KR101588562B1 - surfur removing poison for feedstuff and its product method - Google Patents

surfur removing poison for feedstuff and its product method Download PDF

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KR101588562B1
KR101588562B1 KR1020150026177A KR20150026177A KR101588562B1 KR 101588562 B1 KR101588562 B1 KR 101588562B1 KR 1020150026177 A KR1020150026177 A KR 1020150026177A KR 20150026177 A KR20150026177 A KR 20150026177A KR 101588562 B1 KR101588562 B1 KR 101588562B1
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sulfur
mixture
weight
fermented
parts
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KR1020150026177A
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Korean (ko)
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김상덕
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주식회사 코코스토리
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    • A23K1/16
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • A23K1/106
    • A23K1/14
    • A23K1/175
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/20Animal feeding-stuffs from material of animal origin
    • A23K10/26Animal feeding-stuffs from material of animal origin from waste material, e.g. feathers, bones or skin
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/30Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms

Abstract

The present invention relates to detoxified sulfur for an ingredient feed and a method for preparing the same. The toxicity of sulfur is removed by the method comprising: a first step of mixing extracts of radish, mung beans, and black beans in water to prepare a mixture composition, and mixing a sulfur powder with the mixture composition, followed by heating and stirring at a predetermined temperature and then cooling, thereby preparing a sulfur mixture; a second step of putting microorganism-impregnated zeolite into the sulfur mixture, and then carrying out fermentation while a predetermined temperature is maintained, thereby preparing a fermented sulfur mixture; a third step of sterilizing, disinfecting, and washing the microorganisms put in the fermented sulfur mixture; and a fourth step of separating sulfur precipitated in the fermented sulfur mixture, which has been gone through the process of sterilizing, disinfecting, and washing microorganisms, and then dehydrating and drying the separated sulfur. The ingredient feed containing the detoxified sulfur prepared by the method of the present invention is used in a stock raising feed for cows, pigs, chickens, and the like, and a culture feed for fishes and the like, the immunity of the stocks and fishes is increased without using antibiotics or facilitators through the expression of excellent sulfur effects, thereby raising stocks and fishes to be healthy; the damage by harmful insects is prevented and controlled, thereby increasing the yield of product and improving the texture, and thus obtaining a product quality improving effect; and especially, the additives and the preparing process, which are required for the present invention, are conveniently and easily used, thereby enabling mass-production, and thus acquiring a ingredient feed containing cheap and high-quality detoxified sulfur.

Description

단미사료용 제독유황 및 그 제조방법{surfur removing poison for feedstuff and its product method}[0001] The present invention relates to a method for preparing a feedstock,

본발명은 단미사료용 유황 및 그 제조방법에 관한 것으로, 보다 상세하게는 무우, 녹두, 검정콩의 혼합조성물을 제조하고, 상기 혼합조성물에 유황분말을 혼합하고, 미생물이 함침된 제오라이트를 투입하여, 유황의 독성을 제거한 제독된 유황을 함유하는 단미사료용 유황 및 그 제조방법에 관한 것이다.More particularly, the present invention relates to a sulfur-containing feed sulfur and a method for producing the sulfur-containing feed sulfur, and more particularly, to a sulfur-containing feed sulfur-containing sulfur produced from a mixed composition of radish, mung bean and black bean, The present invention relates to a sulfur for a short dietary feed containing decontaminated sulfur and a method for producing the same.

일반적으로 단미사료라 함은 등록특허공보 등록특허 10-1070993호에 배경기술로 기재된 바와 같이, 가축 사료 일종으로서, 이는, 감자, 옥수수, 콩 따위의 식물성 원료, 또는, 어분, 골분 등의 동물성 원료, 기타 나트륨, 마그네슘등과 같은 광물성 원료를 재료로 하여 제조되는 것이며, 그 외, 음식물쓰레기를 고온에서 증자(Cooking)한 후 이를 건조, 분쇄, 선별하여 가축의 먹이, 즉, 사료로 제공하게 되는 것이다.
In general, a single feed is a kind of livestock feed as described in the background of JP 10-1070993, which is a vegetable feedstock of potato, corn, soybean, or animal feed such as fish meal, , Other sodium, magnesium and the like. In addition, the food waste is cooked at a high temperature and then dried, crushed, and sorted to provide food for livestock, that is, feed will be.

그리고 본발명에서 단미사료로 사용되는 유황은 주기율표 제16족에 속하는 원자번호 16의 산소족 원소로 원소기호 S로 표기하며 Gas 번호: 7704-34-9, 원자량:32.066, 녹는점:112.8℃(α), 끓는점:444.7℃ 비중:2.07(α)의 광물로 선사시대부터 알려져 왔고 소독, 의약품, 훈증, 천의 표백에 자주 사용하는 비금속으로 많은 황 화합물들이 현대 산업에서 여러 용도로 유용하게 사용되며 생물 분자들도 황을 구성 원소로 갖고 있다.
In the present invention, sulfur used as a feedstuff is an oxygen group element of atomic number 16 belonging to group 16 of the periodic table and is represented by an element symbol S, and is represented by Gas number: 7704-34-9, atomic weight: 32.066, melting point: ), Boiling point: 444.7 ℃ Specific gravity: 2.07 (α) minerals that have been known since prehistoric times and are frequently used as disinfectants, medicines, fumigants and bleaching of fabrics. Many sulfur compounds are useful in many applications in modern industries. The molecules also have sulfur as a constituent.

또한 유황은 해독작용으로 인하여 한의학에서는 광물성 약재중의 하나로 그 약성이 매우 강하여 천연의 유황을 융해하여 잡질을 제거한 후 법제를 하여 만성기관지염, 장양산한, 살충통변, 양위,,나창, 노인한결(, 변비허천, 허한사리, 개선, 기생충구제, 설사, 변비, 딸꾹질, 요충구제, 음낭 및음순의 습양, 급성중이염, 한센병, 만성습진, 신경성피부염, 주사비, 홍피병, 화상등을 다스리는데 사용하였고 현대의학은 면역 및 항암효과의 증대, 인체에너지 생성에 관여하는 비타민인 비오틴, 티아민, 리포산의 구성성분이며 담즙, 타액, 호르몬인 인슐린에도 존재하는 생명을 구성하는 근본물질중의 하나 규정하여 널리 이용되고 있다.
In addition, due to its detoxifying effect, sulfur is one of the mineral chemicals in Oriental medicine, and its weakness is very strong, so it is possible to remove natural substances by removing natural substances, , Constipation Hecheon, Huhan sari, improvement, parasitic relief, diarrhea, constipation, hiccups, mucilage, scrotum and labia, acute otitis media, leprosy, chronic eczema, neurogenic dermatitis, Hyundai medicine is one of the basic materials that constitute the life that exists in the bile, saliva, and hormone insulin, which is a component of biotin, thiamine, and lipoic acid, which are vitamins involved in the production of human energy. .

그러나 유황은 천연의 것은 강산화성 맹독성 광물이므로 제독과정을 거쳐 독성을 순화 제거 시키고 수용화 하여야만 가축 등에의 적용이 가능하다는 단점이 있었다. However, since sulfur is a highly toxic mineral that is a strong oxidizing agent, it has a disadvantage in that it can be applied to livestock and the like only when the toxicity is purified and removed by decolorization.

종래기술로서, 등록특허공보 등록번호 10-1390725호에는 유황이 함유된 양돈사료를 이용한 돼지의 사육방법에 있어서, 상기 양돈 사료는 옥수수, 보리, 밀, 수수, 호밀, 귀리 또는 콩비지로 구성된 곡물원료 20~50중량%, 고구마, 감자, 돼지감자, 타피오카로 구성되는 서류원료 10~30중량%, 엽채류, 근채류 또는 과채류로 구성되는 채소원료 20~40중량% 및 알팔파, 이탈리안라이그라스 등 벼과 또는 콩과의 풀사료원료 5~20중량%를 혼합한 배합사료 100중량부에 법제유황 0.5~2중량부, 효모, 유산균 및 광합성 세균으로 구성되는 EM균 0.05~10중량부, 칼슘(Ca)과 인(P), 나트륨(Na), 칼륨(K), 염소(Cl), 마그네슘(Mg), 철(Fe), 요드(I), 구리(Cu), 코발트(Co), 셀렌(Se) 및 아연(Zn)을 포함하는 무기물 및 비타민 A, B군, D, E, K 및 F의 비타민류를 혼합하여 제조된 유황이 함유된 양돈사료를 급이하는 것을 특징으로 하는 돼지의 사육방법이 공개되어 있다.As a prior art, Patent Registration No. 10-1390725 discloses a method of breeding pigs using a feedstuff containing sulfur, wherein the feedstuff is selected from the group consisting of cereal raw materials consisting of corn, barley, wheat, sorghum, rye, oats, 10 to 30% by weight of a raw material of paper comprising 20 to 50% by weight of sweet potatoes, potatoes, potatoes and tapioca, 20 to 40% by weight of vegetable raw materials comprising leaf vegetables, root vegetables or fruit vegetables, and rice paddies such as alfalfa, 0.5 to 2 parts by weight sulfur, 0.05 to 10 parts by weight of EM bacteria consisting of yeast, lactic acid bacteria and photosynthetic bacteria, 0.5 to 10 parts by weight of calcium (Ca) and phosphorus (P), sodium (Na), potassium (K), chlorine (Cl), magnesium (Mg), iron (Fe), iodine, copper (Cu), cobalt (Co), selenium (Zn), and vitamins A, B, D, E, K, and F, Breeding pigs characterized in that it is in the public domain.

또한, 등록특허공보 등록번호 10-1070993호에는 20~50%의 중량비율을 갖는 법제유황을 주성분으로 하여; 여기에, 탄산칼슘 30~40%의 중량비율; 비타민1~2% 중량비율; 황토1~5%의 중량비율; 숯1~5%의 중량비율; 산토필5~10%의 중량비율; 쑥10~20%의 중량비율로 더 첨가하여 혼합, 조성함을 특징으로 하는 법제유황을 이용한 단미사료가 공개되어 있다.
In addition, Patent Registration No. 10-1070993 discloses a process for the preparation of a polyurethane foam, which comprises, as a main component, a legal sulfur having a weight ratio of 20 to 50%; Here, a weight ratio of 30 to 40% of calcium carbonate; 1 to 2% by weight of vitamins; Weight ratio of 1 to 5% of loess; Weight ratio of char to 1-5%; Weight ratio of Santophil 5-10%; And 10 to 20% by weight of mugwort, and mixing and forming the mixture.

그러나 상기와 같은, 유황이 첨가된 사료 제조에 대한 선행기술에는 많은 방법이 동원되고 있으나 사용되는 첨가제의 수가 너무 많고 그 방법 또한 까다로워 대량생산에는 한계가 있고 유황이 첨가된 사료의 사용의 범용성, 보존성 및 효과발현에 문제점이 있다.However, there have been many methods in the prior art for manufacturing sulfur-containing feeds as described above, but the number of additives used is too large and the method is also complicated. Therefore, there is a limit in mass production, and the versatility, And there is a problem in manifesting the effect.

본발명은 소, 돼지, 닭 등의 축산사료와 물고기 등의 양식사료에 사용하면 뛰어난 유황효과의 발현에 의하여 항생제, 촉진제등을 사용하지 않고 면역성을 높여 튼튼하게 키우고 각종 병충해의 피해를 예방 및 방제하여 생산물의 증산은 물론 조직감을 향상시키므로 품질향상 효과를 얻을 수 있으며 특히 본 발명에 필요 되는 첨가제와 제조공정이 간편 용이하여 대량생산이 가능하여 저렴한 가격의 고품질의 단미사료용 제독유황 및 그 제조방법을 제공하고자 하는 것이다.The present invention relates to a method for preventing and treating damages of various insect pests by raising immunity without using antibiotics, accelerators, etc. by the excellent sulfur effect when it is used in animal feed such as cattle, pigs, In addition, it is possible to obtain a quality improvement effect by improving the texture of the product as well as the production of the product. Particularly, it is possible to mass produce the additive and the manufacturing process required in the present invention, .

본발명은 단미사료용 제독유황 및 그 제조방법에 관한 것으로, 무우, 녹두, 검정콩의 추출물을 물에 혼합하여 혼합조성물을 제조하고, 상기 혼합조성물에 유황분말을 혼합하여 일정온도에서 가열 교반 후 식혀서 유황 혼합물을 제조하는 1단계;The present invention relates to a flue gas for short-term feed and a method for producing the flue gas. The present invention relates to a method for producing a flue gas, A step of preparing a mixture;

상기 유황 혼합물에 미생물이 함침된 제오라이트를 투입하고 일정온도를 유지하고 발효하여 발효된 유황 혼합물을 제조하는 2단계;Adding a zeolite impregnated with a microorganism to the sulfur mixture and fermenting the fermented sulfur mixture while maintaining a constant temperature;

상기 발효된 유황 혼합물에 투입된 미생물을 살균, 소독 및 세척하는 3단계;Sterilizing, sterilizing and washing the microorganisms input into the fermented sulfur mixture;

상기 미생물을 살균, 소독 및 세척한 공정을 거친 발효된 유황 혼합물에 침전되어 있는 유황을 분리하고, 상기 분리된 유황을 탈수한 후 건조하는 4단계;Separating the sulfur precipitated in the fermented sulfur mixture after sterilizing, disinfecting and washing the microorganisms, dehydrating the separated sulfur and drying the separated sulfur;

를 포함하여, 유황의 독성을 제거한 단미사료용 제독유황 제조방법 및 그 제조방법에 관한 것이다.And a method for producing the same. 2. Description of the Related Art

본 발명의 제조방법으로 제조된 유황이 함유된 단미사료를 소, 돼지, 닭 등의 축산사료와 물고기 등의 양식사료에 사용하면 뛰어난 유황효과의 발현에 의하여 항생제, 촉진제등을 사용하지 않고 면역성을 높여 튼튼하게 키우고 각종 병충해의 피해를 예방 및 방제하여 생산물의 증산은 물론 조직감을 향상시키므로 품질향상 효과를 얻을 수 있으며 특히 본 발명에 필요 되는 첨가제와 제조공정이 간편 용이하여 대량생산이 가능하여 저렴한 가격의 단미사료용 고품질 제독 유황을 획득 할 수 있는 현저한 효과가 있다.When the sulfur-containing feed prepared by the method of the present invention is used for animal feed such as cattle, pigs, chickens, and aquaculture feeds such as fish, the excellent sulfur effect can be used to improve the immune response without using antibiotics or accelerators It is possible to obtain a quality improvement effect by enhancing the texture of the product as well as the production of the product by preventing the harmful effects of various insect pests and diseases by enhancing the strength of the product. Of high-quality, low-grade feedstock sulfur.

도 1은 본 발명의 단미사료용 제독유황 제조공정도Fig. 1 is a schematic view showing a process for producing a hydrolysis-

본발명은 단미사료용 제독유황 제조방법에 관한 것으로, 무우, 녹두, 검정콩의 추출물을 물에 혼합하여 혼합조성물을 제조하고, 상기 혼합조성물에 유황분말을 혼합하여 일정온도에서 가열 교반 후 식혀서 유황 혼합물을 제조하는 1단계;The present invention relates to a method of producing a virgin sulfur for short diets, which comprises mixing a mixture of radish, mung bean and black bean extract with water to prepare a mixed composition, mixing the mixture with sulfur powder, heating and stirring at a predetermined temperature, Step 1 to manufacture;

상기 유황 혼합물에 미생물이 함침된 제오라이트를 투입하고 일정온도를 유지하고 발효하여 발효된 유황 혼합물을 제조하는 2단계;Adding a zeolite impregnated with a microorganism to the sulfur mixture and fermenting the fermented sulfur mixture while maintaining a constant temperature;

상기 발효된 유황 혼합물에 투입된 미생물을 살균, 소독 및 세척하는 3단계;Sterilizing, sterilizing and washing the microorganisms input into the fermented sulfur mixture;

상기 미생물을 살균, 소독 및 세척한 공정을 거친 발효된 유황 혼합물에 침전되어 있는 유황을 분리하고, 상기 분리된 유황을 탈수한 후 건조하는 4단계;Separating the sulfur precipitated in the fermented sulfur mixture after sterilizing, disinfecting and washing the microorganisms, dehydrating the separated sulfur and drying the separated sulfur;

를 포함하여, 유황의 독성을 제거한 것을 특징으로 한다.And the toxicity of the sulfur is removed.

또한, 상기 3단계에 사용되는 살균제는 차염산소다, 과산화 수소, 수산화 나트륨, 수산화 칼륨중 어느 하나인 것을 특징으로 한다.In addition, the sterilizing agent used in step 3 is characterized by being any one of sodium hypochlorite, hydrogen peroxide, sodium hydroxide, and potassium hydroxide.

그리고 본발명은 단미사료용 제독유황에 관한 것으로, 상기의 방법중 어느 하나의 방법에 의하여 제조되는 것을 특징으로 한다.
Further, the present invention relates to a desalted sulfur for a short-term feed, characterized in that it is produced by any one of the above-mentioned methods.

본발명을 첨부도면에 의해 상세히 설명하면 다음과 같다. 도 1은 본 발명의 유황 단미사료 제조공정도이다.The present invention will be described in detail with reference to the accompanying drawings. Fig. 1 is a diagram showing a process for producing a sulfur feedstuff of the present invention.

본발명은 1단계에서 무우 뿌리, 녹두, 검정콩을 채집하여 분쇄하여 획득한 추출물을 물에 혼합하여 혼합조성물을 제조하고, 상기 혼합조성물에 유황분말(325mesh 정도)을 혼합하여 일정온도에서 가열 교반 후 식혀서 유황 혼합물을 제조하는 공정이다. In the present invention, a mixed composition is prepared by mixing the extract obtained by collecting and extracting radish roots, green beans and black beans in water in an amount of 1 part, mixing the mixture with water, mixing the mixture with sulfur powder (about 325 mesh) Followed by cooling to prepare a sulfur mixture.

무우는 영양성분이 충실하며 매운맛이 적고, 단맛이 강한 것이 특징으로 아밀라아제, 카탈라아제등의 효소가 고루 함유되어있으며 소화 효소가 많아서 소화를 촉진시키며해독·거담작용이 뛰어나며 수분이 풍부하고 비타민A, 비타민C, 비타민B₁, 칼슘 함유량도 많다.The radish is rich in nutritional ingredients, has a low spicy taste, and is characterized by a strong sweet taste. It contains enzymes such as amylase and catalase. It contains digestive enzymes and promotes digestion. It is excellent in detoxification and genetic function. It is rich in water and contains vitamins A and vitamins C, vitamin B₁, and calcium.

녹두는 맛이 달고 성질은 차가우며, 열을 내리며 더위로 인해 생긴 병을 없애며 독을 풀어주는 작용을 한다.The mung bean has a taste and coldness, and it acts to relieve the poison by removing the heat caused by the heat by lowering the heat.

검정콩은 비티민B와 필수아미노산 등을 많이 포함하고 있어 영양이 풍부하며 청열해독 작용이 있다.
Black beans contain B vitamins B and essential amino acids, so they are nutritious and have a detoxifying effect.

혼합조성물의 혼합비율은 물100중량부에 대하여, 무우 35 ~ 45중량부, 녹두 35 ~ 45중량부, 검정콩 15 ~ 25중량부를 혼합한다.The mixing ratio of the mixed composition is 35 to 45 parts by weight of radish, 35 to 45 parts by weight of mung bean and 15 to 25 parts by weight of black soybean to 100 parts by weight of water.

무우가 35중량부 미만일 경우에는 유황에 대한 해독효과가 저감되고, 45중량부를 초과할 경우에는 수분함량이 높아 생산에 어려움이 생긴다. 녹두가 35중량부 미만일 경우에는 유기비료내 영양분이 줄어들게 되어 시비효과가 낮아지고 45중량부를 초과할 경우에는 유황의 양이 상대적으로 적어져서 본발명의 효과가 감소되며, 검정콩이 15중량부 미만일 경우에는 유기비료내 영양분이 줄어들게 되어 시비효과가 낮아지고, 25중량부를 초과할 경우에는 유황의 양이 상대적으로 적어져서 본발명의 효과가 감소된다.When the radish is less than 35 parts by weight, the detoxifying effect against sulfur is reduced. When the radish is more than 45 parts by weight, the moisture content is high, which makes production difficult. When the mung bean is less than 35 parts by weight, the nutrients in the organic fertilizer are reduced and the fertilizing effect is lowered. When the content is more than 45 parts by weight, the effect of the present invention is reduced because the amount of sulfur is relatively small. The nutrients in the organic fertilizer are reduced and the fertilizing effect is lowered. When the amount exceeds 25 parts by weight, the amount of sulfur is relatively small, and the effect of the present invention is reduced.

그리고 유황분말(325Mesh) 100중량부에 대하여, 제조된 유황혼합물 50 ~ 100중량부를 혼합 침지시켜 압력용기에서 100~110℃를 유지하면서 1시간 간격으로 정, 역회전의 방식으로 12시간 교반하고 상온으로 식혀서 유황분말이 추가된 용액인 유황혼합물을 제조하는 것이다. 유황혼합물이 50 중량부 미만일 경우에는 제독이 잘되지 않으며, 100중량부를 초과하면 상대적으로 유황의 효과가 감소된다.
Then, 50 to 100 parts by weight of the prepared sulfur mixture was mixed and immersed in 100 parts by weight of sulfur powder (325 Mesh), stirred at an interval of one hour in a forward and reverse rotation manner for 12 hours while maintaining 100 to 110 ° C in a pressure vessel, To prepare a sulfur mixture which is a solution in which the sulfur content is added. When the sulfur mixture is less than 50 parts by weight, admiral deterioration is poor. When the amount exceeds 100 parts by weight, the effect of sulfur is relatively decreased.

2단계에서는 상기 1단계를 거친 유황 혼합물에 미생물인 Thiospiorillum균, Streptomyces균, Azospirillum균중 어느 하나 또는 두 종류 이상이 함침된 제오라이트를 투입하여 40 ~ 70℃를 유지하여 3일간 발효하는 공정이다.In step 2, zeolite impregnated with one or more of the microorganisms Thiospiorillum, Streptomyces and Azospirillum is added to the sulfur mixture which has been subjected to the above step 1, and the fermentation is carried out for 3 days by maintaining the temperature at 40 to 70 ° C.

상기 1단계를 거친 유황 혼합물 100중량부에 대하여, 미생물이 함침된 제오라이트 5 ~ 15중량부를 혼합하여 제오라이트가 혼합된 혼합물을 제조한다. 미생물이 함침된 제오라이트가 5중량부 미만이면 유황 단미사료의 무게가 너무 가벼워져 사용이 불편하며, 15중량부를 초과하면 유황 단미사료의 무게가 무거워져서 사용이 불편해진다.5 to 15 parts by weight of zeolite impregnated with microorganisms are mixed with 100 parts by weight of the sulfur mixture which has been subjected to the first step to prepare a mixture in which the zeolite is mixed. If the zeolite impregnated with the microorganism is less than 5 parts by weight, the weight of the sulfur semi-synthetic feed becomes too light, which is inconvenient to use. If the amount of the zeolite is more than 15 parts by weight, the weight of the sulfur semi-synthetic feed becomes heavy.

그리고 미생물을 제오라이트에 홍색유황세균인 Thiospiorillum균1012 , 유기물 분해세균인 Streptomyces균1012 , 유해물질 흡수세균인 Azospirillum균1012 중 어느 하나 또는 두 종류 이상을 함침하는 비율은 제오라이트 100중량부에 대하여 0.1 ~ 3중량부를 투입한다. 미생물이 0.1 중량부 미만이면 발효가 잘되지 않고 3중량부를 초과하면 제조단가가 비싸지며, 후공정인 미생물 살균, 소독, 세척공정에 시간 및 비용이 많이 발생한다.
The microorganisms were identified as zeolite, Thiospiorillum 10 12 , which is a red sulfur bacterium, Streptomyces bacterium 10 12 , Azospirillum bacteria 10 12 And 0.1 to 3 parts by weight based on 100 parts by weight of the zeolite. If the amount of the microorganism is less than 0.1 part by weight, the fermentation does not proceed well. If the amount is more than 3 parts by weight, the manufacturing cost is high, and the microbial sterilization, disinfection,

3단계는 상기 2 단계를 거친 발효된 유황 혼합물의 미생물을 살균, 소독 및 세척하는 공정이다.Step 3 is a step of sterilizing, disinfecting and washing microorganisms of the fermented sulfur mixture through the two steps.

이때 사용되는 살균제는 차염산소다, 과산화 수소, 수산화 나트륨, 수산화 칼륨중 어느 하나 또는 2개 이상을 동시 사용한다.At this time, any one or two or more of sodium hypochlorite, hydrogen peroxide, sodium hydroxide and potassium hydroxide are used simultaneously.

4단계는 상기 3단계를 거쳐서 미생물을 살균, 소독 및 세척한 발효된 유황 혼합물에 침전되어 있는 유황을 필터를 사용하여 분리하고, 상기 분리된 유황을 관용의 탈수기로 탈수한 후, 관용의 건조기를 사용하여 건조하는 공정이다. 건조공정은 70 ~ 80℃에서 4시간 정도 건조하거나 또는 상온에서 건조한다.In step 4, the sulfur precipitated in the fermented sulfur mixture sterilized, sterilized and washed through the above three steps is separated by using a filter, the separated sulfur is dehydrated by a conventional dehydrator, And drying. Drying is carried out at 70 ~ 80 ℃ for 4 hours or at room temperature.

상기 1 내지 4단계를 거쳐서 본발명의 유황의 독성을 제거한 제독유황을 제조하고 상기와 같이 제조된 제독유황은 단미사료의 원료로 사용된다.
The above step 1 to step 4 are used to prepare an admiral sulfur in which the toxicity of the sulfur of the present invention is removed, and the adduct sulfur produced as described above is used as a feedstock for a short-term feed.

따라서 본 발명의 제조방법으로 제조된 제독유황을 함유한 단미사료를 소, 돼지, 닭 등의 축산사료와 물고기 등의 양식사료에 사용하면 뛰어난 유황효과의 발현에 의하여 항생제, 촉진제등을 사용하지 않고 면역성을 높여 튼튼하게 키우고 각종 병충해의 피해를 예방 및 방제하여 생산물의 증산은 물론 조직감을 향상시키므로 품질향상 효과를 얻을 수 있으며 특히 본 발명에 필요 되는 첨가제와 제조공정이 간편 용이하여 대량생산이 가능하여 저렴한 가격의 고품질 유황 단미사료를 획득 할 수 있는 현저한 효과가 있다.Therefore, when the feedstuff containing the admiral sulfur produced by the method of the present invention is used for animal feed such as cattle, pigs, chickens, and aquaculture feeds such as fish, the use of antibiotics, accelerators and the like It is possible to obtain a quality improvement effect by enhancing the immunity and strengthening it, and preventing and controlling the damage of various insect pests and diseases, as well as the production of the product and improving the texture, and in particular, the additive and the manufacturing process necessary for the present invention can be easily performed, There is a remarkable effect that can obtain high-quality sulfur low-cost feed of low price.

Claims (3)

물100중량부에 대하여, 무우 35 ~ 45중량부, 녹두 35 ~ 45중량부, 검정콩 15 ~ 25중량부를 혼합하여 혼합조성물을 제조하고, 유황분말 100중량부에 대하여, 제조된 유황혼합물 50 ~ 100중량부를 혼합 침지시켜 압력용기에서 100~110℃를 유지하면서 1시간 간격으로 정, 역회전의 방식으로 12시간 교반하고 상온으로 식혀서 유황분말이 추가된 용액인 유황혼합물을 제조하는 1단계;
상기 1단계를 거친 유황 혼합물에 미생물인 Thiospiorillum균, Streptomyces균, Azospirillum균 중 어느 하나 또는 두 종류 이상이 함침된 제오라이트를 투입하여 40 ~ 70℃를 유지하여 3일간 발효하여 발효된 유황 혼합물을 제조하는 2단계;
상기 발효된 유황 혼합물에 투입된 미생물을 살균, 소독 및 세척하되, 살균제는 차염산소다, 과산화 수소, 수산화 나트륨, 수산화 칼륨중 어느 하나인 3단계;
상기 미생물을 살균, 소독 및 세척한 공정을 거친 발효된 유황 혼합물에 침전되어 있는 유황을 분리하고, 상기 분리된 유황을 탈수한 후 건조하되, 건조공정은 70 ~ 80℃에서 4시간 정도 건조하거나 또는 상온에서 건조하는 4단계;
를 포함하여, 유황의 독성을 제거한 단미사료용 제독유황 제조방법
35 to 45 parts by weight of radish, 35 to 45 parts by weight of mung bean and 15 to 25 parts by weight of black soybean are mixed with 100 parts by weight of water to prepare a mixed composition. To 100 parts by weight of the sulfur powder, And stirring the mixture for 12 hours at a time interval of 1 hour while maintaining the temperature at 100 to 110 ° C in a pressure vessel for 12 hours and cooling to room temperature to prepare a sulfur mixture as a sulfur solution added solution;
The zeolite impregnated with any one or two or more of Thiospiorillum, Streptomyces and Azospirillum, which are microorganisms, is added to the sulfur mixture which has been subjected to the above step 1, and the fermented sulfur mixture is fermented for 3 days while maintaining the temperature at 40 to 70 ° C Step 2;
Sterilizing and washing the microorganisms put into the fermented sulfur mixture, wherein the bactericide is any one of sodium hypochlorite, hydrogen peroxide, sodium hydroxide, and potassium hydroxide;
The sulfur precipitated in the fermented sulfur mixture having been subjected to the sterilization, disinfection and washing processes of the microorganisms is separated, the separated sulfur is dehydrated and dried, and the drying process is carried out at 70 to 80 ° C. for about 4 hours or Four stages of drying at room temperature;
, A method for producing a flue gas for short-term feed, which eliminates the toxicity of sulfur
삭제delete 제1항의 방법에 의하여 제조되는 것을 특징으로 하는 단미사료용 제독유황
Claims [1] A method for producing a detergent sulfur for a short-term feed, which is produced by the method of claim 1
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KR102027581B1 (en) * 2018-05-02 2019-10-01 주식회사 평강비아이엠 Method for producing a formulated feed
KR20220029194A (en) * 2020-09-01 2022-03-08 나라바이오주식회사 Composition for growth promoting comprising non-toxic-sulfur an active ingredient

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KR20100019914A (en) * 2008-08-11 2010-02-19 박상효 Feed composition containing sulphur and manufacturing process thereof uising fermentation
KR20110002901A (en) * 2009-07-03 2011-01-11 권성중 Legal Sulfur Feed Additives

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Publication number Priority date Publication date Assignee Title
KR20100019914A (en) * 2008-08-11 2010-02-19 박상효 Feed composition containing sulphur and manufacturing process thereof uising fermentation
KR20110002901A (en) * 2009-07-03 2011-01-11 권성중 Legal Sulfur Feed Additives

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102027581B1 (en) * 2018-05-02 2019-10-01 주식회사 평강비아이엠 Method for producing a formulated feed
KR20220029194A (en) * 2020-09-01 2022-03-08 나라바이오주식회사 Composition for growth promoting comprising non-toxic-sulfur an active ingredient
KR102488267B1 (en) 2020-09-01 2023-01-16 나라바이오 주식회사 Composition for growth promoting comprising non-toxic-sulfur an active ingredient

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