KR101950076B1 - 아세트산을 제조하는 방법 - Google Patents

아세트산을 제조하는 방법 Download PDF

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Publication number
KR101950076B1
KR101950076B1 KR1020167017379A KR20167017379A KR101950076B1 KR 101950076 B1 KR101950076 B1 KR 101950076B1 KR 1020167017379 A KR1020167017379 A KR 1020167017379A KR 20167017379 A KR20167017379 A KR 20167017379A KR 101950076 B1 KR101950076 B1 KR 101950076B1
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South Korea
Prior art keywords
weight
acetic acid
water
alkane
stream
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Expired - Fee Related
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KR1020167017379A
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English (en)
Korean (ko)
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KR20160081997A (ko
Inventor
노엘 시. 할리난
존 디. 헌
미라지 에스. 파텔
마이클 이. 피츠패트릭
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라이온델바젤 아세틸, 엘엘씨
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/23—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
    • C07C51/235—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/50—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08—Acetic acid
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020167017379A 2011-12-21 2012-12-14 아세트산을 제조하는 방법 Expired - Fee Related KR101950076B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201161578709P 2011-12-21 2011-12-21
US61/578,709 2011-12-21
US13/713,930 US9090554B2 (en) 2011-12-21 2012-12-13 Process for the manufacture of acetic acid
US13/713,930 2012-12-13
PCT/US2012/069735 WO2013096118A1 (en) 2011-12-21 2012-12-14 Process for the manufacture of acetic acid

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
KR20147019087A Division KR20140100998A (ko) 2011-12-21 2012-12-14 아세트산을 제조하는 방법

Related Child Applications (1)

Application Number Title Priority Date Filing Date
KR1020177005968A Division KR20170028454A (ko) 2011-12-21 2012-12-14 아세트산을 제조하는 방법

Publications (2)

Publication Number Publication Date
KR20160081997A KR20160081997A (ko) 2016-07-08
KR101950076B1 true KR101950076B1 (ko) 2019-05-10

Family

ID=48669376

Family Applications (3)

Application Number Title Priority Date Filing Date
KR1020177005968A Abandoned KR20170028454A (ko) 2011-12-21 2012-12-14 아세트산을 제조하는 방법
KR1020167017379A Expired - Fee Related KR101950076B1 (ko) 2011-12-21 2012-12-14 아세트산을 제조하는 방법
KR20147019087A Ceased KR20140100998A (ko) 2011-12-21 2012-12-14 아세트산을 제조하는 방법

Family Applications Before (1)

Application Number Title Priority Date Filing Date
KR1020177005968A Abandoned KR20170028454A (ko) 2011-12-21 2012-12-14 아세트산을 제조하는 방법

Family Applications After (1)

Application Number Title Priority Date Filing Date
KR20147019087A Ceased KR20140100998A (ko) 2011-12-21 2012-12-14 아세트산을 제조하는 방법

Country Status (10)

Country Link
US (1) US9090554B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
EP (1) EP2794542B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
KR (3) KR20170028454A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CN (1) CN104364227B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
BR (1) BR112014015212B8 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CA (1) CA2859037C (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
IN (1) IN2014CN04560A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
RU (1) RU2583789C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
SG (1) SG11201402858PA (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
WO (1) WO2013096118A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9505696B2 (en) * 2015-02-04 2016-11-29 Celanese International Corporation Process to control HI concentration in residuum stream

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090229966A1 (en) * 2008-03-17 2009-09-17 Hallinan Noel C Removing hydrocarbon impurities from acetic acid production process

Family Cites Families (25)

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Publication number Priority date Publication date Assignee Title
US4102922A (en) 1974-12-30 1978-07-25 Monsanto Company Purification of carbonylation products
DE3107731A1 (de) * 1981-02-28 1982-09-16 Basf Ag, 6700 Ludwigshafen Verfahren zur abtrennung organischer jod-verbindungen von carbonylierungsprodukten des methanols, methylacetates und dimethylethers
US5026908A (en) 1984-05-03 1991-06-25 Hoechst Celanese Corporation Methanol carbonylation process
US5144068A (en) 1984-05-03 1992-09-01 Hoechst Celanese Corporation Methanol carbonylation process
US5001259A (en) 1984-05-03 1991-03-19 Hoechst Celanese Corporation Methanol carbonylation process
AU8790391A (en) 1990-11-19 1992-05-21 Hoechst Celanese Corporation Removal of carbonyl impurities from a carbonylation process stream
AU639630B2 (en) 1991-01-28 1993-07-29 Celanese International Corporation Removal of carbonyl impurities from carbonylation process stream
GB9106298D0 (en) 1991-03-25 1991-05-08 Bp Chem Int Ltd Process
US5625095A (en) 1994-06-15 1997-04-29 Daicel Chemical Industries, Ltd. Process for producing high purity acetic acid
US5599976A (en) 1995-04-07 1997-02-04 Hoechst Celanese Corporation Recovery of acetic acid from dilute aqueous streams formed during a carbonylation process
KR100403367B1 (ko) 1995-04-27 2004-03-26 다이셀 가가꾸 고교 가부시끼가이샤 아세트산제조법
US5783731A (en) 1995-09-11 1998-07-21 Hoechst Celanese Corporation Removal of carbonyl impurities from a carbonylation process stream
US5817869A (en) 1995-10-03 1998-10-06 Quantum Chemical Corporation Use of pentavalent Group VA oxides in acetic acid processing
IN192600B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 1996-10-18 2004-05-08 Hoechst Celanese Corp
US6339171B1 (en) 1996-10-18 2002-01-15 Celanese International Corporation Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream
GB9625335D0 (en) 1996-12-05 1997-01-22 Bp Chem Int Ltd Process
US6552221B1 (en) * 1998-12-18 2003-04-22 Millenium Petrochemicals, Inc. Process control for acetic acid manufacture
US7271293B2 (en) 2004-03-02 2007-09-18 Celanese International Corporation Control method for process of removing permanganate reducing compounds from methanol carbonylation process
US7208624B2 (en) * 2004-03-02 2007-04-24 Celanese International Corporation Process for producing acetic acid
US7855306B2 (en) 2005-04-28 2010-12-21 Celanese International Corporation Process for the production of acetic acid
TWI465424B (zh) 2006-03-21 2014-12-21 Bp Chem Int Ltd 製造醋酸的方法
US7619113B2 (en) * 2007-09-27 2009-11-17 Celanese International Corporation Method and apparatus for making acetic acid with improved purification
US7812191B2 (en) 2008-05-07 2010-10-12 Lyondell Chemical Technology, L.P. Removing hydrocarbon impurities from acetic acid by ionic liquid extraction
US7790920B2 (en) 2008-09-11 2010-09-07 Lyondell Chemical Technology, L.P. Preparation of acetic acid
US8586789B2 (en) * 2009-03-30 2013-11-19 Lyondell Chemical Technology, L.P. Removing hydrocarbon impurities from acetic acid production intermediate

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090229966A1 (en) * 2008-03-17 2009-09-17 Hallinan Noel C Removing hydrocarbon impurities from acetic acid production process

Also Published As

Publication number Publication date
CN104364227A (zh) 2015-02-18
KR20140100998A (ko) 2014-08-18
RU2014127297A (ru) 2016-02-10
EP2794542A1 (en) 2014-10-29
US9090554B2 (en) 2015-07-28
CN104364227B (zh) 2016-11-09
RU2583789C2 (ru) 2016-05-10
CA2859037A1 (en) 2013-06-27
KR20170028454A (ko) 2017-03-13
BR112014015212B8 (pt) 2022-07-12
WO2013096118A1 (en) 2013-06-27
EP2794542B1 (en) 2018-03-21
CA2859037C (en) 2016-05-24
BR112014015212B1 (pt) 2020-11-10
US20130296616A1 (en) 2013-11-07
IN2014CN04560A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 2015-09-18
SG11201402858PA (en) 2014-09-26
BR112014015212A2 (pt) 2017-07-04
KR20160081997A (ko) 2016-07-08
EP2794542A4 (en) 2015-05-27

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