KR101991529B1 - 분자체 전구체 및 분자체의 합성 - Google Patents
분자체 전구체 및 분자체의 합성 Download PDFInfo
- Publication number
- KR101991529B1 KR101991529B1 KR1020147007398A KR20147007398A KR101991529B1 KR 101991529 B1 KR101991529 B1 KR 101991529B1 KR 1020147007398 A KR1020147007398 A KR 1020147007398A KR 20147007398 A KR20147007398 A KR 20147007398A KR 101991529 B1 KR101991529 B1 KR 101991529B1
- Authority
- KR
- South Korea
- Prior art keywords
- zeolite
- silica
- colloidal
- colloidal solution
- less
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/86—Catalytic processes
- B01D53/8621—Removing nitrogen compounds
- B01D53/8625—Nitrogen oxides
- B01D53/8628—Processes characterised by a specific catalyst
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/92—Chemical or biological purification of waste gases of engine exhaust gases
- B01D53/94—Chemical or biological purification of waste gases of engine exhaust gases by catalytic processes
- B01D53/9404—Removing only nitrogen compounds
- B01D53/9409—Nitrogen oxides
- B01D53/9413—Processes characterised by a specific catalyst
- B01D53/9418—Processes characterised by a specific catalyst for removing nitrogen oxides by selective catalytic reduction [SCR] using a reducing agent in a lean exhaust gas
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
- B01J29/7015—CHA-type, e.g. Chabazite, LZ-218
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
- C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2255/00—Catalysts
- B01D2255/50—Zeolites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/30—Erionite or offretite type, e.g. zeolite T
- C01B39/305—Erionite or offretite type, e.g. zeolite T using at least one organic template directing agent
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- Analytical Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Combustion & Propulsion (AREA)
- Crystallography & Structural Chemistry (AREA)
- Catalysts (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Exhaust Gas Treatment By Means Of Catalyst (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161527312P | 2011-08-25 | 2011-08-25 | |
| US61/527,312 | 2011-08-25 | ||
| US13/592,726 US9174849B2 (en) | 2011-08-25 | 2012-08-23 | Molecular sieve precursors and synthesis of molecular sieves |
| US13/592,726 | 2012-08-23 | ||
| PCT/US2012/052228 WO2013028958A1 (en) | 2011-08-25 | 2012-08-24 | Molecular sieve precursors and synthesis of molecular sieves |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20140057616A KR20140057616A (ko) | 2014-05-13 |
| KR101991529B1 true KR101991529B1 (ko) | 2019-06-20 |
Family
ID=47744034
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020147007398A Active KR101991529B1 (ko) | 2011-08-25 | 2012-08-24 | 분자체 전구체 및 분자체의 합성 |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US9174849B2 (https=) |
| EP (1) | EP2748109B1 (https=) |
| JP (1) | JP6112568B2 (https=) |
| KR (1) | KR101991529B1 (https=) |
| CN (1) | CN104010971B (https=) |
| ES (1) | ES2812508T3 (https=) |
| PL (1) | PL2748109T3 (https=) |
| WO (1) | WO2013028958A1 (https=) |
Families Citing this family (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20120134916A1 (en) * | 2011-02-28 | 2012-05-31 | Fedeyko Joseph M | High-temperature scr catalyst |
| US9108856B2 (en) * | 2013-09-18 | 2015-08-18 | Chevron U.S.A. Inc. | Method for preparing CHA-type molecular sieves using colloidal aluminosilicate and novel structure directing agents |
| US9908783B2 (en) | 2014-01-22 | 2018-03-06 | California Institute Of Technology | Methods for producing crystalline microporous solids with the RTH topology and compositions derived from the same |
| US9764313B2 (en) | 2014-06-18 | 2017-09-19 | Basf Corporation | Molecular sieve catalyst compositions, catalyst composites, systems, and methods |
| US9889437B2 (en) | 2015-04-15 | 2018-02-13 | Basf Corporation | Isomorphously substituted catalyst |
| RU2727801C2 (ru) * | 2014-06-18 | 2020-07-24 | Басф Корпорейшн | Каталитические композиции молекулярного сита, каталитические композиты, системы и способы |
| CA2952435C (en) * | 2014-06-18 | 2023-10-03 | Basf Corporation | Molecular sieve catalyst compositions, catalyst composites, systems, and methods |
| US10850265B2 (en) | 2014-06-18 | 2020-12-01 | Basf Corporation | Molecular sieve catalyst compositions, catalytic composites, systems, and methods |
| KR20170120656A (ko) * | 2015-02-27 | 2017-10-31 | 바스프 코포레이션 | 배기 가스 처리 시스템 |
| JP6599637B2 (ja) * | 2015-05-13 | 2019-10-30 | イビデン株式会社 | ゼオライト、該ゼオライトの製造方法、該ゼオライトを使用したハニカム触媒及び排ガス浄化装置 |
| JP6616101B2 (ja) * | 2015-05-15 | 2019-12-04 | イビデン株式会社 | ゼオライト、該ゼオライトの製造方法、該ゼオライトを使用したハニカム触媒及び排ガス浄化装置 |
| US9708193B2 (en) * | 2015-08-20 | 2017-07-18 | Chevron U.S.A. Inc. | Synthesis of aluminosilicate LEV framework type zeolites |
| JP6834250B2 (ja) * | 2015-09-01 | 2021-02-24 | 東ソー株式会社 | Aei型ゼオライトの製造方法 |
| US10399859B2 (en) * | 2015-10-26 | 2019-09-03 | Ecolab Usa Inc. | Highly homogenous zeolite precursors |
| CN108290144B (zh) | 2015-11-25 | 2021-04-02 | 三菱化学株式会社 | 沸石催化剂及低级烯烃的制造方法 |
| US20170158520A1 (en) * | 2015-12-04 | 2017-06-08 | Chevron U.S.A. Inc. | Synthesis of aluminosilicate zeolites having the offretite structure |
| CN106145137B (zh) * | 2016-06-27 | 2018-06-05 | 杨晓波 | 一种直接水热合成中硅铝比菱沸石的方法 |
| WO2018065885A1 (en) * | 2016-10-03 | 2018-04-12 | Basf Corporation | Aluminum gradient aluminosilicate zeolite compositions |
| JP7125937B2 (ja) * | 2016-12-02 | 2022-08-25 | エコラブ ユーエスエイ インク | ポリアルミニウム塩ならびに高純度コロイド状アルミナ-シリカ複合粒子およびゼオライトの調製におけるそれらの使用 |
| BR112019011548A2 (pt) * | 2016-12-08 | 2019-10-15 | Basf Corp | método para a cristalização de zeólitos |
| US11001503B2 (en) * | 2016-12-14 | 2021-05-11 | Sogang University Research Foundation | MFI zeolite with microporous and mesoporous hierarchical structure, preparation method therefor, and catalytic use thereof |
| CN107233914A (zh) * | 2017-05-27 | 2017-10-10 | 清华大学 | 一种Cu‑SAPO‑47分子筛脱硝催化剂的制备方法及其脱硝应用 |
| EP3749611A4 (en) * | 2018-02-06 | 2022-02-23 | Basf Se | PROCESS FOR PRODUCTION OF A ZEOLITE MATERIAL WITH RTH FRAME STRUCTURE |
| JP7410048B2 (ja) | 2018-03-21 | 2024-01-09 | ビーエーエスエフ コーポレーション | Chaゼオライト材料および関連する合成方法 |
| EP3781520A1 (en) * | 2018-04-20 | 2021-02-24 | Basf Se | A process for preparing a porous oxidic material which comprises micropores and mesopores and which comprises a zeolitic material having a framework type aei |
| US11878293B2 (en) * | 2018-09-11 | 2024-01-23 | Basf Corporation | Process for preparing a zeolitic material having framework type AEI |
| KR102239941B1 (ko) * | 2019-05-16 | 2021-04-13 | 한국화학연구원 | 메탄올로부터 경질올레핀의 전환을 위한 고활성 ssz-13 제올라이트 합성방법 |
| JP7370194B2 (ja) * | 2019-08-27 | 2023-10-27 | 東ソー株式会社 | ゼオライト製造用有機構造指向剤、及びこれを用いたゼオライトの製造方法 |
| EP4061770A1 (en) * | 2019-11-19 | 2022-09-28 | BASF Corporation | Zeolite synthesis |
| CN111017950A (zh) * | 2019-12-31 | 2020-04-17 | 山东齐鲁华信高科有限公司 | 一种低成本ssz-13分子筛的制备方法及应用 |
| CN115178231B (zh) * | 2021-04-01 | 2024-05-07 | 中国科学院大连化学物理研究所 | 一种吸附剂及其制备方法、应用 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005520763A (ja) * | 2002-03-15 | 2005-07-14 | エクソンモービル・ケミカル・パテンツ・インク | 高シリカシャバサイト、その合成及びオキシジェネート類のオレフィン類への変換におけるその使用 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3030181A (en) | 1957-08-26 | 1962-04-17 | Union Carbide Corp | Crystalline zeolite r |
| GB868846A (en) | 1957-08-26 | 1961-05-25 | Union Carbide Corp | Improvements in and relating to zeolites |
| US4544538A (en) * | 1982-07-09 | 1985-10-01 | Chevron Research Company | Zeolite SSZ-13 and its method of preparation |
| US4440871A (en) | 1982-07-26 | 1984-04-03 | Union Carbide Corporation | Crystalline silicoaluminophosphates |
| US4961917A (en) | 1989-04-20 | 1990-10-09 | Engelhard Corporation | Method for reduction of nitrogen oxides with ammonia using promoted zeolite catalysts |
| CA2121788C (en) | 1991-10-23 | 2004-01-27 | Johannes P. Verduijn | Nanometer-sized molecular sieve crystals or agglomerates and processes for their production |
| US6162415A (en) | 1997-10-14 | 2000-12-19 | Exxon Chemical Patents Inc. | Synthesis of SAPO-44 |
| CN1311757A (zh) | 1998-07-29 | 2001-09-05 | 埃克森化学专利公司 | 制备分子筛的方法 |
| EP1237818B1 (en) | 1999-11-23 | 2003-06-18 | Universite Laval | Mesoporous zeolitic material with microporous crystalline mesopore walls |
| US6709644B2 (en) | 2001-08-30 | 2004-03-23 | Chevron U.S.A. Inc. | Small crystallite zeolite CHA |
| WO2005098232A2 (en) | 2004-03-26 | 2005-10-20 | Michigan State University | Method for the preparation of metal oxides in nanometric particle form |
| US20050234136A1 (en) | 2004-04-19 | 2005-10-20 | Holland Brian T | Colloidal compositions and methods of preparing same |
| US20070104643A1 (en) | 2005-08-05 | 2007-05-10 | Holland Brian T | Mesoporous nanocrystaline zeolite composition and preparation from amorphous colloidal metalosilicates |
| EP2117707B2 (en) * | 2007-02-27 | 2018-08-15 | BASF Corporation | Copper cha zeolite catalysts |
| EP2944377A1 (en) * | 2007-03-26 | 2015-11-18 | PQ Corporation | Novel microporous crystalline material comprising a molecular sieve or zeolite having an 8-ring pore opening structure and methods of making and using same |
| EP3981502B8 (en) * | 2007-04-26 | 2025-04-16 | Johnson Matthey Public Limited Company | Transition metal/zeolite scr catalysts |
| ES2465004T3 (es) * | 2008-05-21 | 2014-06-04 | Basf Se | Procedimiento de síntesis directa de zeolitas que contienen Cu que tienen una estructura de CHA |
| JP5482179B2 (ja) * | 2008-12-22 | 2014-04-23 | 東ソー株式会社 | チャバザイト型ゼオライト及びその製造方法 |
| EP2687284A1 (en) | 2009-06-08 | 2014-01-22 | Basf Se | Cu containing silicoaluminophosphate (Cu-SAPO-34) |
| CN102665902A (zh) | 2009-11-24 | 2012-09-12 | 巴斯夫欧洲公司 | 制备具有cha结构的沸石的方法 |
-
2012
- 2012-08-23 US US13/592,726 patent/US9174849B2/en active Active
- 2012-08-24 EP EP12825021.4A patent/EP2748109B1/en active Active
- 2012-08-24 JP JP2014527323A patent/JP6112568B2/ja active Active
- 2012-08-24 WO PCT/US2012/052228 patent/WO2013028958A1/en not_active Ceased
- 2012-08-24 ES ES12825021T patent/ES2812508T3/es active Active
- 2012-08-24 KR KR1020147007398A patent/KR101991529B1/ko active Active
- 2012-08-24 CN CN201280052903.3A patent/CN104010971B/zh active Active
- 2012-08-24 PL PL12825021T patent/PL2748109T3/pl unknown
-
2015
- 2015-08-07 US US14/821,393 patent/US20150343375A1/en not_active Abandoned
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005520763A (ja) * | 2002-03-15 | 2005-07-14 | エクソンモービル・ケミカル・パテンツ・インク | 高シリカシャバサイト、その合成及びオキシジェネート類のオレフィン類への変換におけるその使用 |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20140057616A (ko) | 2014-05-13 |
| ES2812508T3 (es) | 2021-03-17 |
| WO2013028958A1 (en) | 2013-02-28 |
| CN104010971A (zh) | 2014-08-27 |
| EP2748109A4 (en) | 2015-05-27 |
| JP6112568B2 (ja) | 2017-04-12 |
| CN104010971B (zh) | 2016-11-09 |
| JP2014527017A (ja) | 2014-10-09 |
| US20150343375A1 (en) | 2015-12-03 |
| US20130052125A1 (en) | 2013-02-28 |
| EP2748109B1 (en) | 2020-06-03 |
| PL2748109T3 (pl) | 2020-11-16 |
| US9174849B2 (en) | 2015-11-03 |
| EP2748109A1 (en) | 2014-07-02 |
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