KR102079650B1 - Composition of fig concentrate comprising an extract of ivy trees - Google Patents
Composition of fig concentrate comprising an extract of ivy trees Download PDFInfo
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- KR102079650B1 KR102079650B1 KR1020190085464A KR20190085464A KR102079650B1 KR 102079650 B1 KR102079650 B1 KR 102079650B1 KR 1020190085464 A KR1020190085464 A KR 1020190085464A KR 20190085464 A KR20190085464 A KR 20190085464A KR 102079650 B1 KR102079650 B1 KR 102079650B1
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/30—Artificial sweetening agents
- A23L27/33—Artificial sweetening agents containing sugars or derivatives
- A23L27/35—Starch hydrolysates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/14—Extraction
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Molecular Biology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Botany (AREA)
- Mycology (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
Description
본 발명은 황칠 추출물을 포함하는 무화과 농축액 조성물에 관한 것이다.The present invention relates to a fig concentrate composition comprising the yellow lacquer extract.
무화과는 아시아 서부 및 지중해 연안이 원산지인 아열대성의 반교목성 낙엽활엽수로 뽕나무과(Moraceae)에 속하는 식물이며, 알칼리성 식품으로서 고대 이집트와 로마, 이스라엘에서는 강장제나 암, 간장병 등을 치료하는 약으로 사용하였다. 동양의학에서는 무화과를 소화불량, 변비, 설사, 각혈, 신경통, 피부질환, 빈혈, 부인병 등에 약으로 쓰였으며, 그 잎은 치질에서 오는 종창 등에 사용한다. 우리나라의 동의보감과 민간요법에서는 설사, 각혈, 위통 피부질환과 부인병, 빈혈 등에 좋은 것으로 알려져 있다. 무화과는 약 10% 정도의 당분(포도당과 과당)이 함유되어 있어 당도가 높으며, 사과산과 구연산과 같은 유기산을 포함하고 있으며, 각종 무기질을 주요 성분으로 포함하고 있다.Fig is a subtropical semi-arictic deciduous tree native to western Asia and the Mediterranean, and belongs to Moraceae. It is an alkaline food used in ancient Egypt, Rome, and Israel to treat tonic, cancer, and liver disease. In oriental medicine, figs are used for medicines such as indigestion, constipation, diarrhea, keratin, neuralgia, skin diseases, anemia, and gynecological diseases. The leaves are used for swelling from hemorrhoids. In Korea, consent and folk remedies are known to be good for diarrhea, blood loss, stomach pain, skin diseases, women's diseases, and anemia. Figs contain about 10% of sugar (glucose and fructose) and have high sugar content. They contain organic acids such as malic acid and citric acid and various minerals as main ingredients.
무화과는 열량이 적고 비타민을 다량 함유하고 있기 때문에 여성들의 다이어트와 피부미용에도 효과가 있다. 무화과에 다량 함유되어 있는 비타민 C는 피부 색소인 멜라닌을 탈색시키고 색소 세포 활성 호르몬을 억제하는 미백효과가 있으며, 비타민 B2는 자외선에 대한 저항력을 키워준다. 단백질 분해 효소인 피신(ficin)은 소화작용 을 돕고 변비, 장염, 치질, 부스럼 등을 예방하며, 조리에서는 연육 효소로도 이용된다. 또한, 무화과는 지방과 콜레스테롤이 거의 함유되어 있지 않은 과실로서 다른 과일보다 섬유소의 함유량이 많아 혈중 콜레스테롤의 저하에 따른 심장질환 및 비만치료 효과가 보고되고 있다. 무화과열매 이외에도 무화과가지에는 프소릴렌, 베로갑텐, 아즐렌등의 성분이 함유되어 있으며, 무화과잎은 알칼로이드, 사포닌, 플라보노이드(루틴), 고무질, 수지, 비타민C, 정유등이 함유되어 있다.Figs are low in calories and contain a lot of vitamins, so it is effective for women's diet and skin care. Vitamin C, which is contained in large amounts in figs, has a whitening effect that decolorizes melanin, a skin pigment, and inhibits pigment cell activating hormone. Vitamin B2 increases resistance to ultraviolet rays. Pycin (ficin), a proteolytic enzyme, helps digestion and prevents constipation, enteritis, hemorrhoids, and swelling. It is also used as a meat enzyme in cooking. In addition, figs are fruits that contain little fat and cholesterol, and are higher in fiber than other fruits, and the effects of heart disease and obesity have been reported due to the decrease in blood cholesterol. In addition to fig fruits, fig branches contain constituents such as psorelene, verogatten, and azlene, and fig leaves contain alkaloids, saponins, flavonoids (rutin), gums, resins, vitamin C, and essential oils.
무화과의 경우, 열매의 맛과 당도, 기능성이 매우 높음에도 불구하고, 저장성과 가공성이 다양하지 않아, 그 활용도가 높지 않으며, 무화과잎과 무화과가지를 무화과열매와 혼합하여 가공된 식품을 제조하기에는 무화과잎 특유의 쓰고 역겨운 맛으로 인하여 가공된 식품을 소비자가 취식하는 경우에 심한 취식거부감을 일으키는 문제로 활용성이 높지 않은 문제가 있다.In the case of figs, despite the extremely high taste, sweetness, and functionality of the fruit, the storage and processability are not varied, and their utilization is not high, and the fig leaves and fig branches are mixed with the fig fruit to prepare the processed food Due to the unique bitter and disgusting taste of the leaves, when the consumer eats processed foods, there is a problem of not having high utility as a problem causing severe eating rejection.
한편 황칠나무는 최대 높이 15 m에 달하는 두릅나무과 나무로, 만병통치 나무라는 뜻의 학명 덴드로 파낙스 (Dendropanax morbifera Nakai)를 가지고 있을 정도로 그 약리학적 효능이 매우 뛰어난 약용식물이다. 한국에서만 서식하며, 한국에서도 난대림이 펼쳐진 한반도 남해 도서지역과 해안지역, 특히 해남, 완도 등 서남해안에서 생산되는 것으로 상당히 귀한 약용식물이다.Hwangchil-tree is a medicinal plant with a very high pharmacological effect, which has a dendritic tree (Dendropanax morbifera Nakai) which means a panacea tree up to 15 m high. Inhabited only in Korea, it is a rare medicinal plant that is produced in the South Sea island region and coastal areas, especially in the southwestern coast of Haenam and Wando, where the Nandae Forest is spread.
황칠나무의 껍질에 상처를 내면 노란 액체가 흘러나오는데, 이것을 황칠(黃漆)이라고 하며 오래 전부터 가구의 도료로 사용하였으나, 최근의 연구 결과에 따르면 항암 효과, 간세포 재생, 당뇨 치료, 경조직 세포 재생 등에 효과적인 것으로 밝혀졌다.When the bark of the Hwangchil tree is wounded, yellow liquid flows out, which is called Hwangchil (黄 漆) and has been used as a paint for a long time. According to recent studies, anti-cancer effects, liver cell regeneration, diabetes treatment, hard tissue cell regeneration, etc. It has been found to be effective.
황칠은 금칠이란 도료적 기능, 안식향으로서의 아로마 기능, 열을 내리고 독을 없애며 경기, 중풍, 더위 먹은데 효과를 발휘하는 약재로서의 기능을 갖는다.Hwangchil has the function of paint, which is a medicinal function that acts as a paint function, aroma function as a benzoate, to reduce heat and toxins, and to play an effect on game, stroke and heat.
다만 황칠의 경우, 그 기능성은 매우 높으나 섭취시 쓴 맛이 강하여 소비자가 황칠성분의 추출액을 섭취하는데에 불편감을 호소하는 경우가 많으며, 이에 식품이나 기능성 식품 조성물의 활용성은 매우 낮은 문제가 있다.However, in the case of hwangchil, the functionality is very high, but the bitter taste at the time of ingestion, the consumer often complains of inconvenience in ingesting the extract of the hwangchil component, there is a problem that the utilization of food or functional food composition is very low.
이에, 상기와 같이 약리학적 효능이 우수한 무화과 농축액과 황칠나무 추출물을 식품 조성물로서 개발하는 방법에 대한 요구가 높아지고 있다.Therefore, there is a growing demand for a method of developing a fig concentrate and an extract of Hwangchil-tree as a food composition having excellent pharmacological effects as described above.
본 발명은 상기와 같은 종래 기술상의 필요성을 해결하기 위해 안출된 것으로, 황칠 추출물을 포함하는 무화과 농축액 조성물을 제공하는 것을 그 목적으로 한다. The present invention has been made to solve the prior art needs as described above, and an object of the present invention is to provide a fig concentrate composition comprising a yellow lacquer extract.
그러나 본 발명이 이루고자 하는 기술적 과제는 이상에서 언급한 과제에 제한되지 않으며, 언급되지 않은 또 다른 과제들은 아래의 기재로부터 당업자에게 명확하게 이해될 수 있을 것이다.However, the technical problem to be achieved by the present invention is not limited to the above-mentioned problem, another task that is not mentioned will be clearly understood by those skilled in the art from the following description.
본 발명은 무화과 농축액 및 황칠나무 추출물을 포함하는, 건강기능 식품용 조성물을 제공한다.The present invention provides a dietary supplement composition comprising a fig concentrate and a yellow chile extract.
본 발명의 일 구현예로, 상기 조성물은,In one embodiment of the present invention, the composition,
무화과 잎 5~10 중량%, 무화과 가지 5~10중량%, 무화과 열매 30~35 중량%, 꿀 5~10중량%, 물엿 5~10중량%, 및 설탕 30~35중량%를 1차 농축후 숙성하는 단계(S1);Fig. 5-10 wt% of fig leaves, 5-10 wt% of fig branches, 30-35 wt% of fig fruits, 5-10 wt% of honey, 5-10 wt% of starch syrup, and 30-35 wt% of sugar Aging step (S1);
상기 S1단계에서 숙성후, 필터에 걸러 무화과 농축액을 추출하는 단계(S2);After aging in step S1, the step of extracting the fig concentrate by filtering the filter (S2);
상기 무화과 농축액 총 100 중량부 중 40 중량부를 분리하여, 황칠나무 추출물과 혼합하는 단계(S3);Separating 40 parts by weight of the total 100 parts by weight of the fig concentrate, and mixing with the Hwangchil wood extract (S3);
상기 S3 단계에서 분리하고 남은 무화과 농축액을 2차 숙성하여 2차 숙성액을 제조하는 단계(S4);Preparing a secondary aging solution by secondary aging of the remaining fig concentrate separated in step S3 (S4);
상기 S4 단계의 2차 숙성액 총 60 중량부 중 40 중량부를 분리하여, 황칠나무 추출물과 혼합하는 단계(S5);Separating 40 parts by weight of the total 60 parts by weight of the secondary aging solution of the step S4, and mixing the extract with Hilchi chile (S5);
상기 S5 단계에서 분리하고 남은 2차 숙성액을 3차 숙성하여 3차 숙성액을 제조하는 단계(S6);Preparing a third aging solution by terminating the second aging solution remaining in the step S5 and tertiary aging solution (S6);
상기 S6 단계의 3차 숙성액을 황칠나무 추출물과 혼합하는 단계(S7); 및Mixing the third aging solution of the step S6 with Hwangchil-tree extract (S7); And
상기 S3, S5, 및 S7단계에서 황칠나무 추출물과 혼합된 혼합액을 혼합하는 단계(S8)를 포함하는 제조방법으로 제조된 것을 특징으로 한다.Characterized in that the manufacturing method comprising the step (S8) of mixing the mixed solution mixed with the hwangchil wood extract in the steps S3, S5, and S7.
본 발명의 다른 구현예로, 상기 황칠나무 추출물은 70% 에탄올로 추출된 것을 특징으로 한다.In another embodiment of the present invention, the hwangchil wood extract is characterized in that extracted with 70% ethanol.
본 발명의 조성물은, 무화과의 열매의 고농축 엑기스를 추출하여 농축하는 농축공정을 통해 고당도 및 고농도의 농축액에 무화과 잎과 가지의 성분을 가미하여 기능성을 높이고, 황칠 추출물을 가미하여 무화과 나무의 유익한 성분과 황칠의 성분을 동시에 섭취할 수 있도록 하는 기능성 조성물에 관한 것으로, 소비자의 기호도를 높여 다양한 제품에 응용이 가능할 수 있도록 구현할 수 있다.The composition of the present invention, through the concentration process of extracting and concentrating the high concentration extract of the fruit of the fig to add the components of the fig leaf and eggplant to the high-concentration and high concentration of the concentrate to increase the functionality, the addition of the hwangchil extract beneficial to the fig tree The present invention relates to a functional composition for ingesting a component and a component of a yellow lacquer at the same time, and may be implemented to be applicable to various products by increasing consumer preference.
도 1은 본 발명의 제조방법을 모식화하여 나타낸 도면이다.1 is a view schematically showing the manufacturing method of the present invention.
본 발명자들은 우수한 기능성을 가짐에도 불구하고 특유의 맛에 의해 취식 거부감이 있는 무화과 농축액과 황칠나무 추출물을 포함하는 식품 조성물을 제공하고자 노력한 결과, 무화과 열매의 고당도의 성분을 강화하는 고농축 무화과 액기스의 숙성액에 황칠나무 추출물을 순차적으로 혼합하는 방법을 통해, 무화과 액기스와 황칠의 섭취 거부감을 제거하고, 기능성을 그대로 보유할 수 있는 혼합 조성물을 제조할 수 있다는 것을 확인하여 본 발명을 완성하였다.The inventors of the present invention have tried to provide a food composition comprising a fig concentrate and an extract of yellow chile which have an objectionable taste due to its unique taste despite the excellent functionality of the highly concentrated fig extract that enhances the high sugar content of the fig fruit. Through the method of sequentially mixing the extract of the yellow lacquer tree in the aging solution, it was confirmed that the mixed composition that can retain the intake rejection of the fig extract and the yellow lacquer can be prepared as it is to complete the present invention.
이에, 본 발명은 무화과 농축액 및 황칠나무 추출물을 포함하는, 건강기능 식품용 조성물을 제공한다.Accordingly, the present invention provides a dietary supplement composition comprising a fig concentrate and a yellow chile extract.
본 발명의 식품용 조성물은 무화과 농축액 및 황칠나무 추출물을 포함하는 것으로, 상기 조성물은,The food composition of the present invention comprises a fig concentrate and an extract of Hwangchil, wherein the composition is
무화과 잎 5~10 중량%, 무화과 가지 5~10중량%, 무화과 열매 30~35 중량%, 꿀 5~10중량%, 물엿 5~10중량%, 및 설탕 30~35중량%를 1차 농축후 숙성하는 단계(S1);Fig. 5-10 wt% of fig leaves, 5-10 wt% of fig branches, 30-35 wt% of fig fruits, 5-10 wt% of honey, 5-10 wt% of starch syrup, and 30-35 wt% of sugar Aging step (S1);
상기 S1단계에서 숙성후, 필터에 걸러 무화과 농축액을 추출하는 단계(S2);After aging in step S1, the step of extracting the fig concentrate by filtering the filter (S2);
상기 무화과 농축액 총 100 중량부 중 40 중량부를 분리하여, 황칠나무 추출물과 혼합하는 단계(S3);Separating 40 parts by weight of the total 100 parts by weight of the fig concentrate, and mixing with the Hwangchil wood extract (S3);
상기 S3 단계에서 분리하고 남은 무화과 농축액을 2차 숙성하여 2차 숙성액을 제조하는 단계(S4);Preparing a secondary aging solution by secondary aging of the remaining fig concentrate separated in step S3 (S4);
상기 S4 단계의 2차 숙성액 총 60 중량부 중 40 중량부를 분리하여, 황칠나무 추출물과 혼합하는 단계(S5);Separating 40 parts by weight of the total 60 parts by weight of the secondary aging solution of the step S4, and mixing the extract with Hilchi chile (S5);
상기 S5 단계에서 분리하고 남은 2차 숙성액을 3차 숙성하여 3차 숙성액을 제조하는 단계(S6);Preparing a third aging solution by terminating the second aging solution remaining in the step S5 and tertiary aging solution (S6);
상기 S6 단계의 3차 숙성액을 황칠나무 추출물과 혼합하는 단계(S7); 및Mixing the third aging solution of the step S6 with Hwangchil-tree extract (S7); And
상기 S3, S5, 및 S7단계에서 황칠나무 추출물과 혼합된 혼합액을 혼합하는 단계(S8)를 포함하는 제조방법으로 제조된 것이다.S3, S5, and S7 are prepared by the manufacturing method comprising the step (S8) of mixing the mixed solution mixed with the extract from the yellow chile.
상기 무화과 농축액은 무화과잎, 무화과가지, 무화과열매, 꿀, 물엿, 설탕의 혼합비율은 혼합물의 총 100중량%에 대하여 무화과잎 5~10중량%, 무화과가지 5~10중량%, 무화과열매 30~35중량%, 꿀 5~10중량%, 물엿 5~10중량%, 설탕 30~35중량%를 투입하여 제조되는 것이다. 바람직하게는 무화과 잎, 무화과 가지 및 무화과 열매를 1:1:2~4의 비율로 혼합하여 제조할 수 있다. 당도를 높이기 위해 당분 함량이 높은, 꿀과 물엿, 설탕을 더 포함시킬 수 있다.The fig concentrate is a fig leaf, fig branch, fig fruit, honey, syrup, sugar mixed ratio of 5 to 10% by weight fig leaf, 5 to 10% by weight fig branch, 30 ~ fig fruit relative to 100% by weight of the mixture It is prepared by adding 35% by weight, 5-10% by weight of honey, 5-10% by weight of starch syrup, and 30-35% by weight of sugar. Preferably, fig leaves, fig branches, and fig fruits may be prepared by mixing in a ratio of 1: 1: 2-4. To increase sugar content, sugar, high sugar, starch syrup and sugar may be added.
무화과가지는 해당 년도에 자란 어린 무화과의 가지를 사용하며, 무화과가지에는 프소릴렌, 베로갑텐, 아즐렌등의 성분이 함유되어 있다. 무화과잎은 알칼로이드, 사포닌, 플라보노이드(루틴), 고무질, 수지, 비타민C, 정유 등이 함유되어 있다. 무화과잎, 무화과가지, 무화과열매를 꿀, 물엿, 설탕과 혼합하는 것은 상술한 무화과 잎, 무화과가지가 각종 영양은 풍부하나 특유의 쓰고 역겨운 맛으로 인하여 소비자가 취식하는 경우 거부감을 일으킬 수 있는 문제를 개선할 수 있는 것이다.Fig branches use the branches of young figs grown during the year, and fig branches contain ingredients such as psoralene, verogatten, and azulene. Fig leaves contain alkaloids, saponins, flavonoids (rutin), gums, resins, vitamin C and essential oils. Mixing fig leaves, fig branches, and fig fruits with honey, syrup, and sugar is a problem in which the fig leaves and fig branches described above are rich in various nutrients, but may cause a sense of rejection when consumers eat them due to their unique bitterness. It can be improved.
상기 S1 단계의 숙성 전에 가열 추출하는 등의 방법과 같이 이 기술분야에서 널리 알려진 방법에 따라 농축기에 넣고 농축과정을 더 수행할 수 있다. 이후 숙성고에서 15~20℃의 온도 이내에서 자연숙성되는 것이다. S1 단계에서 숙성한 후 필터에 걸러서 무화과 농축액을 수득할 수 있으며, 상기 무화과 농축액의 총량을 100 중량부로 볼 때, 이중 40 중량부를 분리하여 이를 황칠나무 추출물과 혼합하는 것이다. 황칠나무 추출물과의 혼합 중량비율은 20:80~80:20일 수 있으나 이에 제한되지는 않는다.According to a method well known in the art, such as a method such as heat extraction before the aging of the step S1 may be further concentrated in the concentrator. After maturation in the high temperature within 15 ~ 20 ℃ will be matured. After aging in the step S1 can be obtained by filtering the fig concentrate, when the total amount of the fig concentrate is 100 parts by weight, of which 40 parts by weight is separated and mixed with the yellow lacquer extract. The mixing weight ratio with Hwangchil-tree extract may be 20:80 to 80:20, but is not limited thereto.
상기 40 중량부의 무화과 농축액이 분리된 후 남은 60 중량부의 무화과 농축액은 필터를 통해 불순물을 제거한 후 다시 숙성고에 넣어 2~3개월 동안 2차 숙성할 수 있다. 상기 2차 숙성 후 제조된 2차 숙성액 60 중량부에서 40 중량부를 분리하여 이를 황칠나무 추출물과 혼합하는 것이다. 황칠나무 추출물과의 혼합 중량비율은 20:80~80:20일 수 있으나 이에 제한되지는 않는다.The remaining 60 parts by weight of the fig concentrate after the separation of the 40 parts by weight of the fig concentrate may be subjected to secondary ripening for 2 to 3 months after removing impurities through a filter and then putting them back into maturation. After separating the 40 parts by weight from 60 parts by weight of the secondary aging solution prepared after the second aging it is mixed with the hwangchil wood extract. The mixing weight ratio with Hwangchil-tree extract may be 20:80 to 80:20, but is not limited thereto.
상기 40 중량부의 2차 숙성액이 분리된 후 남은 20 중량부의 2차 숙성액은 필터를 통해 불순물을 제거한 후 다시 숙성고에 넣어 2~3개월 동안 15℃ 이하의 온도로 3차 숙성하여 3차 숙성액을 제조할 수 있다. The remaining 20 parts by weight of the secondary aging liquid after the separation of the 40 parts by weight of the secondary aging liquid is removed by impurities through a filter and put again in the maturation of the second three months at a temperature of 15 ℃ or less for 3 to 3 months Aging liquid can be prepared.
이와 같이 황칠성분의 함유를 위해 S1단계에서 숙성된 무화과 농축액, S4 단계에서 숙성된 무화과 숙성액, S6 단계에서 3차 숙성된 무화과 숙성액을 나누어 황칠 추출물을 2:2:1의 비율로 혼합을 수행하는 것이다.Thus, to contain the yellow lacquer ingredients, the fig concentrate aged in step S1, the fig ripening step in S4, and the third ripening fig ripening step in S6 are divided into two parts: To do.
이때 무화과엑기스의 맛과 향이 변질되는 것을 최소화하기 위하여 냉장기계를 통하여 저온숙성시키는 것이며, 이러한 과정을 통하여 무화과의 개선된 맛과 향이 장기간 보전될 수 있는 무화과엑기스를 얻을 수 있게 되며, 숙성되는 과정에서 황칠추출물을 혼합하여 자연스럽게 황칠액기스의 성분이 융합될 수 있도록 하는 것이다. At this time, in order to minimize the deterioration of the taste and aroma of the fig extract, it is low-temperature aging through a refrigeration machine. Through this process, it is possible to obtain a fig extract that can preserve the improved taste and aroma of the fig. Hwangchil extract by mixing the natural components of the hwangchil extract is to be fused.
상기 무화과로는 청무화과 또는 홍무화과를 사용할 수 있으며, 바람직하게는 청무화과를 이용할 수 있다.As the fig, a blue or red aqua may be used, and preferably, a blue aqua may be used.
상기 황칠나무 추출물은 황칠나무의 잎 추출물, 황칠나무의 줄기(가지) 추출물 및 황칠나무의 수액 추출물 중에서 선택된 하나 이상을 포함할 수 있는 것이다. 각 부위별 추출물은 용매 추출, 초임계 추출, 수증기 증발 추출, 및/또는 용매 분획 추출 등을 통해 얻어질수 있다. 또한, 수액 추출물은 황칠나무로부터 채취된 수액을 용매 분획 추출하여 얻어진 것이나, 황칠나무로부터 채취된 수액을 용매 추출, 초임계 추출 및/또는 수증기 증발 추출을 통해 추출한 후 용매 분획 추출을 진행한 것을 포함할 수 있다. 바람직하게는 70% 에탄올을 사용하여 추출된 것을 사용할 수 있다.The hwangchil wood extract may include one or more selected from the leaves extract of the hwangchil, stem (branch) extract of the hwangchil trees and sap extract of the hwangchil. The extract for each site may be obtained through solvent extraction, supercritical extraction, steam evaporation extraction, and / or solvent fraction extraction. In addition, the sap extract is obtained by the solvent fraction extraction of the sap collected from the yellow lacquer tree, or the extract of the sap collected from the yellow lacquer tree through solvent extraction, supercritical extraction and / or vapor evaporation extraction and then proceeding to the solvent fraction extraction can do. Preferably, extracted with 70% ethanol can be used.
또한 상기 황칠나무 추출물은 정제수를 포함한 물, C1 내지 C4의 저급 알콜 및 헥산으로 이루어진 군에서 선택되는 적어도 하나를 가하여 황칠나무 추출물을 제조하고, 상기 1단계에서 제조된 황칠나무 추출물에 계통분획을 실시하여 황칠나무 분획물을 제조하는 2단계 및 2단계에 제조된 황칠나무 분획물을 크로마토그래피로 분리, 정제하는 3단계를 포함하는 과정으로 추출공정을 수행하여 제조되는 것일 수 있다.In addition, the extract of Hwangchil wood is added to at least one selected from the group consisting of water, C1 to C4 lower alcohol and hexane containing purified water to produce the Hwangchil wood extract, and subjected to a systematic fraction to the Hwangchil wood extract prepared in step 1 By the two steps to prepare the hwangchil wood fractions and may be prepared by performing the extraction process in a process comprising three steps of separating and purifying the hwangchil wood fraction prepared in step 2 by chromatography.
계통분획은 상기 1단계에서 제조된 황칠나무 추출물을 물로 현탁한 후, n-헥산, 클로로포름, 에틸아세테이트 및 n-부탄올로 계통분획을 실시, 3단계의 황칠나무 분획물은 황칠나무의 n-헥산 분획물이고, 상기 3단계의 크로마토그래피는 아세톤 및 헥산이 1:1 내지 100의 질량대 부피비로 혼합된 용매를 이용한 것일 수 있다.The phylogenetic fraction was suspended in water from the yellow lacquer tree extract prepared in step 1, and then subjected to phylogenetic fraction with n-hexane, chloroform, ethyl acetate and n-butanol. The three steps of chromatography may be a solvent in which acetone and hexane are mixed at a mass to volume ratio of 1: 1 to 100.
상기 무화과는 당성분이 많고, GABA에 작용해서, 미백효과 우수하며, 황칠은 당뇨에 효과적인 바, 상기 방법을 통해 제조된 식품은 그 기능성과 동시에 맛이 우수한 장점이 있다.The fig has a lot of sugar components, acts on GABA, excellent whitening effect, and hwangchil is effective for diabetes, food produced through the method has the advantage of excellent functionality and taste at the same time.
이하 본 발명의 실시예에 의해 상세히 설명한다. 단, 하기의 실시예는 본 발명을 예시하는 것일 뿐, 본 발명의 내용이 하기의 실시예에 한정되는 것은 아니다.Hereinafter will be described in detail by the embodiment of the present invention. However, the following examples are merely to illustrate the invention, but the content of the present invention is not limited to the following examples.
[실시예]EXAMPLE
실시예 1. 황칠 추출물의 제조Example 1. Preparation of yellow lacquer extract
황칠나무 잎과 줄기(황칠나무 잎과 줄기는 동일 중량임)를 동결 건조한 후 건조한 잎과 줄기를 분쇄하여 얻은 분쇄물에 2배 중량의 70% 에탄올(ALC)을 가해 상온에서 10시간 동안 추출하고, 그 추출액을 여과. 다음 그 여액을 감압농축 동결 건조하여 분말상의 황칠나무 70% 에탄올 추출액을 제조할 수 있었다.After freeze-drying the yellow leaves and stems (same leaves and stems of the same weight), two times of 70% ethanol (ALC) was added to the ground powder obtained by pulverizing the dried leaves and stems. , Filtered the extract. Then, the filtrate was concentrated under reduced pressure and freeze-dried to prepare a powdery Hwangchil-tree 70% ethanol extract.
실시예 2. 무화과 농축액의 제조Example 2. Preparation of Fig Concentrate
무화과잎, 무화과가지, 무화과열매를 깨끗이 세척해 주었다. 이후 무화과잎, 무화과가지, 무화과열매를 꿀, 물엿, 설탕이 들어있는 용기에 투입하였다. 상기 성분들의 혼합비율은 혼합물의 총 100중량%에 대하여 무화과잎 10중량%, 무화과가지 10중량%, 무화과열매 30중량%, 꿀 10 중량%, 물엿 10중량%, 설탕 30중량%으로 하였다. 이를 농축기에 넣고 농축과정을 수행하였다. 이후, 숙성고에서 15~20℃의 온도 이내에서 1차로 자연 숙성 시켜주었다. The fig leaves, fig branches, and fig fruits were washed clean. Then, fig leaves, fig branches, and fig fruits were put in a container containing honey, syrup, and sugar. The mixing ratio of the components was 10% by weight of fig leaves, 10% by weight of fig branches, 30% by weight of fig fruits, 10% by weight of honey, 10% by weight of starch syrup, and 30% by weight of sugar. This was placed in a concentrator and concentrated. Thereafter, in the maturation of the high-temperature fermentation within 15 ~ 20 ℃ first.
자연 숙성이 완료되면 필터에 걸러 무화과 농축액을 추출하였다.After natural ripening was completed, the filter was extracted through a filter.
실시예 3. 무화과 농축액 및 황칠나무 추출물의 혼합Example 3. Mixture of Fig Concentrate and Hwangchil Tree Extract
상기 실시예 2에서 제조된 무화과 농축액(100 중량부)에서 40 중량부를 분리하여 실시예 1에서 제조된 황칠나무 추출물과 1:1의 비율로 혼합하여 1차 혼합숙성액을 제조하였다.40 parts by weight of the fig concentrate prepared in Example 2 (100 parts by weight) was separated, and mixed with the extract of Hwangchil-tree prepared in Example 1 in a ratio of 1: 1 to prepare a first mixed ripening solution.
상기 40 중량부가 분리된 후 남은 무화과 농축액을 다시 숙성고에 넣어 3개월 동안 2차 숙성시켜 주었다. 숙성이 마무리되어 제조된 2차 숙성액(60 중량부)에서 40 중량부를 분리하여, 역시 실시예 1에서 제조된 황칠나무 추출물과 1:1의 비율로 혼합하여 2차 혼합숙성액을 제조하였다.After the 40 parts by weight was separated, the remaining fig concentrate was aged again and aged for 2 months. 40 parts by weight of the second aging solution (60 parts by weight) prepared by aging was separated, and the mixture was also mixed with the Hilchi chile extract prepared in Example 1 in a ratio of 1: 1 to prepare a secondary mixed aging solution.
상기 2차 숙성액 중 40 중량부가 분리되고 남은 20 중량부의 2차 숙성액을 필터에 걸러 불순물을 제거하고 걸러진 무화과원액을 다시 숙성고에 넣어 3개월 동안 15℃ 이하의 온도로 3차 숙성하였고, 3차 숙성액에 역시 실시예 1에서 제조된 황칠나무 추출물과 1:1의 비율로 혼합하여 3차 혼합숙성액을 제조하였다.40 parts by weight of the second aging liquid was separated and the remaining 20 parts by weight of the second aging liquid was filtered through a filter to remove impurities, and the filtered filtrate was put into aging cell for 3 months at a temperature of 15 ° C. or lower for 3 months. The tertiary aging liquid was also mixed with the Hilchi chile extract prepared in Example 1 in a ratio of 1: 1 to prepare a tertiary mixed aging liquid.
이후 1차 혼합숙성액, 2차혼합숙성액 및 3차 혼합숙성액을 혼합하여, 건강기능성 식품을 제조하였다.Thereafter, the first mixed ripening liquid, the second mixed ripening liquid and the third mixed ripening liquid were mixed to prepare a health functional food.
실시예 4. 제조방법에 따른 관능 평가Example 4. Sensory evaluation according to the manufacturing method
실시예 3에서 제조된 식품을 대상으로, 20대~50대의 남성 및 여성 50명을 시험대상으로 하여 맛에 대한 관능 평가를 실시하였고, 5점 평가 (5:매우 좋음, 4:약간 좋음, 3:보통, 2:약간 나쁨, 1:매우 나쁨)를 기준으로 관능 평가하였다. 그 결과를 평균하여 하기 표 1에 나타내었다.For the food prepared in Example 3, 50 men and women in their 20s to 50s were subjected to sensory evaluation on taste, and five-point evaluation (5: very good, 4: slightly good, 3). : Normal, 2: slightly poor, 1: very poor). The results are averaged and shown in Table 1 below.
비교를 위해, 무화과 잎(15중량%), 무화과 가지(15중량%), 무화과 열매(70중량%)를 꿀, 물엿, 설탕에 넣어 제조한 무화과 혼합 농축액(비교예 1)과, 실시예 1의 황칠나무 추출물(비교예 2)과, 상기 무화과 혼합 농축액과 실시예 1의 황칠나무 추출물을 1:1로 혼합한 식품(비교예 3)을 제공하였다.For comparison, fig leaf (15% by weight), fig eggplant (15% by weight), fig fruit (70% by weight) and a fig mixed concentrate (Comparative Example 1) prepared by adding honey, syrup, and sugar, and Example 1 Hwangchil-tree extract (Comparative Example 2) and the fig mixed concentrate and the Hwangchil-tree extract of Example 1 to provide a food (Comparative Example 3).
상기 표 1의 결과와 같이, 본 발명의 제조방법을 통해 제조된 식품의 우수한 평가를 확인할 수 있다. 비교예 1의 경우 달콤한 맛이 느껴짐에도 불구하고 쓴맛이나 역겨운 맛이 느껴진다는 평가가 많았으며, 이는 무화과 잎특유의 맛이 느껴져서 인 것으로 판단됐다. 비교예 2의 경우 쓴맛이 너무 진하게 느껴진다는 평가가 있었고, 비교예 3의 경우 무난한 맛이었으나, 실시예에 따라 숙성단계별로 황칠나무 추출물을 혼합하여 제조하는 경우가 보다 맛이 우수하여 선호도가 보다 우수함을 알 수 있었다.As shown in Table 1, it can be confirmed the excellent evaluation of the food produced through the production method of the present invention. In Comparative Example 1, although a sweet taste was felt, there were many evaluations that a bitter or disgusting taste was felt, which was judged to be due to the peculiar taste of the fig leaf. In Comparative Example 2, there was an evaluation that the bitter taste was felt too dark, and in the case of Comparative Example 3 was a mild taste, but in the case of producing by mixing the Hilchi Chil wood extract by aging step according to the Example has a better taste and a better preference And it was found.
전술한 본 발명의 설명은 예시를 위한 것이며, 본 발명이 속하는 기술 분야의 통상의 지식을 가진 자는 본 발명의 기술적 사상이나 필수적인 특징을 변경하지 않고서 다른 구체적인 형태로 쉽게 변형이 가능하다는 것을 이해할 수 있을 것이다. 그러므로 이상에서 기술한 실시예들은 모든 면에서 예시적인 것이며 한정적이 아닌 것으로 이해해야 한다.The above description of the present invention is intended for illustration, and it will be understood by those skilled in the art that the present invention may be easily modified in other specific forms without changing the technical spirit or essential features of the present invention. will be. Therefore, it should be understood that the embodiments described above are exemplary in all respects and not restrictive.
Claims (3)
상기 S1단계에서 숙성후, 필터에 걸러 무화과 농축액을 추출하는 단계(S2);
상기 추출한 무화과 농축액 총 100 중량부 중 40 중량부를 분리하여, 황칠나무 추출물과 1:1의 비율로 혼합하는 단계(S3);
상기 S3 단계에서 분리하고 남은 무화과 농축액을 2차 숙성하여 2차 숙성액을 제조하는 단계(S4);
상기 S4 단계의 2차 숙성액 총 60 중량부 중 40 중량부를 분리하여, 황칠나무 추출물과 1:1의 비율로 혼합하는 단계(S5);
상기 S5 단계에서 분리하고 남은 2차 숙성액을 3차 숙성하여 3차 숙성액을 제조하는 단계(S6);
상기 S6 단계의 3차 숙성액을 황칠나무 추출물과 1:1의 비율로 혼합하는 단계(S7); 및
상기 S3, S5, 및 S7단계에서 황칠나무 추출물과 혼합된 혼합액을 혼합하는 단계(S8)를 포함하는, 무화과 농축액 및 황칠나무 추출물을 포함하는 건강기능성 식품용 조성물의 제조방법.
10% by weight of fig leaves, 10% by weight of fig branches, 30% by weight of fig fruit, 10% by weight of honey, 10% by weight of starch syrup, and 30% by weight of sugar, followed by aging (S1);
After aging in the step S1, the step of extracting the fig concentrate by filtering the filter (S2);
Separating 40 parts by weight of the total 100 parts by weight of the extracted fig concentrate, and mixing with the ratio of the Hwangchil wood extract in a ratio of 1: 1 (S3);
Preparing a secondary aging solution by secondary aging of the remaining fig concentrate separated in step S3 (S4);
Separating 40 parts by weight of the total 60 parts by weight of the secondary aging solution of the step S4, mixing with the ratio of the Hwangchil wood 1: 1 (S5);
Preparing a third aging solution by terminating the second aging solution remaining in the step S5 and tertiary aging solution (S6);
Mixing the third aging solution of the step S6 with Hwangchil-tree extract in a ratio of 1: 1 (S7); And
S3, S5, and S7 comprising the step (S8) of mixing the mixed solution and the mixed solution mixed with the yellow lacquer extract, a method for producing a health functional food composition comprising a fig concentrate and yellow lacquer extract.
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KR20100018993A (en) | 2008-08-08 | 2010-02-18 | 김범식 | Manufacturing method for a fig and a fig beverage |
KR20120007275A (en) * | 2010-07-14 | 2012-01-20 | 주식회사 면역과학연구소 | Composition comprising plants extract mixture for immune enhancement |
KR20180054545A (en) | 2018-05-14 | 2018-05-24 | 권성민 | A beverage composition comprising Dendropanax morbifera Extract |
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KR20100018993A (en) | 2008-08-08 | 2010-02-18 | 김범식 | Manufacturing method for a fig and a fig beverage |
KR20120007275A (en) * | 2010-07-14 | 2012-01-20 | 주식회사 면역과학연구소 | Composition comprising plants extract mixture for immune enhancement |
KR20180054545A (en) | 2018-05-14 | 2018-05-24 | 권성민 | A beverage composition comprising Dendropanax morbifera Extract |
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