KR101476468B1 - 시스 및／또는 트랜스―오르토―시클로헥산디아민-개시된 폴리올 및 그로부터 제조된 경질 폴리우레탄 발포체 - Google Patents

시스 및／또는 트랜스―오르토―시클로헥산디아민-개시된 폴리올 및 그로부터 제조된 경질 폴리우레탄 발포체 Download PDF

Info

Publication number
KR101476468B1
KR101476468B1 KR1020097017952A KR20097017952A KR101476468B1 KR 101476468 B1 KR101476468 B1 KR 101476468B1 KR 1020097017952 A KR1020097017952 A KR 1020097017952A KR 20097017952 A KR20097017952 A KR 20097017952A KR 101476468 B1 KR101476468 B1 KR 101476468B1
Authority
KR
South Korea
Prior art keywords
delete delete
foam
polyol
mixture
polyols
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
KR1020097017952A
Other languages
English (en)
Korean (ko)
Other versions
KR20090112736A (ko
Inventor
티모시 에이. 모레이
프랑수아 엠. 카사티
아드리안 제이. 버취
데이비드 에이. 밥
찰스 에이. 마틴
Original Assignee
다우 글로벌 테크놀로지스 엘엘씨
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 다우 글로벌 테크놀로지스 엘엘씨 filed Critical 다우 글로벌 테크놀로지스 엘엘씨
Publication of KR20090112736A publication Critical patent/KR20090112736A/ko
Application granted granted Critical
Publication of KR101476468B1 publication Critical patent/KR101476468B1/ko
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/50—Polyethers having heteroatoms other than oxygen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4804—Two or more polyethers of different physical or chemical nature
    • C08G18/482—Mixtures of polyethers containing at least one polyether containing nitrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/18—Catalysts containing secondary or tertiary amines or salts thereof
    • C08G18/20—Heterocyclic amines; Salts thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/50—Polyethers having heteroatoms other than oxygen
    • C08G18/5021—Polyethers having heteroatoms other than oxygen having nitrogen
    • C08G18/5024—Polyethers having heteroatoms other than oxygen having nitrogen containing primary and/or secondary amino groups
    • C08G18/5027—Polyethers having heteroatoms other than oxygen having nitrogen containing primary and/or secondary amino groups directly linked to carbocyclic groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2618—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing nitrogen
    • C08G65/2621—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing nitrogen containing amine groups
    • C08G65/2624—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing nitrogen containing amine groups containing aliphatic amine groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/22—After-treatment of expandable particles; Forming foamed products
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0025—Foam properties rigid
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0041—Foam properties having specified density
    • C08G2110/005—< 50kg/m3

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020097017952A 2007-01-30 2008-01-30 시스 및／또는 트랜스―오르토―시클로헥산디아민-개시된 폴리올 및 그로부터 제조된 경질 폴리우레탄 발포체 Active KR101476468B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US89833407P 2007-01-30 2007-01-30
US60/898,334 2007-01-30
PCT/US2008/052396 WO2008094963A1 (en) 2007-01-30 2008-01-30 Cis and/or trans-ortho-cyclohexanediamine-initiated polyols and rigid polyurethane foam made therefrom

Publications (2)

Publication Number Publication Date
KR20090112736A KR20090112736A (ko) 2009-10-28
KR101476468B1 true KR101476468B1 (ko) 2014-12-24

Family

ID=39415228

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020097017952A Active KR101476468B1 (ko) 2007-01-30 2008-01-30 시스 및／또는 트랜스―오르토―시클로헥산디아민-개시된 폴리올 및 그로부터 제조된 경질 폴리우레탄 발포체

Country Status (10)

Country Link
US (1) US8318826B2 (enExample)
EP (1) EP2115027B1 (enExample)
JP (1) JP5366829B2 (enExample)
KR (1) KR101476468B1 (enExample)
CN (1) CN101641386A (enExample)
ES (1) ES2699625T3 (enExample)
MX (1) MX2009008156A (enExample)
RU (1) RU2467025C2 (enExample)
TR (1) TR201821164T4 (enExample)
WO (2) WO2008094238A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20240082749A (ko) 2022-12-02 2024-06-11 주식회사 엘지에너지솔루션 표면 처리된 분리막을 포함하는 전극 조립체, 이를 포함하는 이차전지 및 전극 조립체의 제조방법

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8193257B2 (en) 2007-01-30 2012-06-05 Dow Global Technologies Llc Amine-initiated polyols and rigid polyurethane foam made therefrom
WO2010009189A1 (en) * 2008-07-16 2010-01-21 Dow Global Technologies Inc. Hydrogenation of aromatic polyols
KR20110053975A (ko) * 2008-07-30 2011-05-24 다우 글로벌 테크놀로지스 엘엘씨 경질 폴리우레탄 발포체를 위한 오르토-시클로헥산디아민-개시된 폴리올을 함유하는 폴리올 블렌드
KR20110051205A (ko) * 2008-07-30 2011-05-17 다우 글로벌 테크놀로지스 엘엘씨 오르토-시클로헥산디아민-개시된 폴리올을 기재로 한 경질 폴리우레탄 발포체 시스템
ITMI20081867A1 (it) * 2008-10-22 2010-04-22 Dow Global Technologies Inc Processo per lapreparazione di schiume poliuretaniche rigide a celle chiuse
US20110201707A1 (en) 2008-11-10 2011-08-18 Dow Global Technologies Llc Isocyanate trimerisation catalyst system, a precursor formulation, a process for trimerising isocyanates, rigid polyisocyanurate/polyurethane foams made therefrom, and a process for making such foams
US20120004334A1 (en) * 2009-03-24 2012-01-05 Dow Global Technologies Llc Production of rigid polyurethane foams and the use thereof
BR112012005374A2 (pt) * 2009-09-09 2016-03-29 Arkema Inc processos de melhoramento de espuma de poliuretano e propriedades da espuma utilizando agentes de insuflação de olefinas halogenadas
DE102009042971A1 (de) * 2009-09-24 2011-09-15 Clariant International Ltd. Alkoxylierte cyclische Diamine und deren Verwendung als Emulsionsspalter
ES2447292T3 (es) * 2009-09-29 2014-03-11 Dow Global Technologies Llc Mezclas de polioles que contienen un poliol iniciado por 1,3 - y/o 1,4 - bis(aminometil) ciclohexano y al menos uno de un poliol iniciado por metilen - bis - (ciclohexilamina) y un poliol iniciado por ciclohexanodiamina, y poliuretanos preparados a partir de las mismas
EP2386585B1 (en) 2010-04-21 2017-03-22 Dow Global Technologies LLC Foam insulation unit
US8673998B2 (en) 2010-09-22 2014-03-18 Bridgestone Corporation Polymer compositions with improved cold flow
CN103119142B (zh) 2010-09-24 2015-12-02 陶氏环球技术有限责任公司 用于润滑剂的非芳族系抗氧化剂
JP6258037B2 (ja) * 2011-01-06 2018-01-10 ブルーム エナジー コーポレーション Ｓｏｆｃホットボックスの構成要素
RU2579576C2 (ru) * 2013-12-26 2016-04-10 Лариса Владимировна Лучкина Композиции для получения жестких пенополиуретанов теплоизоляционного назначения
JP6287290B2 (ja) * 2014-02-07 2018-03-07 東レ・ファインケミカル株式会社 ｔｒａｎｓ−１，２−ジアミノシクロヘキサンの製造方法
CN104262603A (zh) * 2014-10-10 2015-01-07 天津工业大学 一种以聚醚胺为起始剂的聚醚破乳剂及其制备方法
WO2017058318A1 (en) 2015-09-29 2017-04-06 Dow Global Technologies Llc Toluene diisocyanate biuret based prepolymers for polyurethane foams
TWI793073B (zh) 2016-05-10 2023-02-21 美商陶氏全球科技有限責任公司 包括胺引發的多元醇的雙組分無溶劑黏著劑組合物
WO2021105330A1 (en) * 2019-11-29 2021-06-03 Basf Se Compositions and polymers useful for such compositions

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5114988A (en) * 1989-10-23 1992-05-19 Basf Corporation Polyether polyols having reduced unsaturation and polyurethane foams prepared therefrom
US5461084A (en) * 1994-09-26 1995-10-24 Bayer Corporation Rigid foams with improved insulation and physical properties
KR20050020780A (ko) * 2002-04-17 2005-03-04 바이엘 머티리얼싸이언스 엘엘씨 히드로플루오로카본 및 이산화탄소로 발포된 폴리우레탄또는 폴리이소시아누레이트 폼

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4595743A (en) * 1985-01-22 1986-06-17 The Dow Chemical Company High modulus polyurea elastomers prepared with amine-initiated polyols
GB9022194D0 (en) 1990-10-12 1990-11-28 Ici Plc Method for preparing polyurea-polyurethane flexible foams
DE4200558A1 (de) * 1992-01-11 1993-07-15 Basf Ag Verfahren zur herstellung von polyurethan-hartschaeumen sowie treibmittelmischung hierfuer
CA2132595C (en) * 1993-09-22 1999-03-16 Thomas L. Fishback Polyol composition having good flow and water blown rigid polyurethane foams made thereby having good dimensional stability
US5840212A (en) * 1996-10-23 1998-11-24 Bayer Corporation Rigid foams with improved insulation properties and a process for the production of such foams
IT1289472B1 (it) * 1996-12-19 1998-10-15 Manni S P A Procedimento ed apparecchiatura per la schiumatura sottovuoto di pannelli isolanti,con insufflaggio di gas inerte
DE19723193A1 (de) * 1997-06-03 1998-12-10 Bayer Ag Verfahren zur Herstellung von geschlossenzelligen Polyurethan-Hartschaumstoffen mit geringer Wärmeleitfähigkeit
ATE485323T1 (de) * 2001-05-21 2010-11-15 Huntsman Int Llc Sehr weiches polyurethan elastomer
JP4132758B2 (ja) * 2001-09-06 2008-08-13 サンアプロ株式会社 新規アミジン化合物、その製造法、および使用法
CA2629090C (en) * 2005-11-14 2014-05-27 Dow Global Technologies Inc. Method of molding rigid polyurethane foams with enhanced thermal conductivity
US8193257B2 (en) 2007-01-30 2012-06-05 Dow Global Technologies Llc Amine-initiated polyols and rigid polyurethane foam made therefrom

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5114988A (en) * 1989-10-23 1992-05-19 Basf Corporation Polyether polyols having reduced unsaturation and polyurethane foams prepared therefrom
US5461084A (en) * 1994-09-26 1995-10-24 Bayer Corporation Rigid foams with improved insulation and physical properties
KR20050020780A (ko) * 2002-04-17 2005-03-04 바이엘 머티리얼싸이언스 엘엘씨 히드로플루오로카본 및 이산화탄소로 발포된 폴리우레탄또는 폴리이소시아누레이트 폼

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20240082749A (ko) 2022-12-02 2024-06-11 주식회사 엘지에너지솔루션 표면 처리된 분리막을 포함하는 전극 조립체, 이를 포함하는 이차전지 및 전극 조립체의 제조방법

Also Published As

Publication number Publication date
US20100298458A1 (en) 2010-11-25
EP2115027B1 (en) 2018-10-03
RU2467025C2 (ru) 2012-11-20
JP2010516818A (ja) 2010-05-20
RU2009132507A (ru) 2011-03-10
JP5366829B2 (ja) 2013-12-11
WO2008094963A1 (en) 2008-08-07
WO2008094238A1 (en) 2008-08-07
TR201821164T4 (tr) 2019-01-21
ES2699625T3 (es) 2019-02-12
US8318826B2 (en) 2012-11-27
CN101641386A (zh) 2010-02-03
MX2009008156A (es) 2009-10-08
EP2115027A1 (en) 2009-11-11
KR20090112736A (ko) 2009-10-28

Similar Documents

Publication Publication Date Title
KR101476468B1 (ko) 시스 및／또는 트랜스―오르토―시클로헥산디아민-개시된 폴리올 및 그로부터 제조된 경질 폴리우레탄 발포체
KR101476469B1 (ko) 아민-개시된 폴리올 및 그로부터 제조된 경질 폴리우레탄 발포체
EP2411436B1 (en) Production of rigid polyurethane foams and the use thereof
WO2009091705A2 (en) Thermally insulating isocyanate-based foams
KR101837207B1 (ko) 1,3- 및/또는 1,4-비스(아미노메틸)시클로헥산-개시된 폴리올 및 적어도 하나의 메틸렌 비스(시클로헥실아민)-개시된 폴리올 및 시클로헥산디아민-개시된 폴리올을 포함하는 폴리올 혼합물 및 그들로부터 만들어진 폴리우레탄
JP5612570B2 (ja) メチレンビス（シクロヘキシルアミン）開始ポリオール及び該ポリオールから作製される硬質ポリウレタンフォーム
MX2011001092A (es) Sistemas de poliuretano rigido basados en polioles iniciados con orto-ciclohexanodiamina.
MX2011001094A (es) Mezclas de poliol conteniendo polioles iniciados con orto-ciclohexanodiamina para espumas de poliuretano rigidas.
JP5687190B2 (ja) １，３−又は１，４−ビス（アミノメチル）シクロヘキサン開始ポリオール及び該ポリオールから作製される硬質ポリウレタンフォーム

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

PN2301 Change of applicant

St.27 status event code: A-3-3-R10-R13-asn-PN2301

St.27 status event code: A-3-3-R10-R11-asn-PN2301

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

FPAY Annual fee payment

Payment date: 20171117

Year of fee payment: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

FPAY Annual fee payment

Payment date: 20181115

Year of fee payment: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 9

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 10

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 11

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 12