KR101363824B1 - 최적화된 액상 산화를 위한 기포탑 반응기 - Google Patents

최적화된 액상 산화를 위한 기포탑 반응기 Download PDF

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KR101363824B1
KR101363824B1 KR1020127032262A KR20127032262A KR101363824B1 KR 101363824 B1 KR101363824 B1 KR 101363824B1 KR 1020127032262 A KR1020127032262 A KR 1020127032262A KR 20127032262 A KR20127032262 A KR 20127032262A KR 101363824 B1 KR101363824 B1 KR 101363824B1
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reaction medium
reaction
bubble column
reaction zone
feed
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Korean (ko)
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KR20130003039A (ko
Inventor
알란 조지 원더스
로버트 린
브리데 마르셀 데
리 레이놀즈 파틴
웨인 스코트 스트라세르
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그루포 페트로테멕스 에스.에이. 데 씨.브이.
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Priority claimed from US11/154,202 external-priority patent/US7692036B2/en
Priority claimed from US11/154,218 external-priority patent/US7568361B2/en
Application filed by 그루포 페트로테멕스 에스.에이. 데 씨.브이. filed Critical 그루포 페트로테멕스 에스.에이. 데 씨.브이.
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1872—Details of the fluidised bed reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1836—Heating and cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/23—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
    • C07C51/235—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/0015—Plates; Cylinders

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Combustion & Propulsion (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020127032262A 2004-09-02 2005-08-29 최적화된 액상 산화를 위한 기포탑 반응기 Expired - Lifetime KR101363824B1 (ko)

Applications Claiming Priority (11)

Application Number Priority Date Filing Date Title
US60685604P 2004-09-02 2004-09-02
US60/606,856 2004-09-02
US63132004P 2004-11-29 2004-11-29
US63139904P 2004-11-29 2004-11-29
US60/631,399 2004-11-29
US60/631,320 2004-11-29
US11/154,218 2005-06-16
US11/154,202 2005-06-16
US11/154,202 US7692036B2 (en) 2004-11-29 2005-06-16 Optimized liquid-phase oxidation
US11/154,218 US7568361B2 (en) 2004-09-02 2005-06-16 Optimized liquid-phase oxidation
PCT/US2005/030546 WO2006028752A2 (en) 2004-09-02 2005-08-29 Optimized liquid-phase oxidation

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
KR1020077006865A Division KR101281347B1 (ko) 2004-09-02 2005-08-29 최적화된 액상 산화 방법

Publications (2)

Publication Number Publication Date
KR20130003039A KR20130003039A (ko) 2013-01-08
KR101363824B1 true KR101363824B1 (ko) 2014-02-17

Family

ID=35504618

Family Applications (2)

Application Number Title Priority Date Filing Date
KR1020127032262A Expired - Lifetime KR101363824B1 (ko) 2004-09-02 2005-08-29 최적화된 액상 산화를 위한 기포탑 반응기
KR1020077006865A Expired - Lifetime KR101281347B1 (ko) 2004-09-02 2005-08-29 최적화된 액상 산화 방법

Family Applications After (1)

Application Number Title Priority Date Filing Date
KR1020077006865A Expired - Lifetime KR101281347B1 (ko) 2004-09-02 2005-08-29 최적화된 액상 산화 방법

Country Status (12)

Country Link
EP (1) EP1791800B1 (https=)
JP (1) JP2008511638A (https=)
KR (2) KR101363824B1 (https=)
CN (2) CN101023046B (https=)
BR (1) BRPI0514800B1 (https=)
CA (1) CA2576632A1 (https=)
ES (1) ES2655728T3 (https=)
LT (1) LT1791800T (https=)
MX (1) MX2007002565A (https=)
PL (1) PL1791800T3 (https=)
PT (1) PT1791800T (https=)
WO (1) WO2006028752A2 (https=)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8066949B2 (en) 2008-09-26 2011-11-29 Exxonmobil Research & Engineering Company Scrubber for fluid coker unit
US8933265B2 (en) * 2010-06-30 2015-01-13 Uop Llc Process for oxidizing alkyl aromatic compounds
US8933266B2 (en) * 2010-06-30 2015-01-13 Uop Llc Process for producing terephthalic acid
WO2015043698A1 (de) * 2013-09-25 2015-04-02 Linde Aktiengesellschaft Kolonne mit flüssigkeitsverteiler und stoffaustauschboden aus winkelprofilen
CN109772236B (zh) * 2017-11-14 2022-08-12 中国石油化工股份有限公司 一种流体分布器、反应装置及其应用
KR102849255B1 (ko) * 2021-12-10 2025-08-21 주식회사 엘지화학 기포탑 반응기

Citations (3)

* Cited by examiner, † Cited by third party
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KR19980063918A (ko) * 1996-12-12 1998-10-07 조안엠.젤사 기포 칼럼 반응기에 산소를 직접 주입시키는 방법
KR20020069261A (ko) * 2000-01-21 2002-08-29 비피 코포레이션 노쓰 아메리카 인코포레이티드 벤조산 및 물 용매 중의 산화에 의한 고순도 방향족카르복실산의 제조 방법
KR100400895B1 (ko) * 1998-07-23 2003-10-08 프랙스에어 테크놀로지, 인코포레이티드 반응기 시스템

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AT236346B (de) * 1961-01-25 1964-10-12 Union Carbide Corp Boden zum Inberührungbringen von Flüssigkeit und Gas
GB1062482A (en) * 1963-04-30 1967-03-22 Standard Oil Co High quality phthalic acids
GB1250222A (https=) * 1968-10-25 1971-10-20
US3660476A (en) * 1968-10-30 1972-05-02 Teijin Ltd Method for the preparation of terephthalic acid
BE724040A (https=) * 1968-11-18 1969-05-02
JPS5912096B2 (ja) * 1975-10-31 1984-03-21 三菱化学株式会社 ホウコウゾクポリカルボンサンノセイゾウホウ
JPS58177106A (ja) * 1982-04-13 1983-10-17 Jgc Corp 多段式高流速気液接触装置
JPS59104345A (ja) * 1982-12-03 1984-06-16 Kuraray Yuka Kk 直接重合用に適したテレフタル酸の製造方法
DE4318893A1 (de) * 1993-06-07 1994-12-08 Bayer Ag Reaktor und damit durchzuführendes kontinuierliches Verfahren zur Herstellung von Ethylenglykolcarbonat bzw. Propylenglykolcarbonat
JP3719448B2 (ja) * 1993-07-29 2005-11-24 三菱瓦斯化学株式会社 芳香族ジカルボン酸製造用酸化反応器
SI9500109A (en) * 1995-04-05 1996-10-31 Levec Janez Dipl Ing Prof Dr Apparatus and Process for Thermal Oxidative Treatment of Waste Waters
US5929274A (en) * 1995-06-07 1999-07-27 Hfm International, Inc. Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid
JPH09278709A (ja) * 1996-02-13 1997-10-28 Mitsubishi Chem Corp 芳香族カルボン酸の製造方法
GB9701251D0 (en) * 1997-01-22 1997-03-12 Bp Chem Int Ltd Process
DE19843573A1 (de) * 1998-09-23 2000-03-30 Degussa Blasensäule und deren Verwendung
BR0316462A (pt) * 2002-12-09 2005-10-11 Eastman Chem Co Processos para reduzir uma suspensão de ácido carboxìlico purificado, para purificar um produto de oxidação em estágios, para produzir um produto de ácido carboxìlico purificado, e, suspensão de ácido carboxìlico purificado
JP2006509044A (ja) * 2002-12-09 2006-03-16 イーストマン ケミカル カンパニー 粗製カルボン酸スラリーの精製方法
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid

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Publication number Priority date Publication date Assignee Title
KR19980063918A (ko) * 1996-12-12 1998-10-07 조안엠.젤사 기포 칼럼 반응기에 산소를 직접 주입시키는 방법
KR100400895B1 (ko) * 1998-07-23 2003-10-08 프랙스에어 테크놀로지, 인코포레이티드 반응기 시스템
KR20020069261A (ko) * 2000-01-21 2002-08-29 비피 코포레이션 노쓰 아메리카 인코포레이티드 벤조산 및 물 용매 중의 산화에 의한 고순도 방향족카르복실산의 제조 방법

Also Published As

Publication number Publication date
EP1791800B1 (en) 2017-11-01
LT1791800T (lt) 2018-01-25
JP2008511638A (ja) 2008-04-17
WO2006028752A2 (en) 2006-03-16
PT1791800T (pt) 2018-02-02
BRPI0514800A (pt) 2008-06-24
KR20070048256A (ko) 2007-05-08
MX2007002565A (es) 2007-04-24
CA2576632A1 (en) 2006-03-16
WO2006028752A3 (en) 2006-06-01
PL1791800T3 (pl) 2018-04-30
CN101023046B (zh) 2019-01-18
EP1791800A2 (en) 2007-06-06
CN101023046A (zh) 2007-08-22
KR20130003039A (ko) 2013-01-08
CN101766979B (zh) 2012-12-26
CN101766979A (zh) 2010-07-07
ES2655728T3 (es) 2018-02-21
BRPI0514800B1 (pt) 2015-11-24
KR101281347B1 (ko) 2013-07-02

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