KR101755053B1 - 방향족 및 지환족 아민에 기초한 다공성 겔 - Google Patents

방향족 및 지환족 아민에 기초한 다공성 겔 Download PDF

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Publication number
KR101755053B1
KR101755053B1 KR1020127006489A KR20127006489A KR101755053B1 KR 101755053 B1 KR101755053 B1 KR 101755053B1 KR 1020127006489 A KR1020127006489 A KR 1020127006489A KR 20127006489 A KR20127006489 A KR 20127006489A KR 101755053 B1 KR101755053 B1 KR 101755053B1
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KR
South Korea
Prior art keywords
component
gel
porous gel
solvent
porous
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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KR1020127006489A
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English (en)
Korean (ko)
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KR20120049913A (ko
Inventor
마르크 프리커
마르크 에블링
Original Assignee
바스프 에스이
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Publication of KR20120049913A publication Critical patent/KR20120049913A/ko
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Expired - Fee Related legal-status Critical Current
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3225—Polyamines
    • C08G18/3237—Polyamines aromatic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
    • C08G18/12—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step using two or more compounds having active hydrogen in the first polymerisation step
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3225—Polyamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3225—Polyamines
    • C08G18/3234—Polyamines cycloaliphatic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/28—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum
    • C08J9/286—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum the liquid phase being a solvent for the monomers but not for the resulting macromolecular composition, i.e. macroporous or macroreticular polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0091—Aerogels; Xerogels
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2330/00—Thermal insulation material
    • C08G2330/50—Evacuated open-celled polymer material
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2205/00—Foams characterised by their properties
    • C08J2205/02—Foams characterised by their properties the finished foam itself being a gel or a gel being temporarily formed when processing the foamable composition
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2375/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
    • C08J2375/04—Polyurethanes
    • C08J2375/12—Polyurethanes from compounds containing nitrogen and active hydrogen, the nitrogen atom not being part of an isocyanate group

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Organic Insulating Materials (AREA)
KR1020127006489A 2009-08-13 2010-08-02 방향족 및 지환족 아민에 기초한 다공성 겔 Expired - Fee Related KR101755053B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09167834.2 2009-08-13
EP09167834 2009-08-13
PCT/EP2010/061171 WO2011018371A1 (de) 2009-08-13 2010-08-02 Poröse gele auf basis von aromatischen und cycloaliphatischen aminen

Publications (2)

Publication Number Publication Date
KR20120049913A KR20120049913A (ko) 2012-05-17
KR101755053B1 true KR101755053B1 (ko) 2017-07-06

Family

ID=43479312

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020127006489A Expired - Fee Related KR101755053B1 (ko) 2009-08-13 2010-08-02 방향족 및 지환족 아민에 기초한 다공성 겔

Country Status (11)

Country Link
US (1) US8785512B2 (enExample)
EP (1) EP2464676B1 (enExample)
JP (1) JP5520379B2 (enExample)
KR (1) KR101755053B1 (enExample)
CN (1) CN102471438B (enExample)
AU (1) AU2010283879B9 (enExample)
ES (1) ES2437096T3 (enExample)
MX (1) MX2012001680A (enExample)
PL (1) PL2464676T3 (enExample)
RU (1) RU2541536C2 (enExample)
WO (1) WO2011018371A1 (enExample)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2439047T3 (es) * 2009-06-29 2014-01-21 Basf Se Geles porosos a base de poliurea aromática
US9260580B2 (en) 2010-06-28 2016-02-16 Basf Se Process for producing porous materials based on polyurea
US8697766B2 (en) 2011-02-24 2014-04-15 Basf Se Process for producing pulverulent porous materials
JP5925813B2 (ja) * 2011-03-18 2016-05-25 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ポリウレア系難燃性多孔質材料の製造方法
US20120235070A1 (en) 2011-03-18 2012-09-20 Basf Se Process for producing flame-retardant porous materials based on polyurea
US9188384B2 (en) 2011-03-31 2015-11-17 Basf Se Dynamically evacuable devices comprising organic aerogels or xerogels
AU2012234374B2 (en) * 2011-03-31 2016-10-20 Basf Se Dynamically evacuable apparatuses comprising organic aerogels or xerogels
WO2015193336A1 (en) 2014-06-20 2015-12-23 Basf Se Nanoporous carbon foams
PL3377568T3 (pl) * 2015-11-16 2021-05-17 Huntsman International Llc (super)hydrofobowe materiały porowate na bazie izocyjanianu
US10316161B2 (en) * 2017-03-16 2019-06-11 International Business Machines Corporation Method of making highly porous polyhexahydrotriazines containing antimicrobial agents
EP3849697A1 (de) * 2018-09-12 2021-07-21 Basf Se Verfahren zur kontinuierlichen überkritischen trocknung von aerogelpartikeln

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008138978A1 (de) 2007-05-16 2008-11-20 Basf Se Xerogele auf basis von aromatischem polyharnstoff

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2945614A1 (de) * 1979-11-12 1981-05-21 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von 4,4'diamino-3,3',5,5'-tetraalkyldicyclohexylmethanen
DE3325895A1 (de) 1983-07-19 1985-01-31 Basf Ag, 6700 Ludwigshafen Biscyclohexylaminalkane und verfahren zur bekaempfung von pilzen
EP0288067A1 (en) 1987-04-24 1988-10-26 Asahi Glass Company Ltd. Process for producing polyurethane elastomer and compositon as starting material therefor
US5478867A (en) * 1993-07-07 1995-12-26 The Dow Chemical Company Microporous isocyanate-based polymer compositions and method of preparation
JP2001263926A (ja) * 2000-03-17 2001-09-26 Matsushita Refrig Co Ltd 有機多孔体の製造方法および断熱パネルと断熱箱体
EP2258738B1 (de) 2007-08-28 2017-01-25 Basf Se Xerogele auf Basis von Polyharnstoff
US8026318B2 (en) * 2008-08-22 2011-09-27 Air Products And Chemicals, Inc. Mixed polycycloaliphatic amines (MPCA) and MPCA alkylates
KR20110117084A (ko) 2009-01-20 2011-10-26 바스프 에스이 경질 폴리우레탄 폼의 제조 방법
JP2012520386A (ja) 2009-03-16 2012-09-06 ビーエーエスエフ ソシエタス・ヨーロピア キセロゲル複合材料の製造方法
US20120193286A1 (en) 2009-10-16 2012-08-02 Basf Se Method for producing a nanoporous polyurethane-based coating

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008138978A1 (de) 2007-05-16 2008-11-20 Basf Se Xerogele auf basis von aromatischem polyharnstoff

Also Published As

Publication number Publication date
US20120142800A1 (en) 2012-06-07
RU2541536C2 (ru) 2015-02-20
PL2464676T3 (pl) 2014-03-31
MX2012001680A (es) 2012-03-07
AU2010283879A1 (en) 2012-03-08
AU2010283879B2 (en) 2015-05-28
JP5520379B2 (ja) 2014-06-11
EP2464676B1 (de) 2013-10-16
RU2012109200A (ru) 2013-09-20
US8785512B2 (en) 2014-07-22
ES2437096T3 (es) 2014-01-08
EP2464676A1 (de) 2012-06-20
AU2010283879B9 (en) 2015-10-08
JP2013501834A (ja) 2013-01-17
CN102471438B (zh) 2013-10-23
WO2011018371A1 (de) 2011-02-17
CN102471438A (zh) 2012-05-23
KR20120049913A (ko) 2012-05-17

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