KR101514041B1 - Wood-cultivated ginseng Kyoung-ok-ko and method for preparing the same - Google Patents
Wood-cultivated ginseng Kyoung-ok-ko and method for preparing the same Download PDFInfo
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- KR101514041B1 KR101514041B1 KR1020120150846A KR20120150846A KR101514041B1 KR 101514041 B1 KR101514041 B1 KR 101514041B1 KR 1020120150846 A KR1020120150846 A KR 1020120150846A KR 20120150846 A KR20120150846 A KR 20120150846A KR 101514041 B1 KR101514041 B1 KR 101514041B1
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- ginseng
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- honey
- goat
- gypsum
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Abstract
본 발명은 산양삼경옥고 및 이의 제조방법에 관한 것이다. 본 발명에 따른 산양삼경옥고 및 이를 포함하는 현탁음료는 기존의 시판되는 경옥고를 포함하는 현탁음료보다 기호도 및 저장성이 우수하여, 일상생활에서 섭취가 가능한 건강 기능성 식품으로 산양삼의 이용가치를 증대시킬 수 있고, 전통적인 건강식품이나 수출가능한 문화상품으로 유용하게 이용될 수 있다.The present invention relates to a gypsum gypsum gypsum and a method for producing the same. The ginseng saponaceus japonica according to the present invention and the suspension drink containing the ginseng saponaceous ginseng according to the present invention are superior to the conventional commercially available ginseng cheonggok containing preference drink and storage property and can be used as a health functional food which can be ingested in daily life, , Can be useful as a traditional health food or an exportable cultural product.
Description
본 발명은 산양삼경옥고 및 이의 제조방법에 관한 것이다.
The present invention relates to a gypsum gypsum gypsum and a method for producing the same.
최근 국내외 전반적인 음료시장은 그 동안 주력제품으로 여겨져 왔던 탄산음료나 주스류 등의 일반음료 제품들의 침체 분위기를 겪고 있는 반면, 건강 기능적인 성격이 강한 음료시장은 지속적으로 성장하고 있다. 이는 현대인들의 생활방식과 식생활 변화, 질병 형태 다양화 등 여러 사회적 여건이 변화되고 있는데 기인하며, 현대인의 건강에 대한 관심 증대는 건강 기능성 음료 시장의 쾌속성장과 틈새 수요를 지속적으로 창출하고 있다.In recent years, the domestic beverage market has been experiencing a recession in general beverage products such as carbonated beverages and juices, which have been regarded as flagship products in recent years. This is due to changes in social conditions such as lifestyle, dietary life, and disease diversification of modern people, and the increasing interest in health of modern people is continuously creating rapid growth and niche demand of health functional beverage market.
산양삼은 오가피과(주릅나무과 ; Araliaceae)에 속하는 다년생 초목인 인삼(panax ginseng C. A. meyer)이 야생상태에서 자연 발아하여 성장한 것을 말하며, 한방에서는 예로부터 대표적인 보기약이면서 영약으로 여겨져 왔다. 산삼은 예로부터 원기를 북돋워주고 활발한 두뇌활동과 정신력을 강하게 하는 한편 인체의 저항력을 증가시켜 각종 발병으로부터 면역기능과 자연치유력을 높여주는 작용을 한다고 알려져 있다. 또한 각종 성인병이나 수험생의 스트레스 해소 등에 탁월한 효능이 있다고 전해져 왔다. 이를 바탕으로 산양삼에 대한 연구가 진척되어 최근 항암, 혈압강하, 항산화, 간독성, 지질강하 등에 효능이 있음이 확인되었다.Goat ginseng is a perennial plant belonging to the genus Araliaceae ( Panax ginseng CA meyer) grown in the natural germination and growth in the wild, and has been regarded as a representative medicine in the past and has been regarded as an agar. The ginseng has been known to enhance the immune function and natural healing power from various diseases by increasing the resistance of the human body while strengthening vigorous brain activity and mental strength. It has also been reported that it has excellent efficacy in relieving stress of various adult diseases and examinees. Based on this, research on goat ginseng has been progressed and it has recently been confirmed that it is effective for anticancer, blood pressure reduction, antioxidation, hepatotoxicity and lipid lowering.
경옥고는 인삼, 복령, 생지황, 꿀 등을 구성약재로 하는 고형제제로 동의보감과 방약합편에 처방과 제법이 수제된 보혈강장제이다. 동의보감 하기에는 경옥고의 약효에 대하여 “진정(塡精), 보수(補髓), 조진양생(調眞養性), 반노환동(返老還童)하며 백손(百損)을 보하고 백병(百病)을 제거하며, 만신(萬神)이 모두 족하고 오장(五臟)을 영일(盈溢)하며 백발(白髮)을 검게하고 낙치(落齒)가 다시 나며 분마(奔馬)처럼 달리게 한다” 라고 기재되어 있다. 또한 방약합편에는 “정(精)을 채우고 수(髓)를 보하여, 모발을 검게 하고 치아를 나게 하고 만신(萬神)이 구족(俱足)하여 백병(百病)을 제거한다” 고 기록되어 민간에서도 이를 자양강장 및 허약체질 개선에 널리 사용해왔다. 이러한 문헌적 자료에 기초하여 경옥고의 약리활성에 대한 연구가 활발히 진행되고 있으며, 현재까지 항염증, 위궤양억제, 진통효과 및 정상체온유지, 혈당강하, 혈압강하, 체중감소 및 지구력 증진에 효과가 있음이 알려져 있다.Gyeongokgyo is gyeongokgyo is a medicine that is composed of ginseng, gyeongryeong, rawjihwanghwa, honey, etc. It is a prescription medicine and a prescription medicine. In order to see Donguibogyou, I would like to ask about the medicinal efficacy of Kyoung - Ok 's "Serenity, Remuneration, Cure, Renewal, and Baekson (100 diseases) And all mankind are all satisfied, and the five-year-old is a young man, and his white hair is blackened, and he falls again and runs like a horse. " In addition, it is said that "I fill the jin (精) and see the number (髓)", and the hair is blackened, the teeth are bloomed, And it has been widely used in the private sector for the improvement of nourishing strength and fragility. Based on these literature data, research on the pharmacological activity of Gyeongokgyo has been actively carried out and it is effective for anti-inflammation, gastric ulcer suppression, analgesic effect and maintenance of normal body temperature, hypoglycemia, hypotension, weight loss and endurance enhancement Is known.
최근 기능성이 강화된 경옥고 또는 기존의 경옥고를 이용한 건강식품을 개발하려는 노력이 꾸준히 진행되어 왔다. 예를 들어 대한민국 특허등록 제 10-28639호에는 반고형 죽상태의 종래 경옥고에 한천, 설탕, 팟앙금, 올리고당 등을 가하고 가열하여 제조된 양갱형 또는 젤리형 경옥고 및 그 제조방법이 개시되어 있고, 대한민국 특허등록 제 10-354962호에는 경옥고 용액을 추출하여 동결건조한 분말에 포도당, 인삼향 및 젖산을 포함하는 경옥고 즉석차 및 그 제조방법이 개시되어 있으며, 대한민국 특허등록 제 10-1016195호에는 천마를 넣어 제조한 경옥고 및 그 제조방법이 개시되어 있다. 또한 대한민국 특허공개공보 제 10-1994-6595호에는 인삼농축액기스, 숙지황추출물, 백복령추출물 및 벌꿀을 포함하며 여기에 물을 가하고 균질화시키고 멸균시켜서 제조된 경옥고 액제 및 그의 제조방법이 개시되어 있고, 대한민국 특허공개공보 제 10-2001-79241호에는 생지황, 인삼, 백복령 이외의 대추, 맥문동, 녹용, 구기자 등을 포함하는 기능성이 향상된 경옥고 및 그 제조방법이 개시되어 있다. Recently, efforts have been made to develop health foods using functional mushrooms or conventional mushrooms. For example, Korean Patent Registration No. 10-28639 discloses an omelette-shaped jelly-like jellyfish prepared by adding agar, sugar, potato wool, oligosaccharide, and the like to a conventional jelly-bean jelly in a semi-solid state and its production method, Korean Patent Registration No. 10-354962 discloses a gyeongokgyo instant tea containing glucose, ginseng flavor and lactic acid and a preparation method thereof, which is obtained by extracting a gyeongokgok solution and lyophilizing the powder. Korean Patent Registration No. 10-1016195 discloses a tea gum And a process for producing the same. Also, Korean Patent Laid-Open Publication No. 10-1994-6595 discloses a gyeongokgol solution prepared by adding water, homogenizing and sterilizing ginseng-enriched liquorice, waterweed extract, extract of Baekbokryeong and honey, and a process for producing the same. Japanese Laid-Open Patent Publication No. 10-2001-79241 discloses a mushroom of improved functionality including a fresh persimmon, a ginseng, a jujube other than Baekbokryeong, a ginseng root, a deer antler, a ginger and the like and a manufacturing method thereof.
상기와 같은 약재로의 산양삼의 이용은 그 사용범위를 지나치게 국한시켜 이용가치를 온전히 활용하지 못하는 문제점이 있어 다른 대체상품으로 개발하는 것이 요구되고 있는 실정이다. The use of goat's ginseng as a medicament as described above is restricted to a limited extent of its use and it is required to develop it as another substitute product because it can not fully utilize its utilization value.
이에 본 발명자들은 최고의 보약임에도 불구하고 경옥고의 장기 복용에 따른 비위생적인 보관, 휴대가 어려운 점, 한정된 소비자 층, 가격의 부담 등으로 인한 대중적인 판매의 어려움 및 섭취의 불편함을 극복하고 일상생활에서 산양삼의 섭취가 가능한 건강 기능성 식품을 개발하고자 예의 연구 노력한 결과, 산양삼경옥고의 제조 및 이를 이용한 현탁음료를 제조함으로써, 기존의 시판되는 경옥고를 이용한 현탁음료보다 기호도 및 저장성이 우수함을 확인하여 본 발명을 완성하였다.
Therefore, the inventors of the present invention have found that, although they are the best preservatives, they can overcome the difficulty of popular sales and the inconvenience of ingestion due to unhygienic storage, difficulty to carry, limited consumer floor, As a result of intensive research to develop a health functional food capable of ingesting goat's ginseng, it was confirmed that the present invention is superior to the conventional commercially available gypsum-based suspension drink by the preparation of the goat ginseng kyokoko and the suspension drink using the same, Completed.
본 발명의 목적은 산양삼경옥고 및 이의 제조방법을 제공하는 것이다.It is an object of the present invention to provide a gypsum gypsum gypsum and a method of producing the same.
본 발명의 또 다른 목적은 산양삼경옥고를 포함하는 현탁음료를 제공하는 것이다.
Yet another object of the present invention is to provide a suspension drink containing ginseng mushroom.
상기 과제를 해결하기 위해서, 본 발명은 산양삼경옥고 및 이의 제조방법을 제공한다. In order to solve the above-mentioned problems, the present invention provides a gypsum gypsum gypsum and a method for producing the same.
또한, 본 발명은 산양삼경옥고를 포함하는 현탁음료를 제공한다.
In addition, the present invention provides a suspension beverage comprising ginseng root mushroom.
본 발명에 따른 산양삼경옥고 및 이를 포함하는 현탁음료는 기존의 시판되는 경옥고를 포함하는 현탁음료보다 기호도 및 저장성이 우수하여, 일상생활에서 섭취가 가능한 건강 기능성 식품으로 산양삼의 이용가치를 증대시킬 수 있고, 전통적인 건강식품이나 수출가능한 문화상품으로 유용하게 이용될 수 있다.
The ginseng saponaceus japonica according to the present invention and the suspension drink containing the ginseng saponaceous ginseng according to the present invention are superior to the conventional commercially available ginseng cheonggok containing preference drink and storage property and can be used as a health functional food which can be ingested in daily life, , Can be useful as a traditional health food or an exportable cultural product.
도 1은 진세노사이드(Ginsenoside) Rb1, Rg1, Rg3 표준품의 분석 결과를 나타낸 도이다.
도 2는 본 발명의 산양삼경옥고의 진세노사이드 Rb1, Rg1, Rg3 분석 결과를 나타낸 도이다.
도 3은 본 발명의 산양삼경옥고 현탁음료와 시중 제품 현탁음료의 QDA 묘사분석 도이다.
도 4은 본 발명의 산양삼경옥고 현탁음료의 저장기간별 온도에 따른 당도 변화를 나타낸 도이다.
도 5는 본 발명의 산양삼경옥고 현탁음료의 저장기간별 온도에 따른 pH 변화를 나타낸 도이다.
도 6은 본 발명의 산양삼경옥고 현탁음료의 저장기간별 온도에 따른 산도 변화를 나타낸 도이다.BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a diagram showing the results of analysis of standard products of Ginsenoside Rb1, Rg1, and Rg3.
FIG. 2 is a graph showing the results of analysis of ginsenosides Rb1, Rg1 and Rg3 of the goat ginseng herbaceous plant of the present invention.
FIG. 3 is a QDA depiction analysis chart of the goat ginseng mushroom hot drink of the present invention and a commercial product suspension drink.
FIG. 4 is a graph showing changes in sugar content according to the storage time according to the storage time of the goat's milk jellyfish suspension drink of the present invention.
FIG. 5 is a graph showing the change in pH of the ginseng saplings of the present invention according to the storage time according to the temperature.
FIG. 6 is a graph showing changes in acidity of the ginseng saponaceous mushroom suspension of the present invention at various storage times according to temperature.
본 발명은 산양삼 5-10중량%, 백복령 10-20중량%, 생지황 20-50중량% 및 꿀 30-60중량%를 포함하는 산양삼경옥고를 제공한다.The present invention provides a gypsum gypsum gypsum comprising 5-10% by weight of goose ginseng, 10-20% by weight of white roots, 20-50% by weight of raw persimmon and 30-60% by weight of honey.
이하, 본 발명에 대해 상세히 설명한다.Hereinafter, the present invention will be described in detail.
일반적으로 경옥고는 인삼, 복령, 생지황, 꿀 등을 구성약재로 하는 고형제제로 동의보감과 방약합편에 처방과 제법이 수제된 보혈강장제이다.Generally, Gyeongokgyo is a medicine which is composed of ginseng, gyeongryeong, bamboo, honey,
본 발명의 산양삼경옥고는 백복령, 생지황즙 및 꿀 등 경옥고 제조시에 사용되는 재료에서 인삼 대신 산양삼을 첨가한 것으로, 바람직하게는 산양삼분말을 적절한 비율로 혼합하여 제조한 신규한 건강 보조 식품을 말한다.The ginseng ginseng cake of the present invention refers to a novel health supplement food prepared by adding goat ginseng instead of ginseng in a material used in the production of kyangokgol such as baekbokgyeong, bokbujang juice and honey and preferably mixing raw ginseng powder with an appropriate ratio.
본 발명의 산양삼경옥고의 주요성분인 산양삼, 백복령, 생지황즙 및 꿀의 효능은 하기와 같다.The efficacy of ginseng root, baekbokryeong, jujube juice and honey, which are the main components of the goat ginseng mushroom of the present invention, is as follows.
상기 산양삼은 오가피과(주릅나무과 ; Araliaceae)에 속하는 다년생 초목인 인삼(panax ginseng C. A. Meyer)이 야생상태에서 자연 발아하여 성장한 것을 말한다. 원기를 북돋우고 두뇌활동을 활발하게 하며 정신력을 강하게 한다. 또한 면역기능과 자연치유력을 높여주고 성인병이나 수험생의 스트레스 해소 등에 탁월한 효능이 있다. 성분으로는 ginsengsaponon(ginsenoside Rb1, Rb2, Rg1, Rg2, Rg3, Rd, Re, Rh1, Rh2) 등과 많은 종류의 아미노산, 당류, 비타민, 플라보노이드, 무기질 등이 함유되어 있다. 최근에는 항암, 혈압강하, 항산화, 간독성, 지질강하 등에 효능이 있음이 확인되었다. 본 발명의 산양삼경옥고에서 산양삼은 산양삼경옥고 총 중량에 대해 5-10중량% 포함하는 것이 바람직하다. 만일 산양삼이 5중량% 미만이면 산양삼 특유의 풍미가 적어지고, 10중량% 를 초과하면 쓴맛이 강해져 기호도 떨어지게 된다.The above-mentioned goat ginseng refers to a ginseng ( panax ginseng CA Meyer), a perennial plant belonging to the genus Araliaceae, grown by natural germination in the wild state. It encourages excitement, stimulates brain activity, and strengthens mental strength. It also enhances immune function and natural healing power, and has excellent efficacy in relieving stress of adult diseases and examinees. Ingredients include ginsengsaponon (ginsenoside Rb1, Rb2, Rg1, Rg2, Rg3, Rd, Re, Rh1, Rh2) and many other amino acids, sugars, vitamins, flavonoids and minerals. In recent years, it has been found to be effective for anticancer, hypotensive, antioxidant, hepatotoxicity and lipid lowering. It is preferable that the goat ginseng is 5-10 wt% based on the total weight of the goat ginseng jelly. If the amount of goat's ginseng is less than 5% by weight, the flavor specific to goat's ginseng is reduced. If the amount exceeds 10% by weight, the bitter taste is intensified and the taste is lowered.
상기 백복령은 구멍장이 버섯과의 복령(Poria cocos (Fr.) Wolf)의 균핵을 건조시킨 것이다. 소변을 잘 못보고 배와 전신이 붓는 증상에 효력을 나타내며 해수, 구토, 설사와 가슴이 뛰고 잘 놀라며, 건망증, 유정을 치료한다.신장 부종에도 현저한 반응을 나타낸다. 성분으로서 대표적인 것은 β-pachyman이 약 90%에 이르고 pachymic acid, 단백질, 포도당 등이 함유되어 있다. 흰쥐의 유문부 결찰로 인한 궤양형성을 예방하는 효과가 있고, 다당체는 악성 종양에 있어서 면역증강기능, 만성정신분열증에 효력이 있었고, 간기능을 호전시킨다. 본 발명의 산양삼경옥고에서 백복령은 산양삼경옥고 총 중량에 대해 10-20중량% 포함하는 것이 바람직하다. 만일 백복령 함량이 10중량% 미만이면 백복령의 맛을 줄 수 없고, 20중량% 를 초과하면 기타 재료의 첨가량이 적어짐에 따라 백복령의 맛이 강하고 맛과 향 등에서 기타 재료와의 조화가 이루어지지 않는다.The Baek Bok-ryeong was dried sclerotia of Poria cocos (Fr.) Wolf with the hole mushroom. It is effective for symptom of swelling of the abdomen and whole body. It treats sea water, vomiting, diarrhea and heartbeat and is surprised, forgetfulness and oil well. It also shows remarkable response to kidney edema. Representative of the component is about 90% of β-pachyman, including pachymic acid, protein, and glucose. It has the effect of preventing the ulcer formation by the pyloric ligation of the rats. The polysaccharide is effective for immunity enhancement, chronic schizophrenia and improve liver function in malignant tumor. In the present invention, it is preferable that Baekbokryeong is contained in 10-20% by weight with respect to the total weight of the goat ginseng mushroom. If the content is less than 10% by weight, flavor of white roux can not be obtained. If it exceeds 20% by weight, the amount of other ingredients is decreased, and thus flavor of white roux is strong and flavor and aroma are not harmonized with other ingredients.
상기 생지황은 현삼과의 여러해살이풀 지황(Rehmannia glutinosa Liboschitz), 회경지황(Rehmannia glutinosa Libosch. for. hueichingensis Hshlao)의 날 뿌리를 말한다. 생지황은 당뇨병에 좋으며, 토혈, 코피, 자궁출혈을 그치게 하고, 생리불순, 변비에 좋다. 성분은 β-sistosterol, 미량의 campesterol, rehmanin, alkaloid,지방산 등이 확인되었다. 약리적으로 혈당을 내리고, 순환기계통에 작용하여 강심 및 이뇨 작용을 보이며, 간기능 보호작용, 항균작용이 있다. 본 발명의 산양삼경옥고에서 생지황은 산양삼경옥고 총 중량에 대해 20-50중량% 포함하는 것이 바람직하다. 생지황즙은 몸의 열을 내려주는 것으로 알려져 있으며, 중량비 20중량% 미만 혼합되면 해열효과가 약하고 50중량% 를 초과하여 혼합되면 해열효과에 큰 차이가 없고 쓴 맛이 강하다.The bamboo shoots are root of Rehmannia glutinosa Liboschitz, Rehmannia glutinosa Libosch. For hueichingensis Hshlao, with hymen. Bamboo leaf is good for diabetes, and it stops bleeding, nosebleeds and uterine bleeding, and it is good for menstrual irregularity and constipation. Β-sistosterol, traces of campesterol, rehmanin, alkaloid, and fatty acids were identified. It is pharmacologically reducing blood sugar, acting on the circulatory system, showing a strong heart and diuretic action, liver function protective action, antibacterial action. It is preferable that the raw persimmon in the goat ginseng mushroom of the present invention is 20-50 wt% based on the total weight of the goat mushroom gum. The jujube juice is known to lower the heat of the body, and when the weight ratio is less than 20% by weight, the antipyretic effect is weak and when the antioxidant is mixed by more than 50% by weight, there is no significant difference in the antipyretic effect and the bitter taste is strong.
상기 꿀은 밀원(蜜源)에 따라 약간의 차이가 있기는 하나, 대체로 탄수화물이 78% 가량인데 이중 과당이 47%. 포도당이 37% 정도로 되어 있고 소화성이 좋고 흡수가 잘된다. 수분이 17% 가량이고 0.2% 가량의 단백질과 무기질이 있고 비타민, 개미산, 유산, 사과산, 색소, 방향물질, 고무질, 왁스, 화분 등이 들어있다. 비타민류는 B1, B2, B6 엽산, 판토텐산, 니아신, C 등이 있고 무기지로는 Ca, Fe, Cu, Mn, P, S, K, Cl, Na, Si, Mg 등이 함유된다. 본 발명의 산양삼경옥고에서 꿀은 산양삼경옥고 총 중량에 대해 30-60중량% 포함하는 것이 바람직하다. 만일 꿀이 30중량% 미만 혼합되면 점도가 너무 낮고, 60중량%를 초과하면 점도가 너무 높아 기타 재료들의 혼합이 균일하지 못하다.
Although the honey is slightly different depending on the honey source, it is generally about 78% of the carbohydrate, and the fructose is 47%. Glucose is about 37%, has good digestibility and is well absorbed. It contains about 17% moisture and about 0.2% protein and minerals. It contains vitamins, formic acid, lactic acid, malic acid, coloring matters, aromatic materials, gummies, waxes and pollen. Vitamins include B1, B2, and B6 folic acid, pantothenic acid, niacin, and C, and inorganic minerals include Ca, Fe, Cu, Mn, P, S, K, Cl, Na, Si and Mg. In the present invention, it is preferable that the honey be included in 30-60 wt% of the total weight of the ginseng mushroom. If less than 30% by weight of honey is mixed, the viscosity is too low, and if it exceeds 60% by weight, viscosity is too high to mix the other ingredients.
또한, 본 발명은, Further, according to the present invention,
1) 산양삼, 인삼 및 백복령을 각각 분말화 하는 단계;1) powdering the goat ginseng, ginseng, and bokbok;
2) 생지황을 분쇄하고 즙을 내고, 걸러주어 생지황즙을 얻는 단계;2) pulverizing raw persimmon, juicing and filtering to obtain raw persimmon juice;
3) 꿀을 50-70℃ 에서 15 내지 30분간 물중탕하여 흰 거품과 수분을 제거하고 연밀을 제조하는 단계;3) water-bathing the honey at 50-70 ° C for 15-30 minutes to remove white foam and moisture and make a mill;
4) 상기 산양삼 분말, 인삼 분말, 백복령 분말, 생지황즙 및 연밀을 혼합하는 단계; 및4) mixing the ginseng powder, ginseng powder, Baekbokryeong powder, fresh persimmon juice and millet; And
5) 상기 혼합물을 1차 중탕, 냉각 및 2차 중탕한 후, 실온에서 냉각시켜 산양삼경옥고를 제조하는 단계를 포함하는, 산양삼경옥고의 제조방법을 제공한다.5) a step for preparing the goat ginseng jellyfish by firstly warming the mixture, cooling and secondly boiling the mixture, and then cooling the mixture at room temperature.
이하, 본 발명의 산양삼경옥고의 제조방법을 보다 상세히 설명한다.Hereinafter, the method for producing the gypsum gypsum gypsum of the present invention will be described in more detail.
상기 1)단계는 산양삼, 인삼 및 백복령에 붙어있는 흙 등의 이물질을 수작업으로 깨끗이 제거한 후, 분말화 하는 단계이다. 상기 분말화는 나노 3D mill에 넣고 분쇄하여 300호 체로 걸러낸 것으로, 액상 추출률을 높이기 위해 입도가 작을수록 좋으므로 구체적인 입도로 한정하지는 않는다.The step 1) is a step of manually removing foreign matters such as goat ginseng, ginseng, and soil attached to Baekbok-gil, and then pulverizing it. The pulverization is carried out in a nano 3D mill, pulverized and filtered through a No. 300 sieve. The smaller the particle size is to increase the liquid extraction rate, it is not limited to the specific particle size.
상기 2) 단계는 생지황을 깨끗히 수세하여 분쇄하고 즙을 낸 후, 삼베로 걸러 생지황 즙을 제조하는 단계이다.In step 2), fresh persimilis is washed, ground, juiced, and then filtered with a mortar to produce jujuba juice.
상기 3) 단계는 꿀을 50-70℃, 바람직하게는 60℃ 에서 15 내지 30분간 물중탕하여 위로 뜨는 흰 거품과 수분을 제거하여 연밀을 제조하는 단계이다.In step 3), the honey is soaked in water at 50-70 ° C, preferably 60 ° C for 15-30 minutes to remove the white foam and moisture that float up to produce a mill.
상기 4) 단계는 상기 체로 거른 산양삼분말, 인삼분말 및 백복령분말을 생지황즙과 연밀에 혼합하는 단계이다.The step 4) is a step of mixing the sieved ginseng powder, ginseng powder, and white ginseng powder, which have been sieved through the sieve, with the fresh persimmon juice and the plant.
상기 5) 단계는 상기 혼합물을 중탕, 냉각 및 중탕하는 단계를 거쳐 경옥고를 제조한다. 구체적으로는, 상기 4) 단계에서 얻은 경옥고 원료를 옹기에 넣고, 옹기의 입구를 밀봉한 후 중탕기에 넣고 물중탕하여 경옥고를 만든다. 중탕은 1차 중탕(3일간(72시간) 92 내지 96℃의 온도, 바람직하게 94℃로 중탕) - 냉각(1일간(24시간, 수돗물 5 내지 20℃에서 냉각) - 2차 중탕(1일간(24시간) 92 내지 96℃의 온도, 바람직하게 94℃로 중탕)으로 이루어질 수 있다.In step 5), the mixture is subjected to a step of warming, cooling, and soaking to prepare a moxa gruel. Specifically, the raw material of the gypsum ga so obtained in the step 4) is put into a pottery pot, the inlet of the pottery pot is sealed, the pottery pot is put in a hot water bath, and water bath is made. (1 day (24 hours, water is cooled at 5 to 20 占 폚) - Secondary bath (1 day (72 hours) (24 hours) at a temperature of 92 to 96 占 폚, preferably at 94 占 폚).
상기 중탕 조건(온도, 시간), 냉각조건(온도, 시간)은 최적의 경옥고를 만들기 위한 것으로, 상기 온도보다 낮으면 경옥고 재료의 유효성분을 추출하기 어렵고 상기 온도보다 높으면 경옥고 재료의 물성이 파괴된다. 그리고, 2차에 걸쳐 중탕하는 이유는 유효성분의 추출을 극대화하고 한방으로는 경옥고의 수기(水氣)를 보충하기 위함이다.If the temperature is lower than the above temperature, it is difficult to extract the effective component of the manganese oxide material. If the temperature is higher than the above temperature, the physical properties of the manganese oxide material are destroyed . In addition, the reason for boiling water for the second time is to maximize the extraction of the active ingredient and to supplement the water of the Kyeongok High School in one direction.
본 발명의 산양삼경옥고의 제조 방법에 기재된 각 수치는 본 발명의 효과를 벗어나지 않는 범위 내에서 당업자가 용이하게 조절할 수 있다.
The respective numerical values described in the method of manufacturing gypsum gypsum gypsum of the present invention can be easily adjusted by those skilled in the art without departing from the effect of the present invention.
또한, 본 발명은 현탁음료 총 중량에 대해 산양삼경옥고 15-35중량%를 포함하는, 산양삼경옥고 현탁음료를 제공한다.In addition, the present invention provides a goat ginseng jellyfish suspension drink comprising 15-35% by weight of ginseng gypsum gypsum based on the total weight of the suspension.
상기 산양삼경옥고 현탁음료는 산양삼경옥고 15-35중량%, 꿀 1-10중량%, 자몽종자추출물 0.01-1.0중량%, 구연산 0.1-1.0중량%, 젤란검 0.1-1.0중량% 및 잔량의 정제수를 혼합한 후, 100 내지 500rpm으로, 30분 내지 60분 동안 교반하고, 부유물이 없도록 실온에서 1 내지 3시간 동안 침전시켜 그 상층액을 여과하여 얻는다.The Sansian ginseng jellyfish suspension beverage is prepared by mixing 15-35 wt.% Of Sansian ginseng mushroom, 1-10 wt.% Of honey, 0.01-1.0 wt.% Of grapefruit seed extract, 0.1-1.0 wt.% Of citric acid, 0.1-1.0 wt.% Of gellan gum, , Stirring is carried out at 100 to 500 rpm for 30 to 60 minutes, and the supernatant is filtered out by precipitation at room temperature for 1 to 3 hours so as to be free from suspended matters.
상기 제조방법에 의해 제조된 산양삼경옥고 현탁음료는 시판되는 경옥고를 이용한 현탁음료보다 입자경이 적어 기호도가 높았으며, 시간에 따른 pH 및 산도의 변화가 없으며, 저장 기간에 따른 균이 검출되지 않았으므로 저장 안정성이 우수하다.
The ginseng saponaceous mushroom suspension prepared by the method described above had a smaller particle size than that of the commercially available moss gypsum-based suspension, and it had no change in pH and acidity with time, Stability is excellent.
이하 본 발명의 이해를 돕기 위하여 바람직한 실시예, 실험예 및 제조예를 제시한다. 그러나 하기의 실시예, 실험예 및 제조예는 본 발명을 보다 쉽게 이해하기 위하여 제공되는 것일 뿐, 실시예, 실험예 및 제조예에 의해 본 발명의 내용이 한정되는 것은 아니다.
Hereinafter, preferred embodiments, experimental examples, and production examples are provided to facilitate understanding of the present invention. However, the following examples, experimental examples and production examples are provided only for the purpose of easier understanding of the present invention, and the present invention is not limited by the examples, experimental examples and production examples.
실시예 1. 산양삼경옥고의 제조Example 1: Preparation of goat ginseng
1-1. 산양삼경옥고의 배합1-1. Blend of goat juice moxibustion
산양삼경옥고는 경옥고의 기본배합에서 하기 표 1에 나타낸 바와 같이 인삼과 산양삼의 비율을 조절한 총 6가지의 배합으로 제조하였다.As shown in Table 1 below, the raw ginseng mushroom gums were prepared from six basic combinations of ginseng and goat ginseng in the basic formulation of Gyeongokgok.
1-2. 산양삼경옥고의 제조 공정의 표준화1-2. Standardization of manufacturing process of Sangyang Jangheokgo
1. 재료 1차 가공 : 약재에 붙어있는 흙 등의 이물질을 수작업으로 깨끗이 제거하였다.1. Materials First processing: Foreign materials such as soil attached to the medicinal materials were cleanly removed by hand.
2. 재료 2차 가공2. Material secondary processing
(1) 산양삼, 인삼, 백복령 : 나노 3D mill을 통해 나노입자로 분쇄하였다. (1) Goat ginseng, ginseng, and Baekbokryeong: Nano-sized granules were milled into nanoparticles.
(2) 생지황 : 압착기를 이용하여 즙으로 짜내었다. (2) Raw Persimmon: It was squeezed with juice using a squeezer.
(3) 꿀 : 60℃에서 20분간 서서히 저으면서 물중탕하여 떠오르는 흰거품과 수분을 제거하여, 연밀을 제조하였다. (3) Honey: White foaming and moisture were floated in the water while stirring at 60 占 폚 for 20 minutes to remove the bubbles and moisture, thereby producing a mill.
3. 재료 3차 가공3. Material third processing
(1) 인삼, 산양삼, 백복령 분말 : 300호 체로 걸러서 덩어리가 큰 입자들을 제거한다. (1) Ginseng, goat ginseng, and Baekbok-ri powder: Filter with 300 mesh sieve to remove large particles.
(2) 생지황 즙 : 삼베로 걸러주었다. (2) jujube juice: I filtered it with hemp.
4. 재료 혼합 : 중탕에 사용할 항아리에 재료를 모두 넣고 나무 주걱을 이용하여 반죽덩어리가 뭉치지 않도록 최대한 고르게 혼합하였다.4. Mixing materials: All the ingredients are put into a jar for use in a bath, and the mixture is evenly mixed with a wooden spatula so that the dough does not clump.
5. 중탕 준비5. Preparing the bath
(1) 항아리 뚜껑 준비(I) : 한지를 이용하여 항아리 뚜껑 크기로 자른 후 기름을 먹인 후 음건하였다. (1) Preparation of jar lid (I): The jar was cut into the size of the jar lid using Korean paper, and then oil was added and shaded.
(2) 항아리 뚜껑 준비(II) : 광목을 항아리 뚜껑 크기로 잘라 준비하였다. (2) Preparation of the jar lid (II): The jar lid was prepared to be cut to the size of the lid.
(3) 항아리를 담고 중탕할 용기와 항아리가 직접 가열되지 않도록 밑에 받칠 굄목을 준비하였다. (3) The jar was put in a jar to support the pot and the jar to be heated.
(4) 혼합한 재료가 들어있는 항아리 입구를 기름먹인 한지로 밀봉하고 그 위에 광목을 덮어 밀봉한 후 새지 않도록 단단히 고정하였다. (4) The entrance of the pot containing the mixed material was sealed with oiled paper, covered with a light cover thereon, and tightly fixed so as not to leak.
(5) 항아리를 중탕용기의 굄목위에 안착시키고 중탕할 용기에 항아리 주둥이에서 5cm정도 아래까지 물을 채워 열이 고르게 전달되도록 하였다. (5) The jar was placed on the bamboo tray and the container to be boiled was filled with water up to 5 cm below the jar spout so that the heat was evenly distributed.
6. 물중탕 6. Water bath
(1) 점화한 후 3일간 계속 85~90℃가 유지되도록 중탕하되 물이 증발되어 물 표면이 항아리 내부의 경옥고 높이보다 아래로 내려가지 않도록 뜨거운 물을 지속적으로 보충하였다. (1) After ignition, hot water was constantly replenished so that the surface of the water did not fall below the height of the jellyfish inside the jar.
(2) 항아리를 들어 올려 꺼내고 중탕용기 안에 있는 뜨거운 물을 모두 버린 후에 항아리를 다시 중탕용기에 넣고 찬물을 5-(5)에 나온 것과 같은 요령으로 15℃가 유지되도록 하여 1일간 담가두었다. (2) Lift the pot and remove all the hot water from the hot water bottle. Then put the pot back into the hot water bottle and immerse the cold water for one day so that the temperature is maintained at 15 ° C as shown in 5- (5).
(3) 중탕용기의 온도가 85-90℃가 되도록 다시 가열하여 6-(1)과 같은 요령으로 1일간 중탕하였다. (3) The cup was heated again to a temperature of 85-90 ° C, and the mixture was soaked in the same manner as in 6- (1) for 1 day.
(4) 항아리를 꺼내고 실온에서 천천히 식혀주어 완성하였다. (4) The jar was taken out and cooled slowly at room temperature.
7. 유의사항7. Notice
(1) 만들어진 경옥고는 쇠로 만든 용기나 기구가 닿지 않도록 주의해야 한다. (1) Care should be taken not to reach the masonry container made of iron or steel.
(2) 보관은 기본적으로 냉장실 보관을 원칙으로 한다.
(2) Storage is basically kept in the refrigerator room.
실시예 2. 산양삼경옥고 시료에 대한 기기 분석Example 2: Instrumental analysis for Samples of Gohyanggyo samples
2-1. 산양삼경옥고의 UPLC 패턴 확인2-1. Confirm UPLC pattern of goat jelly
산양삼의 지표성분으로는 진세노사이드(ginsenoside) Rb1, Rg1, Rg3를 설정하였으며, 한국 식품의약품안전청 (KFDA)에서 제공받은 표준품을 사용하였다.Ginsenosides Rb1, Rg1, and Rg3 were set as the indicator components of goat ginseng, and the standard products provided by Korea Food and Drug Administration (KFDA) were used.
표준품 분석 결과는 도 1에 나타내었다.
The results of the standard product analysis are shown in Fig.
2-2. UPLC 조건2-2. UPLC condition
산양삼의 지표 성분의 분석은 UPLC를 이용하여 크로마토그램(chromatogram)으로 나타내었다.Analysis of surface components of goat's ginseng was expressed by chromatogram using UPLC.
UPLC 분석 조건은 표 2에 나타내었다. The UPLC analysis conditions are shown in Table 2.
2-3. UPLC 결과의 분석2-3. Analysis of UPLC results
크로마토그램을 통해 생리활성 성분인 Ginsenoside Rb1 및 Rg1, Rg3가 산양삼경옥고에서 검출되어 지표성분이 존재하고 있음을 확인하였다.The physiologically active components, Ginsenoside Rb1 and Rg1 and Rg3, were detected in the ginseng ginseng at Kyeongokgyo.
UPLC 분석결과는 도 2에 나타내었다.
The results of the UPLC analysis are shown in Fig.
2-4. pH 측정2-4. pH measurement
식품공전에 수록된 일반시험법에 따라 산양삼경옥고 1g을 정확하게 달고 증류수로 10mL로 희석하였다. 그 후, 디지털 pH meter(Orion 410A, Thermo scientific, USA)로 측정하였다.
According to the general test method listed in the Food Code, 1 g of goat ginseng mushroom was precisely weighed and diluted with distilled water to 10 mL. Thereafter, it was measured with a digital pH meter (Orion 410A, Thermo scientific, USA).
2-5. 당도 측정2-5. Sugar content measurement
산양삼경옥고 시료 1g을 증류수로 10배 희석하고 디지털 당도계(PR-100, ATAGO, Japan)로 측정하여˚Brix 값으로 나타내었다.
1 g of Saururus japonica sample was diluted 10 times with distilled water and measured with a digital sugar meter (PR-100, ATAGO, Japan), and expressed as a ˚Brix value.
2-6. 색도 측정2-6. Chromaticity measurement
색도는 색차계(Chroma meter CR-300, Minolta, Japan)을 이용하여 L(명도), a(적색도), b(황색도) 값을 3회 반복 측정하고 그 평균치를 구하였다.L (lightness), a (redness) and b (yellowness) values were repeatedly measured three times using a colorimeter (Chroma meter CR-300, Minolta, Japan).
2-7. 침강용적2-7. Sedimentation volume
원래 용적 V0 와 침강물의 최종 용적 Vu 를 측정하여 Vu / V0 의 비로 나타내었다.
The original volume V 0 and the final volume V u of the sediment were measured and expressed as the ratio of V u / V 0 .
2-8. 입자경2-8. Drop size
입자분석기(S3500, Micortrac, USA) 으로 측정하여 전체 입자 직경의 평균값을 나타내었다.
(S3500, Micortrac, USA), and the average value of the total particle diameters was shown.
본 발명의 산양삼경옥고의 pH, 당도 및 색도를 표 3에 나타내었다.Table 3 shows the pH, the sugar content and the chromaticity of the gypsum gypsum of the present invention.
(˚Brix)Sugar content
(˚Brix)
표 3에 나타난 바와 같이, 산양삼경옥고는 pH 4-5, 당도 7-10˚Brix, L(명도)값은 19-22, a(적색도)값은 0.4-0.0.8, b(황색도)값은 0.5-0.8 임을 확인하였다.
As shown in Table 3, the raw ginseng jellyfish has a pH of 4-5, a sugar content of 7-10 ° Brix, an L value of 19-22, a (redness) value of 0.4-0.0.8, b (yellowness) Value was found to be 0.5-0.8.
실시예 3. 산양삼경옥고의 기호도 조사Example 3. Examination of preference of the goat ginseng kyokoko
상기 실시예 1에서의 배합비만 바꾸어 전통적인 제조방법을 이용하여 제조된 6종류의 산양삼경옥고를 원광대학교 원광한약연구소에 재직하는 직원 중 20~30대 10명(남:5명, 여:5명)의 평가 요원을 무작위로 선발하여 관능평가를 실시하였다.Six (10 male, 5 male, 5 female) among the employees of the Wonkwang University Wonkwang Chinese Medicine Research Institute who made six kinds of Sangyang ginseng kyokoko using the traditional manufacturing method, Were randomly selected and evaluated for sensory evaluation.
제조된 산양삼경옥고의 관능평가는 5점 측정법 (1점:매우 나쁘다, 2점:조금 나쁘다, 3점:보통이다, 4점:조금 좋다, 5점:매우 좋다)으로 맛과 향에 대해 평가하였다. 그 결과를 표4에 나타내었다.
The taste and flavor of the prepared ginseng jellyfish was evaluated by 5 point method (1 point: very bad, 2 points: slightly worse, 3 points: normal, 4 points: slightly good, 5 points: very good) . The results are shown in Table 4.
표 4에 나타난 바와 같이, 전체적인 기호도를 볼 때 인삼 대신 산양삼을 넣어 만든 경옥고 6번에 대한 평가가 가장 좋았으며, 다른 경옥고에 비해 상대적으로 맛이 좋고 뒷맛이 깔끔한 것으로 나타났다. 결과적으로 인삼 대신 산양삼을 넣어 제조한 경옥고가 제품화하기에 가장 적합할 것으로 판단된다.
As shown in Table 4, the most favorable evaluation of Gyeongokgyo No. 6 made with ginseng ginseng instead of ginseng showed better taste and better aftertaste than those of other gyeongokgyo. As a result, gyeongokgyo, which is prepared by putting goose ginseng instead of ginseng, is considered to be most suitable for commercialization.
실시예 4. 기호도 평가에 의한 산양삼경옥고 함유 현탁음료 배합비 확정Example 4. Determination of Mixed Ratio of Suspended Bean Containing Goya-gyu Jyokokgol by Evaluation of Preference Rating
상기 실시예 3의 결과를 바탕으로, 산양삼경옥고 6을 주재료로 하여 구연산, 감미료, 현탁화제의 최적 배합비를 얻기 위해 기호도를 평가하였다. 기호도 평가의 패널은 원광한약연구소의 숙련된 관능평가요원 10명(남:5명, 여:5명)을 대상으로 하였다.
Based on the results of Example 3, the preference degree of citric acid, sweetener, and suspending agent was evaluated to obtain an optimal blend ratio of Sanshin Gyepo 6 as a main ingredient. The panel of the preference evaluation was conducted by 10 skilled workers in the Wonkwang Institute of Chinese Medicine (male: 5, female: 5).
4-1. 1차 기호도 평가4-1. Evaluation of primary preference
1차 기호도 평가에서는 하기 표 5와 같이, 산양삼경옥고 6의 양을 10, 20, 30, 40중량%로 다르게 첨가하고, 잔량의 정제수를 혼합한 4가지 시료를 준비하였다.
In the evaluation of the primary preference, four samples were prepared by adding 10%, 20%, 30%, and 40% by weight of Sangyang Jangheokgyo 6 in different amounts as shown in Table 5 below and mixing the remaining amount of purified water.
정제수
Purified water
90
90
80
80
70
70
60
60
실험 전날 제조하여 3시간 침전시킨 후 여과하여 4℃ 냉장고에 보관하여, 평가 직전에 일회용 종이컵에 약 50mL씩 담아 무작위로 제시하였다. 시료와 시료 사이에 입을 헹굴 수 있도록 정수된 물을 함께 제공하여 시료를 평가하기 전에 시료의 특성에 따른 전 시료와의 혼란과 감각의 둔화를 줄이기 위해 2~3회 정도 충분히 입안을 헹군 후 평가하도록 하였다.They were prepared on the day before the experiment, precipitated for 3 hours, filtered and stored in a refrigerator at 4 ° C. Randomly presented with a volume of about 50 mL in a disposable paper cup immediately before evaluation. Rinse the mouth thoroughly 2-3 times before the sample is evaluated by providing purified water to rinse the mouth between the sample and the sample to reduce the confusion with the sample and the slowing of the sensation according to the characteristics of the sample. Respectively.
평가는 소비자 패널과 1:1 면접방식으로 진행하여 타인의 의견에 영향을 받지 않도록 하였으며, 전반적인 기호도를 5점 척도법을 사용하여 1점은‘매우 좋지 않다’, 5점은 ‘매우 좋다’로 평가하였다. 그 결과를 표 6에 나타내었다.
The evaluation was conducted in a one-to-one interview with the consumer panel to avoid being influenced by other people's opinions. The overall likelihood was evaluated using the 5-point scale method, with 1 point being "not very good" and 5 points being "very good" Respectively. The results are shown in Table 6.
표 6에 나타난 바와 같이, 본 발명의 산양삼경옥고의 함량이 20중량% 일 때, 가장 좋은 기호도 경향을 보였다.
As shown in Table 6, when the content of the gypsum mushroom of the present invention was 20% by weight, the best preference tendency was shown.
4-2. 2차 기호도 평가 4-2. Secondary preference evaluation
2차 기호도 평가에서는 표 7에서와 같이, 산양삼경옥고(10˚Brix)를 20중량%로 고정하고, 꿀의 양만을 0, 1.3, 2.6, 3.9, 5.2, 6.5중량%로 달리하여 첨가한 6가지 시료를 준비하였다.
In the evaluation of the secondary preference, as shown in Table 7, six kinds of six kinds of honeycombs were prepared, in which the amount of honey was fixed at 0, 1.3, 2.6, 3.9, 5.2, and 6.5 wt% Samples were prepared.
상기 실시예 4-1에 나타낸 1차 기호도 평가와 마찬가지로, 실험 전날 제조하여 4℃ 냉장고에 보관하여, 평가 직전에 일회용 종이컵에 50mL씩 담아 무작위로 제시하였다. 시료와 시료 사이에 입을 헹굴 수 있도록 정수된 물을 함께 제공하여 시료를 평가하기 전에 시료의 특성에 따른 전 시료와의 혼란과 감각의 둔화를 줄이기 위해 2~3회정도 충분히 입안을 헹군 후 평가하도록 하였다.Similar to the first preference evaluation shown in Example 4-1, the sample was prepared on the day before the experiment and stored in a refrigerator at 4 DEG C, and 50 mL of the disposable paper cup was randomly presented immediately before the evaluation. Rinse the mouth thoroughly 2-3 times before the sample is evaluated by providing purified water to rinse the mouth between the sample and the sample to reduce the confusion with the sample and the slowing of the sensation according to the characteristics of the sample. Respectively.
평가는 소비자 패널과 1:1 면접방식으로 진행하여 타인의 의견에 영향을 받지 않도록 하였으며, 전반적인 기호도를 5점 척도법을 사용하여 1점은‘매우 좋지 않다’, 5점은 ‘매우 좋다’로 평가하였다. 그 결과를 도 8에 나타내었다.
The evaluation was conducted in a one-to-one interview with the consumer panel to avoid being influenced by other people's opinions. The overall likelihood was evaluated using the 5-point scale method, with 1 point being "not very good" and 5 points being "very good" Respectively. The results are shown in Fig.
표 8에 나타난 바와 같이, 산양삼경옥고(10˚Brix)를 20중량%로 고정하고, 꿀의 양이 5.2중량%일 때, 가장 좋은 기호도를 보였다.
As shown in Table 8, when the amount of honey was 5.2 wt%, the best preference was shown when the ginseng root (10 ˚ Brix) was fixed at 20 wt%.
4-3. 3차 기호도 평가4-3. Evaluate third degree preference
3차 기호도 평가에서는 표 9에와 같이, 산양삼경옥고(10˚Brix) 20중량%, 꿀 5.2중량%로 고정하고, 구연산 함량을 0, 0.1, 0.2, 0.3, 0.4, 0.5 로 달리하여 첨가한 6가지 시료를 준비하였다.
In the evaluation of the third preference, as shown in Table 9, 20% by weight of 10 ˚ Brix and 22% by weight of honey were fixed, and the citric acid content was changed to 0, 0.1, 0.2, 0.3, 0.4, A branch sample was prepared.
실험 전날 제조하여 4℃ 냉장고에 넣어두었다가 평가 직전에 일회용 종이컵에 50mL씩 담아 무작위로 제시하였다. 시료와 시료 사이에 입을 헹굴 수 있도록 정수된 물을 함께 제공하여 시료를 평가하기 전에 시료의 특성에 따른 전 시료와의 혼란과 감각의 둔화를 줄이기 위해 2~3회정도 충분히 입안을 헹군 후 평가하도록 하였다.It was prepared on the day before the experiment, placed in a refrigerator at 4 ° C and randomly presented with 50 ml of disposable paper cup just before the evaluation. Rinse the mouth thoroughly 2-3 times before the sample is evaluated by providing purified water to rinse the mouth between the sample and the sample to reduce the confusion with the sample and the slowing of the sensation according to the characteristics of the sample. Respectively.
평가는 소비자 패널과 1:1 면접방식으로 진행하여 타인의 의견에 영향을 받지 않도록 하였으며, 전반적인 기호도를 5점 척도법을 사용하여 1점은 ‘매우 좋지 않다’, 5점은 ‘매우 좋다’로 평가하였다. 그 결과를 표 10에 나타내었다.
The evaluation was conducted in a one-to-one interview with the consumer panel to avoid being influenced by other people's opinions. The overall likelihood was evaluated using the 5-point scale method, with 1 point being "not very good" and 5 points being "very good" Respectively. The results are shown in Table 10.
(중량%)Citric acid content
(weight%)
표 10에 나타난 바와 같이, 산양삼경옥고(10˚Brix) 20중량%, 꿀 5.2중량%, 구연산 0.2중량%일 때, 가장 높은 기호도를 보였다.
As shown in Table 10, the highest preference was shown when 20% by weight of ginseng root (10 占 rix), 5.2% by weight of honey, and 0.2% by weight of citric acid.
4-4. 4차 기호도 평가4-4. 4th likelihood evaluation
4차 기호도 평가에서는 표 11에서와 같이, 산양삼경옥고(10˚Brix) 20중량%, 꿀 5.2중량%, 구연산 0.2중량%로 고정하고, 젤란검의 함량을 0, 0.1, 0.2, 0.3, 0.4, 0.5로 달리하여 첨가한 6가지 시료를 준비하였다.
In the fourth rank preference evaluation, as shown in Table 11, the content of gellan gum was fixed at 20% by weight, 10% by weight, 10% by weight of honey, 5.2% by weight of honey and 0.2% by weight of citric acid, 0.5 were prepared. Six samples were prepared.
실험 전날 제조하여 4℃ 냉장고에 보관하여, 평가 직전에 일회용 종이컵에 50mL씩 담아 무작위로 제시하였다. 시료와 시료 사이에 입을 헹굴 수 있도록 정수된 물을 함께 제공하여 시료를 평가하기 전에 시료의 특성에 따른 전 시료와의 혼란과 감각의 둔화를 줄이기 위해 2~3회 정도 충분히 입안을 헹군 후 평가하도록 하였다.They were prepared on the day before the experiment and stored in a refrigerator at 4 ° C. Randomly presented with 50 mL of disposable paper cup just before evaluation. Rinse the mouth thoroughly 2-3 times before the sample is evaluated by providing purified water to rinse the mouth between the sample and the sample to reduce the confusion with the sample and the slowing of the sensation according to the characteristics of the sample. Respectively.
평가는 소비자 패널과 1:1 면접방식으로 진행하여 타인의 의견에 영향을 받지 않도록 하였으며, 전반적인 기호도를 5점 척도법을 사용하여 1점은 ‘매우 좋지 않다’, 5점은 ‘매우 좋다’로 평가하였다. 그 결과를 표 12에 나타내었다.
The evaluation was conducted in a one-to-one interview with the consumer panel to avoid being influenced by other people's opinions. The overall likelihood was evaluated using the 5-point scale method, with 1 point being "not very good" and 5 points being "very good" Respectively. The results are shown in Table 12.
(중량%)Content of gellan gum
(weight%)
표 12이 나타난 바와 같이, 산양삼경옥고(10˚Brix) 20중량%, 꿀 5.2중량%, 산 0.2중량%, 젤란검 0.2중량%일 때, 가장 높은 기호도를 보였다. 또한, 젤란검이 0.2중량%로 첨가될 때,침강용적이 가장 높은 것을 확인하였다.As shown in Table 12, the highest preference was shown when 20% by weight of ginseng root (10 占 rix), 5.2% by weight of honey, 0.2% by weight of acid and 0.2% by weight of gellan gum. Furthermore, when gellan gum was added at 0.2 wt%, it was confirmed that the sedimentation volume was the highest.
상기 결과에서 침강용적은 원래의 용적 V0와 침강물의 최종용적 Vu을 측정하여 Vu/V0의 비로 나타내었으며, 침강용적이 1일 때 이상적인 현탁 음료이다.
In the above results, the sedimentation volume is expressed as the ratio of V u / V 0 by measuring the original volume V 0 and the final volume V u of the sediment, and is an ideal suspension drink when the sedimentation volume is 1.
실시예 5. 최종 기호도 평가Example 5. Final Preference Evaluation
상기 실시예4의 기호도 평가에 의한 산양삼경옥고 함유 현탁음료 배합비를 바탕으로 최종 기호도 평가를 실시하였다.The final preference degree evaluation was carried out based on the blending ratio of the suspension-containing beverage containing ginseng saponaceae by the preference evaluation of Example 4 above.
본 발명의 산양삼경옥고 및 시중에 판매되는 경옥고(00사 00제품)를 이용하여 각각 현탁음료를 제조한 후, 비교 평가하였다. 최종 기호도 평가에 사용된 현탁음료의 제조방법은 표 13과 같다.
The suspension drink of the present invention was prepared using the goat ginseng mushroom and the commercially available mushroom (product of 000000). Table 13 shows the manufacturing method of the suspended beverage used for the final acceptability evaluation.
실험 전날 제조하여 4℃ 냉장고에 보관하여, 평가 직전에 일회용 종이컵에 50mL씩 담아 무작위로 제시하였다. 시료와 시료 사이에 입을 헹굴 수 있도록 정수된 물을 함께 제공하여 시료를 평가하기 전에 시료의 특성에 따른 전 시료와의 혼란과 감각의 둔화를 줄이기 위해 2~3회 정도 충분히 입안을 헹군 후 평가하도록 하였다.They were prepared on the day before the experiment and stored in a refrigerator at 4 ° C. Randomly presented with 50 mL of disposable paper cup just before evaluation. Rinse the mouth thoroughly 2-3 times before the sample is evaluated by providing purified water to rinse the mouth between the sample and the sample to reduce the confusion with the sample and the slowing of the sensation according to the characteristics of the sample. Respectively.
평가는 소비자 패널과 1:1 면접방식으로 진행하여 타인의 의견에 영향을 받지 않도록 하였으며, 전반적인 기호도를 5점 척도법을 사용하여 1점은 ‘매우 좋지 않다’, 5점은 ‘매우 좋다’로 평가하였다. 그 결과를 도 3에 나타내었다.The evaluation was conducted in a one-to-one interview with the consumer panel so that it was not affected by the opinions of others. Overall score was rated as "not very good" and 5 points "very good" Respectively. The results are shown in Fig.
또한, 산양삼경옥고 현탁음료와 시제품 현탁음료의 이화학적 특성 비교 결과를 표 14에 나타내었으며, 입자경과 침강용적 비교 결과를 표 15에 나타내었다.
Table 14 shows the results of comparison between physicochemical properties of Sangyang Jangheokgo suspended beverage and prototype beverage suspension, and Table 15 shows the comparison of sedimentation volume and sedimentation volume.
(˚Brix)Sugar content
(˚Brix)
표 14에 나타난 바와 같이, 산양삼경옥고 현탁음료 및 시제품 현탁음료의 비교 시, 두 제품의 당도는 동일하나, pH, 산도 및 색도는 산양삼경옥고 현탁음료가 더 높음을 확인하였다.As shown in Table 14, the sugar content of the two products was the same, but pH, acidity and chromaticity were higher than that of the goat ginseng jellyfish suspension drink.
또한, 표 15에 나타난 바와 같이, 산양삼경옥고 현탁음료 및 시제품 현탁음료의 입자경과 침강용적 비교 시, 산양삼경옥고 현탁음료의 입자경이 시제품 현탁음료 보다 더 작고, 침강용적 또한 산양삼경옥고 현탁음료의 수치가 더 높아, 종합적 기호도가 산양삼경옥고 현탁음료가 더 높음을 확인할 수 있었다.
In addition, as shown in Table 15, when the particle sedimentation volume of the goat ginseng moxibustion suspension drink and prototype suspension drink were compared, the particle size of the goat ginseng moxibustion suspension was smaller than that of the prototype suspension, and the sedimentation volume was also higher And it was confirmed that the preference degree of Sangyang Gyeongokgyo suspension drink was higher than that of Sangyang gyeongokgyo suspension drink.
실시예 6. 산양삼경옥고 현탁음료 제조 공정의 확립Example 6. Establishment of the manufacturing process of Suyang ginseng kyokoko suspension beverage
산양삼경옥고 음료 조성물의 혼합, 살균 및 충진 공정을 확립하고자 하였다.The purpose of this study was to establish the mixing, sterilization and filling process of Sangyang ginseng cheongokgok beverage composition.
6-1. 혼합 조건의 확립6-1. Establishment of mixing conditions
본 발명에 따른 음료 조성물의 혼합에 있어서, 상기 실시예 5의 최종 기호도 평가 결과 기호도가 가장 우수한 것으로 평가된 배합비에 따라 산양삼경옥고(10˚Brix) 20중량%, 꿀 5.2중량%, 자몽종자추출물 0.1중량%, 구연산 0.2중량%, 젤란검 0.2중량% 및 잔량의 정제수를 포함하는 음료 조성물을 제조하였다.
In the mixing of the beverage composition according to the present invention, 20% by weight of Sangyang Jangheokgyo (10 ˚ Brix), 5.2% by weight of honey, 0.1% of grapefruit seed extract 0.2% by weight of citric acid, 0.2% by weight of gellan gum and a balance of purified water.
6-2. 충진 조건의 확립6-2. Establishment of filling conditions
실시예 5에서 혼합한 음료 조성물을 병입하였다. 이때 60℃ 이상의 핫필링을 하였다.
The beverage composition mixed in Example 5 was bottled. At this time, hot peeling was performed at 60 ° C or more.
6-3. 살균 조건의 확립6-3. Establishment of sterilization conditions
실시예 5에서 충진한 음료 조성물을 80℃의 온도에서 30분간 살균하였다.
The beverage composition filled in Example 5 was sterilized at a temperature of 80 DEG C for 30 minutes.
실험예 1. 산양삼경옥고 현탁음료 조성물의 품질 변화 측정Experimental Example 1. Measurement of change in quality of the composition
1-1. 당도 측정1-1. Sugar content measurement
상기 실시예 6에 따라 제조된 음료의 당도를 디지털 당도계 (PR-100, ATAGO, Japan)로 측정하여 ˚Brix 값으로 나타내었다. 단, 샘플링한 시료는 가속실험을 진행한 온도를 유지한 상태에서 측정하였다. 당도 측정 결과는 도 4에 나타내었다.The sugar content of the beverage prepared according to Example 6 was measured with a digital sugar meter (PR-100, ATAGO, Japan) and expressed as a ˚Brix value. However, the sampled samples were measured while maintaining the temperature at which the acceleration test was performed. The results of the sugar content measurement are shown in Fig.
도 4에 나타난 바와 같이, 당도는 저장기간이나 온도에 크게 차이가 생기지 않음을 확인하였다.
As shown in FIG. 4, it was confirmed that the sugar content did not significantly differ between the storage period and the temperature.
1-2. pH 측정1-2. pH measurement
상기 실시예 6에 따라 제조된 음료의 pH를 디지털 pH meter(Orion 410A, Thermo scientific, USA)로 측정하였다. pH 측정 결과는 도 5에 나타내었다. The pH of the beverage prepared according to Example 6 was measured with a digital pH meter (Orion 410A, Thermo scientific, USA). The results of pH measurement are shown in Fig.
도 5에 나타난 바와 같이, pH는 시간의 경과에 따라 약간 감소하였으나, pH 3.7 전후로 크게 변화가 없음을 확인하였다.
As shown in FIG. 5, the pH slightly decreased with the lapse of time, but it was confirmed that the pH did not change significantly around 3.7.
1-3. 산도 측정1-3. Acidity measurement
상기 실시예 6에 따라 제조된 음료의 산도를 식품공전의 방법에 따라 0.1 N NaOH로 적정하여 구연산(%)으로 나타내었다. 산도 측정 결과는 도 6에 나타내었다. The acidity of the beverage prepared according to Example 6 was titrated with 0.1 N NaOH according to the method of food revolution and expressed as citric acid (%). The results of the acidity measurement are shown in Fig.
도 6에 나타난 바와 같이, 산도는 저장기간이나 온도에 크게 차이가 생기지 않았다.
As shown in FIG. 6, the acidity did not significantly differ between the storage period and the temperature.
1-4. 총 균수 측정1-4. Total number of bacteria
상기 실시예 6에 따라 제조된 음료의 일반세균과 대장균군의 측정을 위해 따로 샘플링한 것을 무균적으로 채취하여 측정하였다. 일반세균은 식품공전 제Ⅱ권 제10. 일반시험법 3. 미생물시험법 3.5 세균수 시험법을, 대장균군은 식품공전 제Ⅱ권 제10. 일반시험법 3. 미생물시험법 3.7 대장균군 시험법에 따라 시료는 각 온도당 3개씩 3회 반복하여 측정하였다. 저장기간별 일반세균 및 대장균군 측정 결과는 표 16 및 표 17에 나타내었다.
For the measurement of general bacteria and coliform bacteria in the beverage prepared according to Example 6, the samples separately sampled were aseptically collected and measured. General microorganisms are found in Foodstuffs Vol.
표 16 및 표 17에 나타난 바와 같이, 20℃와 30℃, 40℃ 모두에서 일반세균(표 16)과 대장균(표 17)이 검출되지 않았데, 이는 살균의 방법이 적절함과 동시에 장시간 유통에도 안정적인 제품을 제공할 수 있는 지표가 됨을 알 수 있었다.
As shown in Table 16 and Table 17, no general bacteria (Table 16) and E. coli (Table 17) were detected at 20 ° C, 30 ° C and 40 ° C, And it is an index that can provide stable products.
Claims (8)
2) 생지황을 분쇄하고 즙을 내고, 걸러주어 생지황즙을 얻는 단계;
3) 꿀을 50-70℃ 에서 15 내지 30분간 물중탕하여 흰 거품과 수분을 제거하고 연밀을 제조하는 단계;
4) 상기 산양삼 분말, 인삼 분말 및 백복령 분말을 생지황즙 및 연밀을 혼합하는 단계; 및
5) 상기 혼합물을 1차 중탕, 냉각 및 2차 중탕한 후, 실온에서 냉각시켜 산양삼경옥고를 제조하는 단계를 포함하는 것을 특징으로 하는, 산양삼경옥고의 제조방법.1) powdering the goat ginseng, ginseng, and bokbok;
2) pulverizing raw persimmon, juicing and filtering to obtain raw persimmon juice;
3) water-bathing the honey at 50-70 ° C for 15-30 minutes to remove white foam and moisture and make a mill;
4) mixing the raw ginseng powder, ginseng powder and white ginseng powder with fresh persimmon juice and vinegar; And
5) A method for producing gypsum gypsum gypsum comprising the step of firstly boiling the mixture, cooling and secondly boiling the mixture, and then cooling the mixture at room temperature.
The present invention relates to a method for preparing a suspension, which comprises 15-35% by weight of goat juice jellyfish, 1-10% by weight of honey, 0.01-1.0% by weight of grapefruit seed extract, 0.1-1.0% by weight of citric acid, 0.1-1.0% Wherein the ginseng saponin is selected from the group consisting of:
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KR101844591B1 (en) | 2016-08-02 | 2018-04-02 | 류태경 | Kyungokgo and manufacturing method of the same |
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KR101601105B1 (en) | 2014-07-01 | 2016-03-08 | 현대자동차 주식회사 | Oil pressure supply system of automatic transmission |
KR101725187B1 (en) * | 2015-04-07 | 2017-04-10 | 대전대학교 산학협력단 | Method for preparing of Gyoungokgo and Gyoungokgo prepared therefrom |
KR20180065468A (en) * | 2016-12-08 | 2018-06-18 | 해천바이오 주식회사 | Preparation method of beverage composition using natural herb extract and beverage composition thereby |
KR102229756B1 (en) * | 2019-06-10 | 2021-03-19 | 농업회사법인미리내산림주식회사 | health supplement food with medicinal herbs |
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KR101844591B1 (en) | 2016-08-02 | 2018-04-02 | 류태경 | Kyungokgo and manufacturing method of the same |
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