CN101721330A - Preparation method of cucumber oil - Google Patents
Preparation method of cucumber oil Download PDFInfo
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- CN101721330A CN101721330A CN200810046383A CN200810046383A CN101721330A CN 101721330 A CN101721330 A CN 101721330A CN 200810046383 A CN200810046383 A CN 200810046383A CN 200810046383 A CN200810046383 A CN 200810046383A CN 101721330 A CN101721330 A CN 101721330A
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Abstract
The invention discloses a preparation method of cucumber oil and comprises the following steps: washing-crushing-distillation-mixing diethyl ether-separation-mixing muriatic acid-washing-dehydration.The cucumber oil can effectively improve nutrient condition of skin, treat skin inflammation and features good beautifying effect.
Description
Technical field
The present invention relates to a kind of preparation method of Fructus Cucumidis sativi oil.
Background technology
Along with improving constantly of living standards of the people, looks improving and the skin nourishing has become fashion pursuit in, but present beauty treatment, cosmetic product all are synthetics mostly, even some of them also contain harmful material, in addition, for guaranteeing its certain use, resting period, add materials such as some preservatives toward the contact meeting, therefore, natural cosmetics are subjected to people's favor.And in the prior art, utilizing Fructus Cucumidis sativi beauty treatment, skin Caring is a kind of traditional beauty method, Fructus Cucumidis sativi can play the effect of moistening reply, smash Fructus Cucumidis sativi to pieces pulping and can also treat skin burn, but these all are the elementary uses to natural materials, lack the deep processing means, give full play to its effect, make it reach better result of use.
Summary of the invention
The objective of the invention is to overcome above-mentioned technological deficiency, a kind of preparation method of Fructus Cucumidis sativi oil is provided.The present invention effectively improves the skin-nourishing situation, the treatment scytitis, and cosmetic result is good.
For achieving the above object, the technical solution used in the present invention is:
The preparation method of Fructus Cucumidis sativi oil is characterized in that: make by following step;
Once filter in A, the bag of packing into after Fructus Cucumidis sativi cleaned, smashs to pieces, obtain first-time filtrate, the disintegrating slag after will filtering is again worn into slurry, and slurry is carried out secondary filter, obtains secondary filtrate;
B, put into boiler after will first and second filtrate mixing, feed steam distillation, collect distillate, add isopyknic ether, leave standstill after jolting 25-35 minute, make its abundant layering after, emit lower floor's water;
C, the water in the B step added behind isopyknic ether again leaves standstill after jolting 25-35 minute, make its abundant layering after, emit lower floor's water again;
D, twice ether used heating in water bath mutually, ether is reclaimed in the decompression back, and the residual liquid reheat is to 40-45 ℃, under slowly stirring, add the 4-6% sodium hydroxide, make its pH value=8, and continue slowly to stir 18-22 minute, leave standstill once more and make its abundant layering, aqueous phase discarded keeps oil phase;
E, D step gained oil phase is heated to 50-55 ℃ after, under slowly stirring, add 1-3% hydrochloric acid, make its pH value=7, after continuing to stir 18-22 minute, left standstill 24 hours, aqueous phase discarded obtains oil phase;
F, with the E step oil phase 60 ℃, the washing of 2% sodium chloride solution 2 times, behind 60 ℃ of deionized water wash of reuse 2 times, leave standstill and make its abundant layering, aqueous phase discarded with oil phase vacuum dehydration, obtains finished product.
The invention has the advantages that:
After Fructus Cucumidis sativi oil and the contact skin, can expand blood capillary, accelerate blood circulation, promote the skin metabolism effect, improve the skin-nourishing state, make skin delicate and lubricated.The present invention has and prevents skin tanning, prevention pachylosis, moistens and beautify the effect of skin, and can eliminate acne, freckle, senile plaque and scytitis, can also improve the gloss and the flexibility of hair.
Description of drawings:
Fig. 1 is a process chart of the present invention.
The specific embodiment
Embodiment 1:
The preparation method of Fructus Cucumidis sativi oil is characterized in that: make by following step;
Once filter in A, the bag of packing into after Fructus Cucumidis sativi cleaned, smashs to pieces, obtain first-time filtrate, the disintegrating slag after will filtering is again worn into slurry, and slurry is carried out secondary filter, obtains secondary filtrate;
B, put into boiler after will first and second filtrate mixing, and feed steam distillation, and collect distillate, and add isopyknic ether, jolting was left standstill after 25 minutes, make its abundant layering after, emit lower floor's water;
C, the water in the B step added isopyknic ether again after jolting leave standstill after 25 minutes, make its abundant layering after, emit lower floor's water again;
D, twice ether used heating in water bath mutually, ether is reclaimed in the decompression back, and residual liquid reheat to 40 ℃ adds 4% sodium hydroxide under slowly stirring, make its pH value=8, and continue slowly to stir 18 minutes, leaves standstill once more and makes its abundant layering, and aqueous phase discarded keeps oil phase;
E, D step gained oil phase is heated to 50 ℃ after, under slowly stirring, add 1% hydrochloric acid, make its pH value=7, after continuing to stir 18 minutes, left standstill 24 hours, aqueous phase discarded obtains oil phase;
F, with the E step oil phase 60 ℃, the washing of 2% sodium chloride solution 2 times, behind 60 ℃ of deionized water wash of reuse 2 times, leave standstill and make its abundant layering, aqueous phase discarded with oil phase vacuum dehydration, obtains finished product.
After Fructus Cucumidis sativi oil and the contact skin, can expand blood capillary, accelerate blood circulation, promote the skin metabolism effect, improve the skin-nourishing state, make skin delicate and lubricated.The present invention has and prevents skin tanning, prevention pachylosis, moistens and beautify the effect of skin, and can eliminate acne, freckle, senile plaque and scytitis, can also improve the gloss and the flexibility of hair.
Embodiment 2:
The preparation method of Fructus Cucumidis sativi oil is characterized in that: make by following step;
Once filter in A, the bag of packing into after Fructus Cucumidis sativi cleaned, smashs to pieces, obtain first-time filtrate, the disintegrating slag after will filtering is again worn into slurry, and slurry is carried out secondary filter, obtains secondary filtrate;
B, put into boiler after will first and second filtrate mixing, and feed steam distillation, and collect distillate, and add isopyknic ether, jolting was left standstill after 35 minutes, make its abundant layering after, emit lower floor's water;
C, the water in the B step added isopyknic ether again after jolting leave standstill after 35 minutes, make its abundant layering after, emit lower floor's water again;
D, twice ether used heating in water bath mutually, ether is reclaimed in the decompression back, and residual liquid reheat to 45 ℃ adds 6% sodium hydroxide under slowly stirring, make its pH value=8, and continue slowly to stir 22 minutes, leaves standstill once more and makes its abundant layering, and aqueous phase discarded keeps oil phase;
E, D step gained oil phase is heated to 55 ℃ after, under slowly stirring, add 3% hydrochloric acid, make its pH value=7, after continuing to stir 22 minutes, left standstill 24 hours, aqueous phase discarded obtains oil phase;
F, with the E step oil phase 60 ℃, the washing of 2% sodium chloride solution 2 times, behind 60 ℃ of deionized water wash of reuse 2 times, leave standstill and make its abundant layering, aqueous phase discarded with oil phase vacuum dehydration, obtains finished product.
Embodiment 3:
The preparation method of Fructus Cucumidis sativi oil is characterized in that: make by following step;
Once filter in A, the bag of packing into after Fructus Cucumidis sativi cleaned, smashs to pieces, obtain first-time filtrate, the disintegrating slag after will filtering is again worn into slurry, and slurry is carried out secondary filter, obtains secondary filtrate;
B, put into boiler after will first and second filtrate mixing, and feed steam distillation, and collect distillate, and add isopyknic ether, jolting was left standstill after 30 minutes, make its abundant layering after, emit lower floor's water;
C, the water in the B step added isopyknic ether again after jolting leave standstill after 30 minutes, make its abundant layering after, emit lower floor's water again;
D, twice ether used heating in water bath mutually, ether is reclaimed in the decompression back, and residual liquid reheat to 40 ℃ adds 5% sodium hydroxide under slowly stirring, make its pH value=8, and continue slowly to stir 20 minutes, leaves standstill once more and makes its abundant layering, and aqueous phase discarded keeps oil phase;
E, D step gained oil phase is heated to 50 ℃ after, under slowly stirring, add 2% hydrochloric acid, make its pH value=7, after continuing to stir 20 minutes, left standstill 24 hours, aqueous phase discarded obtains oil phase;
F, with the E step oil phase 60 ℃, the washing of 2% sodium chloride solution 2 times, behind 60 ℃ of deionized water wash of reuse 2 times, leave standstill and make its abundant layering, aqueous phase discarded with oil phase vacuum dehydration, obtains finished product.
Claims (1)
1. the preparation method of Fructus Cucumidis sativi oil is characterized in that: make by following step;
Once filter in A, the bag of packing into after Fructus Cucumidis sativi cleaned, smashs to pieces, obtain first-time filtrate, the disintegrating slag after will filtering is again worn into slurry, and slurry is carried out secondary filter, obtains secondary filtrate;
B, put into boiler after will first and second filtrate mixing, feed steam distillation, collect distillate, add isopyknic ether, leave standstill after jolting 25-35 minute, make its abundant layering after, emit lower floor's water;
C, the water in the B step added behind isopyknic ether again leaves standstill after jolting 25-35 minute, make its abundant layering after, emit lower floor's water again;
D, twice ether used heating in water bath mutually, ether is reclaimed in the decompression back, and the residual liquid reheat is to 40-45 ℃, under slowly stirring, add the 4-6% sodium hydroxide, make its pH value=8, and continue slowly to stir 18-22 minute, leave standstill once more and make its abundant layering, aqueous phase discarded keeps oil phase;
E, D step gained oil phase is heated to 50-55 ℃ after, under slowly stirring, add 1-3% hydrochloric acid, make its pH value=7, after continuing to stir 18-22 minute, left standstill 24 hours, aqueous phase discarded obtains oil phase;
F, with the E step oil phase 60 ℃, the washing of 2% sodium chloride solution 2 times, behind 60 ℃ of deionized water wash of reuse 2 times, leave standstill and make its abundant layering, aqueous phase discarded with oil phase vacuum dehydration, obtains finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200810046383A CN101721330A (en) | 2008-10-27 | 2008-10-27 | Preparation method of cucumber oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200810046383A CN101721330A (en) | 2008-10-27 | 2008-10-27 | Preparation method of cucumber oil |
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| CN101721330A true CN101721330A (en) | 2010-06-09 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN200810046383A Pending CN101721330A (en) | 2008-10-27 | 2008-10-27 | Preparation method of cucumber oil |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106420573A (en) * | 2016-11-09 | 2017-02-22 | 芜湖智美网络科技有限公司 | Formula and using method of cucumber essential oil with effects of whitening and skin caring |
| CN108424811A (en) * | 2018-04-03 | 2018-08-21 | 青岛科技大学 | A kind of method of refined walnut oil smell removal |
-
2008
- 2008-10-27 CN CN200810046383A patent/CN101721330A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106420573A (en) * | 2016-11-09 | 2017-02-22 | 芜湖智美网络科技有限公司 | Formula and using method of cucumber essential oil with effects of whitening and skin caring |
| CN108424811A (en) * | 2018-04-03 | 2018-08-21 | 青岛科技大学 | A kind of method of refined walnut oil smell removal |
| CN108424811B (en) * | 2018-04-03 | 2021-06-18 | 青岛科技大学 | Method for removing odor of refined walnut oil |
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Open date: 20100609 |