KR101984282B1 - 첨가된 조절제를 이용하는 에폭시화 공정 - Google Patents
첨가된 조절제를 이용하는 에폭시화 공정 Download PDFInfo
- Publication number
- KR101984282B1 KR101984282B1 KR1020147013188A KR20147013188A KR101984282B1 KR 101984282 B1 KR101984282 B1 KR 101984282B1 KR 1020147013188 A KR1020147013188 A KR 1020147013188A KR 20147013188 A KR20147013188 A KR 20147013188A KR 101984282 B1 KR101984282 B1 KR 101984282B1
- Authority
- KR
- South Korea
- Prior art keywords
- selectivity
- catalyst
- concentration
- temperature
- modifier
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
- C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
- C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
- C07D301/10—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Epoxy Compounds (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161548502P | 2011-10-18 | 2011-10-18 | |
| US61/548,502 | 2011-10-18 | ||
| PCT/US2012/060482 WO2013059225A1 (en) | 2011-10-18 | 2012-10-17 | Epoxidation process with added moderator |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20150101919A KR20150101919A (ko) | 2015-09-04 |
| KR101984282B1 true KR101984282B1 (ko) | 2019-05-30 |
Family
ID=48086410
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020147013188A Active KR101984282B1 (ko) | 2011-10-18 | 2012-10-17 | 첨가된 조절제를 이용하는 에폭시화 공정 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9221774B2 (https=) |
| EP (1) | EP2768815B2 (https=) |
| KR (1) | KR101984282B1 (https=) |
| CN (2) | CN104203931A (https=) |
| BR (1) | BR112014009339A2 (https=) |
| IN (1) | IN2014DN03028A (https=) |
| TW (1) | TW201335143A (https=) |
| WO (1) | WO2013059225A1 (https=) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SG190901A1 (en) | 2010-12-15 | 2013-07-31 | Dow Technology Investments Llc | Method of starting-up a process of producing an alkylene oxide using a high-efficiency catalyst |
| CN105980368B (zh) * | 2013-12-23 | 2019-02-19 | 科学设计有限公司 | 环氧化方法 |
| WO2016137777A1 (en) | 2015-02-27 | 2016-09-01 | 3M Innovative Properties Company | Optical film including collimating reflective polarizer and structured layer |
| WO2019055773A1 (en) | 2017-09-15 | 2019-03-21 | MultiPhase Solutions, Inc. | GAS PHASE CHROMATOGRAPHY OF SELECTIVE HALOGEN DETECTION FOR ONLINE ANALYSIS AND CONTROL OF SELECTIVE OXIDATION CHEMICAL PRODUCTION PROCESSES |
| CN117099163A (zh) * | 2021-04-08 | 2023-11-21 | 国际壳牌研究有限公司 | 乙烯环氧化的缓和剂和催化剂性能优化 |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2279469A (en) | 1942-04-14 | Process of making olefin oxides | ||
| SE321462B (https=) | 1962-10-10 | 1970-03-09 | Halcon International Inc | |
| GB1170663A (en) | 1967-03-22 | 1969-11-12 | Shell Int Research | Process for preparing Silver Catalysts |
| US3702259A (en) | 1970-12-02 | 1972-11-07 | Shell Oil Co | Chemical production of metallic silver deposits |
| US4766105A (en) † | 1986-10-31 | 1988-08-23 | Shell Oil Company | Ethylene oxide catalyst and process for preparing the catalyst |
| US4761394A (en) † | 1986-10-31 | 1988-08-02 | Shell Oil Company | Ethylene oxide catalyst and process for preparing the catalyst |
| US4908343A (en) | 1987-02-20 | 1990-03-13 | Union Carbide Chemicals And Plastics Company Inc. | Catalyst composition for oxidation of ethylene to ethylene oxide |
| US5057481A (en) | 1987-02-20 | 1991-10-15 | Union Carbide Chemicals And Plastics Technology Corporation | Catalyst composition for oxidation of ethylene to ethylene oxide |
| CA1339317C (en) * | 1988-07-25 | 1997-08-19 | Ann Marie Lauritzen | Process for producing ethylene oxide |
| EP0357293B1 (en) | 1988-08-30 | 1996-02-28 | Union Carbide Corporation | Catalysts for the production of ethylene oxide and their preparation processes |
| US5187140A (en) | 1989-10-18 | 1993-02-16 | Union Carbide Chemicals & Plastics Technology Corporation | Alkylene oxide catalysts containing high silver content |
| US5102848A (en) | 1990-09-28 | 1992-04-07 | Union Carbide Chemicals & Plastics Technology Corporation | Catalyst composition for oxidation of ethylene to ethylene oxide |
| US5407888A (en) | 1992-05-12 | 1995-04-18 | Basf Aktiengesellschaft | Silver catalyst |
| BR0214282A (pt) * | 2001-11-20 | 2004-09-21 | Shell Int Research | Processos e sistemas para epoxidação de uma olefina |
| US7193094B2 (en) | 2001-11-20 | 2007-03-20 | Shell Oil Company | Process and systems for the epoxidation of an olefin |
| KR100980123B1 (ko) * | 2002-06-28 | 2010-09-03 | 셀 인터나쵸나아레 레사아치 마아츠샤피 비이부이 | 촉매 선택성을 향상시키는 방법 및 올레핀 에폭시화 방법 |
| RU2005102097A (ru) * | 2002-06-28 | 2005-08-27 | Шелл Интернэшнл Рисерч Маатсхаппий Б.В. (NL) | Способ введения в действие способа эпоксидирования и способ эпоксидирования олефина |
| RU2360908C2 (ru) | 2003-09-29 | 2009-07-10 | Дау Текнолоджи Инвестментс Ллс. | Способ получения алкиленоксида с использованием газофазной промоторной системы |
| US8791280B2 (en) | 2005-08-10 | 2014-07-29 | Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg | Process for preparation of catalyst carrier and its use in catalyst preparation |
| KR101485955B1 (ko) * | 2007-05-11 | 2015-01-22 | 베리 제이. 빌릭 | 산화올레핀 제조 공장에서의 고선택성 촉매의 개시 방법 |
| JP2012524785A (ja) * | 2009-04-21 | 2012-10-18 | ダウ テクノロジー インベストメンツ リミティド ライアビリティー カンパニー | 高効率触媒を用いたアルキレンオキシド簡易製造方法 |
| CN102421766B (zh) * | 2009-04-21 | 2015-03-25 | 陶氏技术投资有限公司 | 提高铼助催化的环氧化催化剂的效率的方法以及使用它们的环氧化方法 |
| WO2010123844A1 (en) * | 2009-04-21 | 2010-10-28 | Dow Technology Investments Llc | Improved method of achieving and maintaining a specified alkylene oxide production parameter with a high efficiency catalyst |
| CN102414189B (zh) * | 2009-04-21 | 2014-09-17 | 陶氏技术投资有限公司 | 环氧化反应及其操作条件 |
| JP2013515730A (ja) * | 2009-12-23 | 2013-05-09 | サイエンティフィック・デザイン・カンパニー・インコーポレーテッド | 高選択性酸化エチレン触媒の開始工程 |
-
2012
- 2012-10-17 WO PCT/US2012/060482 patent/WO2013059225A1/en not_active Ceased
- 2012-10-17 EP EP12841718.5A patent/EP2768815B2/en active Active
- 2012-10-17 BR BR112014009339A patent/BR112014009339A2/pt not_active IP Right Cessation
- 2012-10-17 IN IN3028DEN2014 patent/IN2014DN03028A/en unknown
- 2012-10-17 KR KR1020147013188A patent/KR101984282B1/ko active Active
- 2012-10-17 TW TW101138264A patent/TW201335143A/zh unknown
- 2012-10-17 CN CN201280062741.1A patent/CN104203931A/zh active Pending
- 2012-10-17 CN CN201810386174.4A patent/CN108707125A/zh active Pending
- 2012-10-18 US US13/655,000 patent/US9221774B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP2768815B1 (en) | 2018-12-12 |
| CN104203931A (zh) | 2014-12-10 |
| US20130096330A1 (en) | 2013-04-18 |
| TW201335143A (zh) | 2013-09-01 |
| WO2013059225A1 (en) | 2013-04-25 |
| US9221774B2 (en) | 2015-12-29 |
| BR112014009339A2 (pt) | 2017-04-18 |
| EP2768815A1 (en) | 2014-08-27 |
| CN108707125A (zh) | 2018-10-26 |
| IN2014DN03028A (https=) | 2015-05-08 |
| EP2768815B2 (en) | 2021-12-29 |
| KR20150101919A (ko) | 2015-09-04 |
| EP2768815A4 (en) | 2015-05-27 |
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| KR20150103716A (ko) | 고 선택성 산화에틸렌 촉매를 위한 스타트-업 공정 | |
| KR101984282B1 (ko) | 첨가된 조절제를 이용하는 에폭시화 공정 | |
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| US8624045B2 (en) | Process for olefin oxide production | |
| US11931725B2 (en) | Ethylene oxide high selectivity catalyst conditioning process |
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