KR102242148B1 - Manufacturing method of Selaginella tamariscina extract - Google Patents

Abstract

The present invention relates to a method for manufacturing a cosmetic raw material extract of Buddha, the washing step of washing the collected Buddha hand to remove foreign substances, the drying step of drying the washed Buddha hand, water and water of 40 ℃ to 70 ℃ dried in a container. After the addition, the first extraction step of producing a primary mixture by allowing the active ingredient to ooze out of the water for 12 hours in a state in which the budo-son was immersed in water, and heat was applied to the first mixture produced in the first extraction step. , By maintaining the temperature of the first mixture at 100°C for 30 minutes, a second extraction step of generating a second mixture through second extraction and sterilization, and introducing EM into the second mixture generated through the second extraction step , A fermentation step of generating a fermentation mixture by fermentation in the shade for a week, and the fermentation mixture generated through the fermentation step using at least one of filtration, sedimentation, flotation, and centrifugation, and included in the fermentation mixture. It characterized in that it comprises a; a post-treatment step of removing the buddha hand to finally prepare a buddha hand extract for cosmetic raw materials.

Description

A method for manufacturing a cosmetic raw material butcherson extract, and a cosmetic toner comprising the extract produced by the butcherson {Manufacturing method of Selaginella tamariscina extract}

The present invention relates to a method for preparing a bucheo-son extract and a cosmetic toner, and more particularly, to a method for preparing a bucheo-son extract for use as a cosmetic raw material, and to a cosmetic toner comprising the bucheo-son extract prepared therefrom.

Selaginella tamariscina is a fern that grows on sunny rocks in the mountainous region.It is sometimes called Gwonbaek (卷柏) from ancient times, and is a medicinal plant belonging to the Selaginellaceae family. , The scientific name is Selaginella tamariscina (P.Beauv.) Spring.

Buddha-son is almost evangelized in Korea, distributed in Japan, Taiwan, China, and Manchuria. It is an evergreen perennial plant growing on the surface of dry and cool rocks or cliffs, and has been used in oriental medicine to treat bloody stools, hematuria, and anal hernias. Recently, as blood sugar lowering has been known, interest in efficacy components is increasing.

As described in Korean Patent Registration No. 10-1353191, the above-described Buddha-son is mainly made of tea or pharmaceutical compositions and used to improve health functions by ingesting it by humans.In particular, leaves, stems, and roots are mainly used for medicinal purposes. .

On the other hand, as in Korean Patent Registration No. 10-0561036, some technologies using Buddhason as a raw material for cosmetics are being developed, but most of the technologies that simply include Buddhason as a raw material along with other raw materials are the most efficient extraction of active ingredients contained in Buddhason. There is little development of technology for a method of manufacturing the extract of Buchoson, which improves the functionality as a cosmetic raw material by improving it.

As described above, an object of the present invention is to provide a method for producing a cosmetic ingredient extract for improving the extraction efficiency of an active ingredient contained in a cosmetic ingredient so as to improve the functionality as a cosmetic ingredient.

The method for producing a cosmetic raw material extract according to the present invention includes a washing step of washing the collected buddha hand to remove foreign substances, a drying step of drying the washed buddha hand, and putting the dried water at 40°C to 70°C and the buddha hand in a container. After that, the first extraction step of producing a primary mixture by allowing active ingredients to ooze out of the water from the buddha-son for 12 hours while the budoe-son was immersed in water, by applying heat to the first mixture produced in the first extraction step, In the second extraction step of generating a second mixture through the second extraction and sterilization by maintaining the temperature of the first mixture at 100° C. for 30 minutes, EM is added to the second mixture generated through the second extraction step, A fermentation step in which a fermentation mixture is generated by fermentation in the shade for a week, and the fermentation mixture produced through the fermentation step are filtered, precipitated, suspended, and centrifuged. It characterized in that it comprises a post-treatment step of finally preparing the extract for cosmetic raw materials by removing the.

In addition, the first extraction step is characterized in that the dried bucheoson gradually increases the temperature of the water injected into the container from 40°C to 70°C.

In addition, the first extraction step is performed for a total of 12 hours, but for the first 7 hours, the water temperature is maintained at a temperature of 40°C to 50°C. It is characterized in that it is configured to gradually and gradually increase from ℃ to 70 ℃ soaking the Buddha and extracting the active ingredient at the same time.

In addition, the drying step is characterized in that it is configured to dry the washed Buddha hands at 65 ℃ to 70 ℃ 4 days through a drying device.

In addition, between the drying step and the first extraction step, it characterized in that it further comprises a pre-soaking step of immersing the dried Buddha hand in water of 40 ℃ or less for 24 hours.

The method of manufacturing a cosmetic raw material extract according to the present invention includes a washing step, a drying step, a first extraction step, a second extraction step, a fermentation step, and a post-treatment step, and the first extraction step is a 40° C. to 70° C. It is constructed so that the active ingredients are first poured into the water by putting it in water at °C and immersing it in water. At temperatures exceeding 70 °C, the buddha-son cannot be restored similarly to the state before drying, and as the Buddha-son itself is cooked, the external surface of the Buddha-son By curing, it is possible to solve the problem of lowering the extraction efficiency of the active ingredient as the active ingredient contained in the Buddha-son cannot be properly poured out into water due to the cured outer surface, thereby improving the extraction efficiency of the active ingredient contained in the Buddha-son. There is an effect that can be made.

Figure 1 is a flow chart showing a method for producing a cosmetic raw material bucheoson extract according to an embodiment of the present invention.
FIG. 2 shows a state before the injection of water into the container after the injection of bucheolson into the container in the first extraction step of the method of manufacturing the extract of the cosmetic raw material according to Preparation Example 1 and Comparative Example 1 of the present invention.
FIG. 3 is a first step of 10 minutes in a state in which water and Buddha hands are immersed in water by putting water and Buddha hands into a container in the first extraction step in the method of manufacturing the extract for cosmetic raw materials according to Preparation Example 1 and Comparative Example 1 of the present invention. It indicates the state in which extraction has been made.
Figure 4 shows a state in which the first extraction step is completed in the method for producing a cosmetic raw material extract according to Preparation Example 1 of the present invention.
Figure 5 shows a state in which the first extraction step is completed in the method for producing a cosmetic raw material extract according to Comparative Example 1 of the present invention.

Specific matters including the problems to be solved in the present invention as described above, solutions to the problems, and effects of the invention are included in the following examples and drawings. Advantages and features of the present invention, and a method of achieving them will become apparent with reference to the embodiments described below in detail together with the accompanying drawings.

In addition, when a part of the specification is said to “include” or “equipped” a certain element, this does not exclude other elements, but may further include or include other elements unless otherwise stated. Means that.

Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings. First, in adding reference numerals to elements of each drawing, it should be noted that the same elements are assigned the same numerals as possible even if they are indicated on different drawings. In addition, in describing the present invention, when it is determined that a detailed description of a related known configuration or function may obscure the subject matter of the present invention, the detailed description thereof will be omitted.

First of all, the present invention relates to a method for preparing a budo-son extract, and to a method for producing a budo-son extract to improve the extraction efficiency of the active ingredient contained in the budo-son, and to prepare a budo-son extract for use as a cosmetic raw material.

Figure 1 is a flow chart showing a method of manufacturing a cosmetic raw material extract bucheoson according to an embodiment of the present invention.

Referring to Figure 1, the method of manufacturing the extract for cosmetic raw materials according to an embodiment of the present invention is largely a washing step (S100), a drying step (S200), a first extraction step (S300), a second extraction step (S400), fermentation It includes a step (S500) and a post-processing step (S600).

1) First, the washing step (S100) is a step of removing foreign substances by washing the collected Buddha hand, and may be configured to remove foreign substances attached to the outside of the Buddha hand using water or air.

2) Next, the drying step (S200) is a step of drying the washed Buddha hands, and may be configured to dry naturally in shaded or sunny areas, or dried through a drying device.

The drying step (S200), for example, when drying the Buddha hand through a drying device, may be configured to dry the Buddha hand at 65° C. to 70° C. for 3 to 5 days, preferably for 4 days, which is 70 When drying the Buddha hand at a temperature exceeding ℃, there is a problem that not only the moisture contained in the Buddha hand is removed, but the active ingredients contained in the Buddha hand are destroyed or deteriorated. Drying time when drying the Buddha hand at a temperature below 65 ℃ There is a problem that the drying efficiency decreases due to the lengthening.

3) Next, the first extraction step (S300) is a step of immersing the dried Buddha hand in water through the drying step (S200), soaking the dried Buddha hand, and extracting the active ingredients contained in the Buddha hand at the same time. , After pouring water at 40°C to 70°C into a container, and the active ingredient oozes out of the water for 12 hours in the state that the Buddha is immersed in the water, a primary mixture may be formed, at this time. The first mixture generated through the first extraction step (S300) is composed of the Buddha hand put into the container, the water in which the Buddha hand is immersed, and the active ingredient from the Buddha hand in the first extraction step (S300).

At this time, at temperatures below 40°C, the soaking effect and the extracting effect of active ingredients cannot be sufficiently expressed, and at temperatures exceeding 70°C, the Buddha hands cannot be restored similarly to the state before drying, and the Buddha hands themselves are cooked. Accordingly, the external surface of the Buddha's hand is hardened, so that the active ingredient contained inside the Buddha's hand cannot be properly poured out into water due to the hardened outer surface, so that there is a problem in that the extraction efficiency of the active ingredient is lowered.

Therefore, in the first extraction step (S300) of the present invention, the extraction of the active ingredient from the first extraction process can be maximized by injecting the buchoson into water at 40°C to 70°C. There is an advantage.

On the other hand, the first extraction step (S300) is preferably configured to gradually gradually increase the temperature of the water immersed in the water while the first extraction is made from 40 ℃ to 70 ℃. More specifically, for the first 7 hours out of a total of 12 hours, the water temperature was maintained at a temperature of 40°C to 50°C to extract the active ingredient while soaking the water, and then gradually from 50°C to 70°C for the remaining 5 hours. It may be configured to increase slowly so as to soak the buddha-son and to improve the extraction efficiency of the active ingredient.

4) Next, in the second extraction step (S400), heat is applied to the first mixture generated in the first extraction step (S300) so that the temperature of the liquid contained in the first mixture is maintained at 100°C. It may be configured to produce a second mixture by sterilizing the first mixture at the same time while further secondary extraction is made from the Buchoson in a short time for minutes to 35 minutes, preferably 30 minutes, and the second mixture is configured to be produced. In this case, the secondary mixture generated through the secondary extraction step (S400) is the bucheo-son injected into the container, the water in which the bu-cheol-son is immersed, and through the first extraction step (S300) and the second extraction step (S400). It is composed of active ingredients derived from.

5) Next, the fermentation step (S500) is a step of fermenting the secondary mixture generated through the secondary extraction step (S400), and 1 part by weight of EM is added to 100 parts by weight of the secondary mixture for a week in the shade. It is configured to be fermented during the fermentation process to produce a fermentation mixture.

At this time, EM (Effective Micro-organisms) refers to a microbial complex obtained by combining and cultivating dozens of useful microorganisms used in food and medical fields among the numerous microorganisms in nature. Yeast, lactic acid bacteria, and photosynthetic bacteria This EM is a major species that makes up the EM, and when the secondary mixture is fermented through EM as described above, EM is made of natural materials that do not use synthetic chemicals, so it is eco-friendly and uses organic solvents such as ethanol. Compared to the case of fermentation, the extraction efficiency is also improved.

In addition, with respect to 100 parts by weight of the secondary mixture, if the amount of EM to be added is less than 1 part by weight, sufficient fermentation is difficult to achieve, and if the amount exceeds 1 part by weight, the fermentation efficiency improved compared to the amount of EM is insignificant and economical efficiency is lowered There is a problem.

6) Next, the post-treatment step (S600) is configured to remove the extracted and fermented budoeson from the fermentation mixture generated through the fermentation step (S500) to finally prepare a budoeson extract for cosmetic raw materials.

In this case, the method of removing the buchoson contained in the fermentation mixture may be configured to use at least one of filtration, sedimentation, flotation, and centrifugation.

Additionally, the method for manufacturing a cosmetic raw material extract according to the present invention may further include a pre-soaking step between the drying step (S200) and the first extraction step (S300) in the method for preparing a cosmetic ingredient extract as described above. have.

The pre-soaking step is a step for soaking the buddha hand dried through the drying step (S200) in water so that the buddha hand can be restored to the state before drying before the primary extraction was performed, and the buddha hand was immersed in water for 24 hours. It may be configured to be soaked, and at this time, it is preferable that the water into which the Buddha is immersed is made of 40° C. or less.

Figure 2 shows the state before the injection of water into the container after the first extraction step (S300) of the method for producing a cosmetic raw material bucheoson extract according to Preparation Example 1 and Comparative Example 1 of the present invention, FIG. 3 is a diagram illustrating a method for manufacturing an extract for a cosmetic raw material according to Preparation Example 1 and Comparative Example 1 of the present invention, in a state in which water and Buddha hand are put into a container in the first extraction step (S300), and the Buddha hand is immersed in the water. Figure 4 shows a state in which the primary extraction has been made for a minute, and Figure 4 shows a state in which the first extraction step (S300) is completed in the method for manufacturing a cosmetic raw material extract according to Preparation Example 1 of the present invention, and Figure 5 is a comparison of the present invention. In the method for manufacturing a cosmetic raw material extract according to Example 1, the first extraction step (S300) is completed.

With reference to FIGS. 2 to 5, a method of manufacturing a cosmetic raw material extract for a cosmetic ingredient according to Preparation Example 1 and Comparative Example 1 of the present invention will be described in more detail as follows.

(Production Example 1)

Preparation Example 1 was prepared in accordance with the method for producing a cosmetic raw material bucherson extract prepared according to the embodiment of the present invention. In more detail, the washing step (the collected Buddha hand was washed with water), the drying step (the washed Buddha hand was dried for 4 days in a temperature range of 65°C to 70°C through a drying device), and the first extraction step (container After adding 400ml of water and 50g of Buddhason, the temperature of the water is gradually increased from 40℃ to 50℃ for the first 7 hours and from 50℃ to 70℃ for the remaining 5 hours. At the same time, the active ingredient is extracted so that the first mixture is produced), the second extraction step (the generated first mixture is heated to 100°C for 30 minutes to generate a second mixture through additional extraction and sterilization), Fermentation step (injecting the EM stock solution prepared in a solution type into the second mixture, 1 part by weight of the EM stock solution is added to 100 parts by weight of the second mixture, and fermentation is performed for some days in the shade to create a fermentation mixture), post-treatment step (generating The resulting fermentation mixture was filtered through a net to remove the budo-son contained in the fermentation mixture to prepare a bud-cho-son extract). As a result, a bud-cho-son extract for cosmetic ingredients was prepared.

(Comparative Example 1)

In Comparative Example 1, in the method for preparing the extract of Bucheo-son as described in Preparation Example 1 above, a bucheo-son extract for cosmetic ingredients was prepared by varying only the temperature of the water in which the Bucheo-son was immersed in the first extraction step (S300), and the temperature of the water was Preparation Example 1 Unlike this, it was kept above 70℃.

First, in FIGS. 2 and 3, the right side of the two containers represents Preparation Example 1, and the left side represents Comparative Example 1,

Referring to FIG. 3, in a state in which water and Buddha hands are put into a container in the first extraction step (S300), and the first extraction is performed for 10 minutes in a state in which the Buddha hands are immersed in water, the Buddha hands are shown in Comparative Example 1 on the left. The soaking state and the active ingredient extraction state were better compared to the soaking state and the active ingredient extraction state of Preparation Example 1 shown on the right.

Referring to FIGS. 4 and 5, in the method for manufacturing a cosmetic raw material bucheo-son extract according to Preparation Example 1 of the present invention shown in FIG. 4, looking at a state in which the first extraction step (S300) is completed, the color of the bucheo-son is dried. Previously, it can be confirmed that it has a greenish color similar to the color of the original Buddha-son, and in the method for manufacturing a cosmetic raw material Buddha-son extract according to Comparative Example 1 of the present invention shown in FIG. 5, the first extraction step (S300) is completed. If you look at it, you can see the state that the color of the Buddha's hand has turned yellow,

As a result, it can be seen that when the temperature of the water in which the buddha-son is immersed in the first extraction step (S300) is maintained above 70°C, the nature and state of the bud-cheolson are altered.

(Production Example 2)

Preparation Example 2 is to prepare a toner using the extract of Bucheo-son prepared according to Preparation Example 1, and with respect to 100% by weight of the final produced toner, 80% by weight of the prepared cosmetic material extract of Bucheo-son, 3% by weight of elastin, Toner was prepared by adding 3% by weight of collagen, 3% by weight of ceramide, 3% by weight of hyaluronic acid, 5% by weight of aloe vera, and 3% by weight of a fragrance.

(Comparative Example 2)

In Comparative Example 2, a toner was prepared using the extract of Bucheomone prepared according to Comparative Example 1, and in the same manner as in Preparation Example 2, 80% by weight of the prepared cosmetic ingredient extract for 100% by weight of the toner was finally prepared. Wow, 3% by weight of elastin, 3% by weight of collagen, 3% by weight of ceramide, 3% by weight of hyaluronic acid, 5% by weight of aloe vera, and 3% by weight of a fragrance were added to prepare a toner.

(Experimental example)

In this experimental example, the usability evaluation was performed on the toners prepared through Preparation Example 2 and Comparative Example 2 above, and the usability evaluation of the toner was conducted on 20 women in their 10s to 40s. The people used the toner prepared according to Preparation Example 2 for a week, twice a day, and applied toner after washing their faces in the morning and evening, respectively, and the remaining 10 subjects of the second experimental group used the toner prepared according to Comparative Example 2 for a week, Twice a day, in the morning and in the evening, toner was applied after washing, respectively. At this time, the 1st and 2nd experimental groups included 5 people in their teens to 40s each.

After conducting the experiment as described above, a questionnaire survey on toner was conducted, and evaluation was conducted with a total of 5 points as the highest satisfaction level for each item, and the survey results are shown in the following table.

division Whitening Moisturizing Inflammation relief elasticity stimulus Manufacturing Example 2 2 4 4 One 2 Comparative Example 2 One 2 3 One 2

Referring to Table 1, when using the toner prepared according to Preparation Example 2, it can be confirmed that overall satisfaction is higher than that of Comparative Example 2, and in particular, it can be confirmed that satisfaction with inflammation relief and moisturizing is high. It can be seen that the bucheol-son extract produced by the method for manufacturing the bucheo-son extract for cosmetic raw materials according to the present invention has an effect of improving the functionality as a cosmetic raw material by improving the efficiency of extracting the active ingredient from the bucheo-son.

As described above, it will be appreciated that the above-described technical configuration of the present invention can be implemented in other specific forms without changing the technical spirit or essential features of the present invention by those skilled in the art.

Therefore, it should be understood that the above-described embodiments are illustrative and non-limiting in all respects, and the scope of the present invention is indicated by the claims to be described later rather than the detailed description, and the meaning and scope of the claims and their equivalents All changes or modifications derived from the concept should be construed as being included in the scope of the present invention.

S100: washing step
S200: drying step
S300: first extraction step
S400: second extraction step
S500: fermentation stage
S600: post-processing step

Claims (5)

A washing step of removing foreign substances by washing the collected Buddha hands;
A drying step of drying the washed Buddha hand;
After adding water and Buddha hand to the container, let the active ingredient ooze out of the water for 12 hours while the Buddha hand is immersed in the water, but the temperature of the water is maintained at a temperature of 40 ℃ to 50 ℃ for the first 7 hours, For the remaining 5 hours, the temperature of the water is gradually increased from 50 ℃ to 70 ℃, the first extraction step of extracting the active ingredient while soaking the hand to create a first mixture;
A second extraction step of generating a second mixture through secondary extraction and sterilization by applying heat to the first mixture generated in the first extraction step and maintaining the temperature of the first mixture at 100° C. for 30 minutes;
A fermentation step in which EM is added to the second mixture generated through the second extraction step, and fermented in the shade for a week to produce a fermentation mixture; And
A post-treatment step of filtering the fermentation mixture generated through the fermentation step to remove the budoeson contained in the fermentation mixture to finally prepare a budoeson extract for cosmetic raw materials; characterized in that it comprises a butcherson extract for cosmetic raw materials, comprising: Manufacturing method.
Including Buddhason extract, elastin, collagen, ceramide, hyaluronic acid, aloe vera, and fragrance,
The Buddha-son extract is
A washing step of washing the collected Buddha hands to remove foreign substances, and
A drying step of drying the washed Buddha hand,
After pouring water and dried Buddha-son into the container, let the active ingredients ooze out of the water from the Buddha-son during 12 o'clock while the Buddha-son is immersed in water, but keep the temperature of the water at a temperature of 40℃ to 50℃ for the first 7 hours. And, for the remaining 5 hours, the temperature of the water is gradually increased from 50° C. to 70° C., and the active ingredient is extracted while soaking the hand, and a first extraction step of producing a first mixture,
A second extraction step of generating a second mixture through secondary extraction and sterilization by applying heat to the first mixture generated in the first extraction step and maintaining the temperature of the first mixture at 100° C. for 30 minutes,
A fermentation step in which EM is added to the second mixture generated through the second extraction step, and fermented for a week in the shade to generate a fermentation mixture, and
A cosmetic toner produced by a manufacturing method comprising a post-treatment step of filtering the fermentation mixture generated through the fermentation step to remove the budoeson contained in the fermentation mixture to prepare a budoeson extract.
The method of claim 2,
Based on 100% by weight of the cosmetic toner
A cosmetic toner comprising 80% by weight of the Buddhason extract, 3% by weight of elastin, 3% by weight of collagen, 3% by weight of ceramide, 3% by weight of hyaluronic acid, 5% by weight of aloe vera, and 3% by weight of fragrance. delete delete

Images