling of coolness and warmth, and the scent of the massage cosmetic composition according to the present invention.

Each component constituting the composition of the present invention was mixed at an appropriate blending ratio (weight ratio) to make Examples 1 to 3, but in particular, hydrolyzed sponges (spicules) were added in different ways. In addition, conventional aroma massage cosmetics, that is, hydrolyzed sponges (spicules) were not used, and the mixing ratio of each component was varied as Comparative Examples 1 to 3, which are shown in Table 1 below.

ingredient Example 1 Example 2 Example 3 Comparative Example 1 Comparative Example 2 Comparative Example 3 Cypress oil One Bergamot oil One Sandwood Oil One Rose oil One One Lavender oil One One Eucalyptus oil One One menthol One One One One One One ethanol 5 5 Iropropanol 5 Mineral oil 15 Isopropyl myristate 15 Hydrolyzed Sponge (Spicul) 0.5 One 1.5 - - - glycerin 5 5 5 5 5 5 Carbomer 0.1 0.2 0.5 0.5 0.2 Laureth-7 0.5 Sodium polyacrylate 0.3 0.3 0.3 0.5 Triethanolamine 0.1 0.2 0.5 0.5 0.2 Disodium EDTA 0.05 0.05 0.05 0.05 0.05 0.05 Methylparaben 0.1 0.1 0.1 0.1 0.1 0.1 Profile Paraben 0.1 0.1 0.1 0.1 0.1 0.1 Tween 80 0.5 0.5 0.5 0.1 0.5 0.5 Purified water 100 100 100 100 100 100

Test example

Each cosmetic composition obtained by the blending ratio shown in Table 1 was evenly applied to the shoulders, neck, knees and waist regions for users whose muscles were stiff and fatigued due to excessive exercise, and after a certain period of time, symptoms (effect ) It is shown in Table 2 below for the change.

Item Example 1 Example 2 Example 3 Comparative Example 1 Comparative Example 2 Comparative Example 3 Initial cool feeling delivery time
(second) 30 25 22 55 55 65 Dry or sticky skin after use Appropriate without feeling dry or sticky Dryness Sticky Cold duration
(minute) 65 75 80 50 50 60 Smell Stable aroma without alcohol odor Alcohol intoxication Stable aroma

According to the results of Table 2, in the case of Examples 1 to 3, the initial cooling sensation of the aroma components appeared 30 seconds before, and the duration of the cooling sensation was also maintained for a long time without alcohol-induced skin dryness, unlike Comparative Examples 1 and 2. In addition, even though alcohol was not used at all, it was found that the duration of the cooling sensation reached or reached the value of the comparative example. Since it can deliver scent well, it can be seen that it is effective in the fragrance treatment function, which is the original characteristic of aroma oil. In addition, Comparative Example 3 uses mineral oil instead of alcohol as a material that delivers the aroma component to the skin, thereby reducing the skin dryness that appears due to the rapid vaporization of the alcohol components of Comparative Examples 1 and 2, and imparting a moisturizing sensation, as well as aroma fragrance. Although it was possible to save more, the feeling of use was burdensome as the initial rate of expression of cool sensation was lower than in Examples 1 to 3, and stickiness was felt on the skin surface.

In the above, preferred embodiments of the present invention have been illustrated and described, but the present invention is not limited to the specific embodiments described above, and the present invention is generally in the technical field to which the present invention belongs without departing from the gist of the present invention claimed in the claims. Of course, various modifications may be made by those skilled in the art, and these modifications should not be understood individually from the technical idea or perspective of the present invention.

Claims (3)

In the cosmetic composition containing spicule,
The cosmetic composition,
(a) hydrolyzed sponge;
(b) extracts derived from nature, including white oyster mushroom extract and olive leaf extract;
(c) aromatic oils; And
(d) solvent
Including,
The hydrolyzed sponge,
(i) washing the collected sponge and then drying it so that the moisture content is less than 10% by weight;
(ii) heating the dried sponge by immersing it in water at 90 to 100° C. for 10 to 40 minutes;
(iii) immersing the heated sponge in an acidic solution having a pH of 2 to 4 for 10 to 20 days;
(iv) separating the acidic solution from the solid content of the sponge, and then washing the solid content with water by repeating 2 to 5 times;
(v) immersing the washed solids in water and then washing them using ultrasonic waves;
(vi) after the ultrasonic cleaning is completed, immersing the sponge in a basic solution having a pH of 8 to 10 for 1 to 5 days;
(vii) separating the basic solution from the solid and then washing the solid with water by repeating 2 to 5 times; And
(viii) immersing the washed solids in water and then washing them using ultrasonic waves;
It is manufactured by a manufacturing method comprising a,
The acidic solution is a mixture of one or more selected from the group containing lemon juice, citron juice, sugar citron juice, orange juice and vinegar,
The basic solution is
Separating the shells and then washing them;
Sintering the washed clam shells at a temperature of 800 to 1200°C;
Crushing the sintered shellfish shell;
Mixing the crushed clam shells with 1000 to 5000 parts by weight of water relative to 100 parts by weight of clam shells, and then leaving them for 2 to 10 days; And
Separating the solid content of the shellfish shell;
It is a solution prepared by a method containing,
The ultrasonic wave has a frequency of 20 to 130 kHz,
The hydrolyzed sponge contains 0.005 to 0.1 parts by weight based on 100 parts by weight of the solvent,
The natural-derived extract contains 0.1 to 5.0 parts by weight of white oyster mushroom extract and 0.01 to 5.0 parts by weight of olive leaf extract relative to 100 parts by weight of the solvent,
The natural extract further comprises an extract of Sangbaekpi, Eoseongcho, Mokdanpi, or a mixture thereof,
The aromatic oil is a mixture of menthol and one or more extracts selected from the group of lavender, rosemary, eucalyptus, cypress, bergamot, sandalwood, rose, and lemon,
The cosmetic composition is a cosmetic composition comprising a spicule extract, characterized in that it further comprises a thickener, a preservative, a pH adjusting agent, an antioxidant, an emulsifying agent, and an emulsifying aid.
delete A water-soluble dissolving step of mixing and dissolving hydrolyzed sponges in a water-soluble component including a natural extract including a white wood ear mushroom extract and an olive leaf extract, a thickener, a preservative, and a moisturizing agent to obtain an aqueous mixture;
A fat-soluble dissolving step of dissolving aroma oil and fat-soluble components including menthol in silicone oil to obtain a fat-soluble mixture;
Emulsifying step of mixing the water-soluble mixture, the oil-soluble mixture, and an emulsifier to obtain an O/W-type gel; And
A packaging step of injecting the O/W-type gel into an aluminum container;
Including,
The hydrolyzed sponge,
(i) washing the collected sponge and then drying it so that the moisture content is less than 10% by weight;
(ii) heating the dried sponge by immersing it in water at 90 to 100° C. for 10 to 40 minutes;
(iii) immersing the heated sponge in an acidic solution having a pH of 2 to 4 for 10 to 20 days;
(iv) separating the acidic solution from the solid content of the sponge, and then washing the solid content with water by repeating 2 to 5 times;
(v) immersing the washed solids in water and then washing them using ultrasonic waves;
(vi) after the ultrasonic cleaning is completed, immersing the sponge in a basic solution having a pH of 8 to 10 for 1 to 5 days;
(vii) separating the basic solution from the solid content, and then washing the solid content with water by repeating 2 to 5 times; And
(viii) immersing the washed solids in water and then washing them using ultrasonic waves;
It is manufactured by a manufacturing method comprising a,
The acidic solution is a mixture of one or more selected from the group containing lemon juice, citron juice, sugar citron juice, orange juice and vinegar,
The basic solution is
Separating the shells and then washing them;
Sintering the washed clam shells at a temperature of 800 to 1200°C;
Crushing the sintered shellfish shell;
Mixing the crushed clam shells with 1000 to 5000 parts by weight of water relative to 100 parts by weight of clam shells, and then leaving them for 2 to 10 days; And
Separating the solid content of the shellfish shell;
It is a solution prepared by a method containing,
The ultrasonic wave has a frequency of 20 to 130 kHz,
The hydrolyzed sponge contains 0.005 to 0.1 parts by weight based on 100 parts by weight of the solvent,
The natural-derived extract contains 0.1 to 5.0 parts by weight of white oyster mushroom extract and 0.01 to 5.0 parts by weight of olive leaf extract relative to 100 parts by weight of the solvent,
The natural-derived extract further comprises an extract of Sangbaekpi, Eoseongcho, Mokdanpi, or a mixture thereof,
The aromatic oil is a mixture of menthol and one or more extracts selected from the group of lavender, rosemary, eucalyptus, cypress, bergamot, sandalwood, rose, and lemon,
After the emulsification step is completed, a method for producing a cosmetic composition comprising a spicule extract, further comprising: mixing a thickener, a preservative, a pH adjuster, an antioxidant, an emulsifier, and an emulsifier.