KR102193375B1 - Cream-typed cleanzing compostion containing horse oil and method for preparing the same - Google Patents
Cream-typed cleanzing compostion containing horse oil and method for preparing the same Download PDFInfo
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Abstract
본 발명은 마유를 함유하는 크림 타입 클렌징 조성물 및 이를 제조하는 방법에 관한 것이다. 본 발명에 따른 크림 타입 클렌징 조성물은 정제된 마유, 미네랄 오일, 계면활성제, 보습제 및 향료를 함유하는 마유를 함유한다. 본 발명에 의하면, 마유 특유의 색감이 없으면서도 냄새가 나지 않는 마유를 함유하는 크림 타입의 클렌징 조성물이 생성된다. The present invention relates to a cream-type cleansing composition containing horse oil and a method of manufacturing the same. The cream-type cleansing composition according to the present invention contains horse oil containing refined horse oil, mineral oil, surfactant, moisturizer and fragrance. According to the present invention, a cream-type cleansing composition containing horse oil that does not emit an odor without having a unique color sense of horse oil is produced.
Description
본 발명은 마유를 함유하는 크림 타입 클렌징 조성물 및 이를 제조하는 방법에 관한 것이다. The present invention relates to a cream-type cleansing composition containing horse oil and a method of manufacturing the same.
보통 마지(horse fats)에서 분리된 마유(horse oil)는 많은 양의 불포화 지방산을 포함하고 있으며, 디엔(diene), 삼산(three acid)이 많아 피부의 침투성이 매우 우수하여 피부보호와 보습뿐만 아니라 혈관을 유연하게 하여 말초 혈액 순환 증가를 노화 방지 등 화장품의 이상적인 원료로 활용 될 수 있어 마유는 사람들에게 점점 주목 받고 있다.Horse oil, which is usually isolated from horse fats, contains a large amount of unsaturated fatty acids, and has excellent skin permeability due to its high levels of diene and three acids. Horse oil is getting more and more attention from people because it can be used as an ideal raw material for cosmetics, such as anti-aging, to increase peripheral blood circulation by making blood vessels flexible.
최근, 대한민국 특허공개 제10-2018-0101125호 (2018년09월12일 공개, 출원인 (주)유앤아이제주, 발명의 명칭 "마유 및 애기수영 추출물을 함유하는 피부 미백 및 주름 개선용 화장료 조성물")에서는 마유 추출물을 이용하여 미백 및 주름 개선용 화장료 조성물을 제안하였다. 이 공개특허문헌에서는 마유 외에도 아니라 애기수영 추출물도 함께 포함하고 있다.Recently, Korean Patent Publication No. 10-2018-0101125 (published on September 12, 2018, Applicant U&I Jeju, the name of the invention "a cosmetic composition for skin whitening and wrinkle improvement containing horse oil and baby swimming extract") In the following, a cosmetic composition for whitening and wrinkle improvement using horse oil extract was proposed. In this published patent document, in addition to horse oil, it also contains a baby swimming extract.
또한, 대한민국 특허공개 제10-2018-0101124호 (2018년09월12일, 출원인 (주)유앤아이제주, 발명의 명칭 "마유 및 새싹 추출물을 함유하는 피부 염증 개선용 화장료 조성물")에서는 마유 추출물과 새싹 추출물을 이용하여 피부 염증 개선용 화장료 조성물을 제안하였다.In addition, in Korean Patent Publication No. 10-2018-0101124 (September 12, 2018, Applicant U&I Jeju, the name of the invention "a cosmetic composition for improving skin inflammation containing horse oil and sprout extract"), horse oil extract and A cosmetic composition for improving skin inflammation was proposed using sprout extract.
이외에도, 대한민국 특허등록 제10-119114호 (2012.10.09 등록, 출원인 (주)리코리스, 발명의 명칭 "장딸기 열매 추출물 및 마유를 함유하는 피부 보호용 화장료 조성물")에서는 장딸기 열매 추출물과 마유를 이용하여 피부 보호용 화장료 조성물을 제안하였다.In addition, in Korean Patent Registration No. 10-119114 (registered on Oct. 9, 2012, Applicant Lycoris Co., Ltd., the name of the invention "a skin-protective cosmetic composition containing berry fruit extract and horse oil"), a berry fruit extract and horse oil are used. A cosmetic composition for skin protection was proposed.
그러나, 마유에는 특유의 냄새가 있어 실제로 화장료 조성물에 직접적으로 적용하는 것은 그리 쉬운 문제는 아니다. 또한, 마유는 특유의 색이 있어 다량으로 함유되는 경우에는 화장료 조성물의 전체적인 색감을 조정하기가 쉽지 않은 문제가 있다.However, since horse oil has a peculiar smell, it is not so easy to actually apply it directly to a cosmetic composition. In addition, horse oil has a unique color, so when it is contained in a large amount, it is difficult to adjust the overall color of the cosmetic composition.
본 발명은 종래기술의 문제점을 해결하기 위해 안출된 것으로, 본 발명의 목적은 마유 특유의 색감이 없으면서도 냄새가 나지 않는 마유를 함유하는 크림 타입의 클렌징 조성물 및 이의 제조 방법을 제공하는 데에 있다. The present invention was conceived to solve the problems of the prior art, and an object of the present invention is to provide a cream-type cleansing composition containing horse oil that does not have a peculiar color of horse oil and does not smell, and a method for manufacturing the same. .
상기 및 그 밖의 목적을 달성하기 위하여, 본 발명은,In order to achieve the above and other objects, the present invention,
정제된 마유, 미네랄 오일, 계면활성제, 보습제 및 향료를 함유하는 마유를 함유하는 크림 타입 클렌징 조성물을 제공한다. It provides a cream-type cleansing composition containing horse oil containing refined horse oil, mineral oil, surfactant, moisturizer and fragrance.
상기 정제된 마유는 조성물 총중량에 대하여 0.01 내지 10중량%의 양으로 함유되는 것을 특징으로 한다. The refined horse oil is characterized in that it is contained in an amount of 0.01 to 10% by weight based on the total weight of the composition.
상기 정제된 마유는 파파인을 통해 추출된 후 인산 용액을 정제된 것임을 특징으로 한다. The purified horse oil is characterized in that the phosphoric acid solution is purified after being extracted through papain.
본 발명은 또한 상기 크림 타입 클렌징 조성물은 파파인을 통해 추출된 후 인산 용액을 정제된 마유를 사용하는 것을 특징으로 하는 크림 타입 클렌징 조성물의 제조 방법을 제공한다. The present invention also provides a method for producing a cream-type cleansing composition, characterized in that the cream-type cleansing composition is extracted through papain and then a phosphoric acid solution is purified using horse oil.
본 발명에 의하면, 마유 특유의 색감이 없으면서도 냄새가 나지 않는 마유를 함유하는 크림 타입의 클렌징 조성물이 생성된다. According to the present invention, a cream-type cleansing composition containing horse oil that does not emit an odor without having a unique color sense of horse oil is produced.
도 1은 papain 처리 농도별 직후의 사진이다.
도 2는 농도별 papain 처리 및 incubator 24시간 반응 후의 사진이다.
도 3은 papain 처리 농도별 1h autoclave 반응 후의 사진이다.
도 4는 각 처리 공정 중의 사진이다.
도 5는 본 발명을 통해 생성된 마유 크림을 보여주는 사진이다.
도 6은 본 발명을 통해 획득한 마유 추출물을 보여주는 사진으로 좌측 사진이 본 발명을 통해 획득한 마유 추출물이고 우측 사진이 비교용 사진이다. 1 is a photograph immediately after papain treatment concentration.
2 is a photograph of papain treatment by concentration and reaction for 24 hours in an incubator.
3 is a photograph after 1h autoclave reaction according to papain treatment concentration.
4 is a photograph during each treatment process.
5 is a photograph showing the horse oil cream produced through the present invention.
6 is a picture showing the horse oil extract obtained through the present invention, the left picture is the horse oil extract obtained through the present invention, and the right picture is a picture for comparison.
이하, 본 발명은 첨부된 예시 도면 및 실시예를 참조하여 보다 상세하게 설명된다. 본 발명을 설명함에 있어서, 이미 공지된 기능 혹은 구성에 대한 설명은 본 발명의 요지를 명료하게 하기 위하여 생략하기로 한다. Hereinafter, the present invention will be described in more detail with reference to the accompanying exemplary drawings and examples. In describing the present invention, descriptions of functions or configurations already known will be omitted to clarify the subject matter of the present invention.
본 발명은 정제된 마유, 미네랄 오일, 계면활성제, 보습제 및 향료를 함유하는 마유를 함유하는 크림 타입 클렌징 조성물을 제공한다. 미네랄 오일, 계면활성제, 보습제 및 향료는 통상적인 성분이므로 이에 대한 설명은 생략하기로 한다. The present invention provides a cream-type cleansing composition containing horse oil containing refined horse oil, mineral oil, surfactant, moisturizer and fragrance. Mineral oils, surfactants, moisturizers, and fragrances are common ingredients, so descriptions thereof will be omitted.
본 발명에서 사용되는 정제된 마유는 조성물의 총중량에 대하여 0.01 내지 10중량%의 양으로 사용된다.The refined horse oil used in the present invention is used in an amount of 0.01 to 10% by weight based on the total weight of the composition.
본 발명에서 사용되는 정제된 마유는 하기의 공정을 통해 획득되며, 기본적으로 하기의 특성을 갖는다. The refined horse oil used in the present invention is obtained through the following process, and basically has the following characteristics.
추출 공정Extraction process
(1) 마유 추출(1) horse oil extraction
- 파파인을 이용한 마유 추출 최적화 농도 계산 실험-Optimized concentration calculation experiment for horse oil extraction using papain
1) papain의 최적 처리 농도를 결정하기 위하여 0.5g(지방 100%)의 말고기를 가위로 잘게 세분화한(15ml sample) 뒤 Papain을 생리식염수에 농도별(0%,0.2%,1%,5%,10%)로 희석 처리함1) To determine the optimal concentration of papain, 0.5g (100% fat) of horse meat was finely divided (15ml sample) with scissors, and Papain was added to physiological saline by concentration (0%, 0.2%, 1%, 5%). ,10%)
2) 효소액을 만들어 0.5g 말고기에 Papain 효소액을 1:1로 넣었음2) Enzyme solution was made and Papain enzyme solution was added 1:1 to 0.5g horse meat.
3) 효소처리한 말고기를 건조기(60℃)에서 24h동안 반응시킨 뒤 반응된 말고기를 Autoclave를 이용하여 121℃에서 1h동안 추출3) After reacting the enzyme-treated horse meat in a dryer (60℃) for 24h, the reacted horse meat is extracted for 1h at 121℃ using an autoclave.
4) 원심분리하여 지방층인 상등액을 새로운 tube로 옮겨 지방추출 수율을 계산하였음4) After centrifugation, the fat layer, the supernatant, was transferred to a new tube and the fat extraction yield was calculated.
- 파파인을 이용한 마유 추출 최적화 반응 시간 계산 실험-Optimized reaction time calculation experiment for horse oil extraction using papain
1) papain의 최적 처리 시간을 결정하기 위하여 0.5g(지방 100%)의 말고기를 가위로 잘게 세분화한(15ml sample) 뒤 Papain을 생리식염수에 녹여 5% Papain 효소액을 만들어 줌1) To determine the optimal processing time for papain, 0.5g (100% fat) horse meat was finely divided (15ml sample) with scissors, and then Papain was dissolved in physiological saline to make 5% Papain enzyme solution.
2) 0.5g 말고기에 5% Papain 효소액을 1:1(w/v)로 넣었주고 효소처리한 말고기를 배양기(60℃)에서 각각의 시간별로(0,5,12,24,36,48시간) 반응시킨 뒤 반응된 말고기를 Autoclave를 이용하여 121℃에서 1h동안 추출2) 5% Papain enzyme solution was added 1:1 (w/v) to 0.5g horse meat, and the enzyme-treated horse meat was placed in an incubator (60℃) for each hour (0,5,12,24,36,48 hours). ) After reacting, the reacted horse meat is extracted for 1 h at 121℃ using an Autoclave
3) 원심분리 하여 지방층인 상등액을 새로운 tube로 옮겨 지방추출 수율을 계산하였음3) After centrifugation, the fat layer, the supernatant, was transferred to a new tube and the fat extraction yield was calculated.
- 파파인을 이용한 마유 추출 최적화 반응 온도 계산 실험-Experiment for calculating reaction temperature for horse oil extraction optimization using papain
1) papain의 최적 처리 시간을 결정하기 위하여 0.5g(지방 100%)의 말고기를 가위로 잘게 세분화한(15ml sample) 뒤 Papain을 생리식염수에 녹여 5% Papain 효소액을 만들어 줌1) To determine the optimal processing time for papain, 0.5g (100% fat) horse meat was finely divided (15ml sample) with scissors, and then Papain was dissolved in physiological saline to make 5% Papain enzyme solution.
2) 0.5g 말고기에 5% Papain 효소액을 1:1(w/v)로 넣었주고 효소처리한 말고기를 배양기에서 각각의 온도별로 (30,40,50,60,70,80oC) 24시간동안 반응시킨 뒤 반응된 말고기를 Autoclave를 이용하여 121℃에서 1h동안 추출2) 5% Papain enzyme solution was added 1:1 (w/v) to 0.5g horse meat and reacted for 24 hours at each temperature (30,40,50,60,70,80oC) in the incubator. After making, the reacted horse meat is extracted for 1h at 121℃ using an autoclave.
3) 원심분리 하여 지방층인 상등액을 새로운 tube로 옮겨 지방추출 수율을 계산하였음3) After centrifugation, the fat layer, the supernatant, was transferred to a new tube and the fat extraction yield was calculated.
- 마유 추출 실험 결과-Horse oil extraction experiment result
- 본 실험은 말고기에서 마유의 추출량을 늘리기 위해 단백질 분해 효소인 파파인의 연육작용을 이용하였음. 말고기의 결합조직을 분해시켜 추출의 효율을 높이고자 최적의 파파인 처리 농도와 최적의 반응시간을 구하고자 하였음-This experiment used the softening action of papain, a proteolytic enzyme, to increase the amount of horse oil extracted from horse meat. In order to increase the extraction efficiency by decomposing the connective tissue of horse meat, an optimal papain treatment concentration and an optimal reaction time were sought
- 최적의 파파인의 농도는 5%이며 수율이 82.57%로 가장 높게 나왔으며 최적의 파파인 처리 시간은 24시간 반응으로 수율이 89.50%가 나왔음 최적의 파파인 반응온도는 60oC로 나왔음 -The optimum concentration of papain was 5% and the yield was the highest at 82.57%, and the optimum papain treatment time was 89.50% with a 24 hour reaction.The optimum papain reaction temperature was 60oC.
- 실험결과 최적의 파파인 처리 조건은 60oC에서 5%의 파파인을 24시간동안 반응하였을 시 추출 수율이 가장 좋았으며 추출 수율이 89.50%로 달성지표인 85%보다 높은 수치를 기록 달성 목표를 도달하였음-As a result of the experiment, the optimum papain treatment condition was that when 5% papain was reacted at 60oC for 24 hours, the extraction yield was the best, and the extraction yield was 89.50%, which was higher than the achievement indicator of 85%.
말 지방육으로부터 추출한 마유의 정제 과정The purification process of horse oil extracted from horse fat meat
-마유의 정제 및 여과-Purification and filtration of horse oil
1) 탈검: 추출한 마유 0.5g을 microtube에 넣은 뒤 85% 인산용액을 마유 중량 0.1% 만큼 첨가 하여 20분간 처리함 1) Degum: Put 0.5g of extracted horse oil into a microtube, add 85% phosphoric acid solution as much as 0.1% by weight of horse oil, and treat for 20 minutes
2) 수세: 70℃의 물로 충분히 수세하여줌 2) Washing: Wash with water at 70℃ sufficiently.
3) 탈산: 2.5% NaOH 상기 마유 중량만큼 첨가함 3) Deoxidation: 2.5% NaOH added by the weight of the horse oil
4) 수세: 70℃의 물로 충분히 수세함 4) Washing: Wash enough with 70℃ water
5) 탈수/색/취: 상기 마유 중량 5% 중량 산성백토 첨가함 5) Dehydration/color/odor: 5% by weight of the horse oil and acid clay added
6) 가열: 100℃, 교반 가열함 6) Heating: 100℃, stirring and heating
7) 여과: 0.45 ㎛ 필터 여과함 7) Filtration: Filtered with 0.45 μm filter
마유 정제 실험 결과Horse oil purification experiment results
- 본 실험은 말고기에서 추출한 마유의 불순물을 제거하기 위해 인산, NaOH, 산성백토를 처리하여 검질제거, 유리된 자방산의 제거, 수분제거 탈색을 수행하였음-In this experiment, phosphoric acid, NaOH, and acid clay were treated to remove impurities in horse oil extracted from horse meat to remove gum quality, remove free self-propagating acid, and remove moisture.
- 각각의 검질제거, 유리된 자방산의 제거, 수분제거 탈색을 수행하였을 시 수율이 계속 낮아지게 됨 따라서 본 실험을 통해 위 정제과정의 수율이 달성지표인 85%을 도달 할 수 있는지 알아보는 시험을 진행하였음. -When each of the gums removal, free self-propagating acid removal, and moisture removal and decolorization are performed, the yield continues to decrease. Therefore, through this experiment, a test to see if the yield of the above purification process can reach 85%, the achievement indicator. Proceeded.
- 실험결과 마유 정제 수율은 평균 85.16%로 달성지표인 85%을 도달하였다. -As a result of the experiment, the horse oil refining yield averaged 85.16%, reaching 85%, the achievement indicator.
이상에서는 본 발명의 바람직한 구체예를 참조하여 설명하였지만, 해당 기술분야의 숙련된 당업자라면 하기의 특허청구범위에 기재된 본 발명의 사상 및 영역으로부터 벗어나지 않는 범위 내에서 본 발명을 다양하게 수정 및 변경시킬 수 있음을 이해할 수 있을 것이다.Although the above has been described with reference to preferred embodiments of the present invention, those skilled in the art will be able to variously modify and change the present invention within the scope not departing from the spirit and scope of the present invention described in the following claims. You will understand that you can.
Claims (4)
상기 마유는
1) 파파인(papain)의 최적 처리 농도를 결정하기 위하여 0.5g(지방 100%)의 말고기를 가위로 잘게 세분화한 뒤 파파인(Papain)을 생리식염수에 농도별(0%,0.2%,1%,5%,10%)로 희석 처리하는 단계;
2) 효소액을 만들어 0.5g 말고기에 파파인(Papain) 효소액을 1:1로 넣는 단계; 및
3) 효소처리한 말고기를 건조기에서 60℃의 조건하에 24h동안 반응시킨 뒤 반응된 말고기를 오토클레이브를 이용하여 121℃에서 1 시간 동안 추출하는 단계로부터 얻어진 마유인 것을 특징으로 하는 크림 타입 클렌징 조성물을 제조하는 방법. In the method for preparing a cream-type cleansing composition containing horse oil extracted through papain and then purified from a phosphoric acid solution in an amount of 0.01 to 10% by weight based on the total weight of the composition, and the remaining mineral oil, surfactant, moisturizer, and fragrance ,
The horse oil is
1) To determine the optimal concentration of papain, 0.5g (100% fat) of horse meat was finely divided with scissors, and papain was added to physiological saline by concentration (0%, 0.2%, 1%, 5%, 10%) dilution treatment;
2) making an enzyme solution and adding papain enzyme solution 1:1 to 0.5g horse meat; And
3) A cream-type cleansing composition characterized in that it is horse oil obtained from the step of reacting the enzyme-treated horse meat in a dryer under conditions of 60°C for 24 hours and then extracting the reacted horse meat at 121°C for 1 hour using an autoclave. How to manufacture.
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