KR101281347B1 - 최적화된 액상 산화 방법 - Google Patents

최적화된 액상 산화 방법 Download PDF

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Publication number
KR101281347B1
KR101281347B1 KR1020077006865A KR20077006865A KR101281347B1 KR 101281347 B1 KR101281347 B1 KR 101281347B1 KR 1020077006865 A KR1020077006865 A KR 1020077006865A KR 20077006865 A KR20077006865 A KR 20077006865A KR 101281347 B1 KR101281347 B1 KR 101281347B1
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South Korea
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reaction medium
reaction
reaction zone
oxidation
horizontal
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KR1020077006865A
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English (en)
Korean (ko)
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KR20070048256A (ko
Inventor
알란 조지 원더스
로버트 린
브리데 마르셀 데
리 레이놀즈 파틴
웨인 스코트 스트라세르
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그루포 페트로테멕스 에스.에이. 데 씨.브이.
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Priority claimed from US11/154,218 external-priority patent/US7568361B2/en
Priority claimed from US11/154,202 external-priority patent/US7692036B2/en
Application filed by 그루포 페트로테멕스 에스.에이. 데 씨.브이. filed Critical 그루포 페트로테멕스 에스.에이. 데 씨.브이.
Publication of KR20070048256A publication Critical patent/KR20070048256A/ko
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1872—Details of the fluidised bed reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1836—Heating and cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/23—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
    • C07C51/235—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/0015—Plates; Cylinders

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Combustion & Propulsion (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020077006865A 2004-09-02 2005-08-29 최적화된 액상 산화 방법 Expired - Lifetime KR101281347B1 (ko)

Applications Claiming Priority (11)

Application Number Priority Date Filing Date Title
US60685604P 2004-09-02 2004-09-02
US60/606,856 2004-09-02
US63132004P 2004-11-29 2004-11-29
US63139904P 2004-11-29 2004-11-29
US60/631,399 2004-11-29
US60/631,320 2004-11-29
US11/154,202 2005-06-16
US11/154,218 US7568361B2 (en) 2004-09-02 2005-06-16 Optimized liquid-phase oxidation
US11/154,218 2005-06-16
US11/154,202 US7692036B2 (en) 2004-11-29 2005-06-16 Optimized liquid-phase oxidation
PCT/US2005/030546 WO2006028752A2 (en) 2004-09-02 2005-08-29 Optimized liquid-phase oxidation

Related Child Applications (1)

Application Number Title Priority Date Filing Date
KR1020127032262A Division KR101363824B1 (ko) 2004-09-02 2005-08-29 최적화된 액상 산화를 위한 기포탑 반응기

Publications (2)

Publication Number Publication Date
KR20070048256A KR20070048256A (ko) 2007-05-08
KR101281347B1 true KR101281347B1 (ko) 2013-07-02

Family

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Application Number Title Priority Date Filing Date
KR1020077006865A Expired - Lifetime KR101281347B1 (ko) 2004-09-02 2005-08-29 최적화된 액상 산화 방법
KR1020127032262A Expired - Lifetime KR101363824B1 (ko) 2004-09-02 2005-08-29 최적화된 액상 산화를 위한 기포탑 반응기

Family Applications After (1)

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KR1020127032262A Expired - Lifetime KR101363824B1 (ko) 2004-09-02 2005-08-29 최적화된 액상 산화를 위한 기포탑 반응기

Country Status (12)

Country Link
EP (1) EP1791800B1 (https=)
JP (1) JP2008511638A (https=)
KR (2) KR101281347B1 (https=)
CN (2) CN101766979B (https=)
BR (1) BRPI0514800B1 (https=)
CA (1) CA2576632A1 (https=)
ES (1) ES2655728T3 (https=)
LT (1) LT1791800T (https=)
MX (1) MX2007002565A (https=)
PL (1) PL1791800T3 (https=)
PT (1) PT1791800T (https=)
WO (1) WO2006028752A2 (https=)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8066949B2 (en) 2008-09-26 2011-11-29 Exxonmobil Research & Engineering Company Scrubber for fluid coker unit
US8933266B2 (en) * 2010-06-30 2015-01-13 Uop Llc Process for producing terephthalic acid
US8933265B2 (en) * 2010-06-30 2015-01-13 Uop Llc Process for oxidizing alkyl aromatic compounds
RU2670891C9 (ru) * 2013-09-25 2018-12-11 Линде Акциенгезелльшафт Колонна с жидкостными распределителями и массообменными тарелками из уголковых профилей
CN109772236B (zh) * 2017-11-14 2022-08-12 中国石油化工股份有限公司 一种流体分布器、反应装置及其应用
KR102849255B1 (ko) 2021-12-10 2025-08-21 주식회사 엘지화학 기포탑 반응기
CN116351334A (zh) * 2022-12-14 2023-06-30 安徽利科新材料科技有限公司 Mnmp生产装置及生产方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR19980063918A (ko) * 1996-12-12 1998-10-07 조안엠.젤사 기포 칼럼 반응기에 산소를 직접 주입시키는 방법
KR20000070341A (ko) * 1997-01-22 2000-11-25 데이 수잔 자넷 아세트산의 제조방법
KR20020069261A (ko) * 2000-01-21 2002-08-29 비피 코포레이션 노쓰 아메리카 인코포레이티드 벤조산 및 물 용매 중의 산화에 의한 고순도 방향족카르복실산의 제조 방법

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT236346B (de) * 1961-01-25 1964-10-12 Union Carbide Corp Boden zum Inberührungbringen von Flüssigkeit und Gas
DE1493192A1 (de) * 1963-04-30 1969-02-20 Standard Oil Co Verfahren zur Herstellung von aromatischen Saeuren
GB1250222A (https=) * 1968-10-25 1971-10-20
US3660476A (en) * 1968-10-30 1972-05-02 Teijin Ltd Method for the preparation of terephthalic acid
BE724040A (https=) * 1968-11-18 1969-05-02
JPS5912096B2 (ja) * 1975-10-31 1984-03-21 三菱化学株式会社 ホウコウゾクポリカルボンサンノセイゾウホウ
JPS58177106A (ja) * 1982-04-13 1983-10-17 Jgc Corp 多段式高流速気液接触装置
JPS59104345A (ja) * 1982-12-03 1984-06-16 Kuraray Yuka Kk 直接重合用に適したテレフタル酸の製造方法
DE4318893A1 (de) * 1993-06-07 1994-12-08 Bayer Ag Reaktor und damit durchzuführendes kontinuierliches Verfahren zur Herstellung von Ethylenglykolcarbonat bzw. Propylenglykolcarbonat
JP3719448B2 (ja) * 1993-07-29 2005-11-24 三菱瓦斯化学株式会社 芳香族ジカルボン酸製造用酸化反応器
SI9500109A (en) * 1995-04-05 1996-10-31 Levec Janez Dipl Ing Prof Dr Apparatus and Process for Thermal Oxidative Treatment of Waste Waters
US5929274A (en) * 1995-06-07 1999-07-27 Hfm International, Inc. Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid
JPH09278709A (ja) * 1996-02-13 1997-10-28 Mitsubishi Chem Corp 芳香族カルボン酸の製造方法
US6084125A (en) * 1996-02-27 2000-07-04 Praxair Technology, Inc. Process for producing aliphatic acids using a reactor system having a shell and a tube reactor configuration to force circulation of reaction liquid
DE19843573A1 (de) * 1998-09-23 2000-03-30 Degussa Blasensäule und deren Verwendung
WO2004052821A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
JP2006509044A (ja) * 2002-12-09 2006-03-16 イーストマン ケミカル カンパニー 粗製カルボン酸スラリーの精製方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR19980063918A (ko) * 1996-12-12 1998-10-07 조안엠.젤사 기포 칼럼 반응기에 산소를 직접 주입시키는 방법
KR20000070341A (ko) * 1997-01-22 2000-11-25 데이 수잔 자넷 아세트산의 제조방법
KR20020069261A (ko) * 2000-01-21 2002-08-29 비피 코포레이션 노쓰 아메리카 인코포레이티드 벤조산 및 물 용매 중의 산화에 의한 고순도 방향족카르복실산의 제조 방법

Also Published As

Publication number Publication date
PL1791800T3 (pl) 2018-04-30
LT1791800T (lt) 2018-01-25
KR20070048256A (ko) 2007-05-08
EP1791800B1 (en) 2017-11-01
ES2655728T3 (es) 2018-02-21
WO2006028752A2 (en) 2006-03-16
WO2006028752A3 (en) 2006-06-01
BRPI0514800A (pt) 2008-06-24
CN101023046A (zh) 2007-08-22
CN101766979A (zh) 2010-07-07
CA2576632A1 (en) 2006-03-16
KR20130003039A (ko) 2013-01-08
JP2008511638A (ja) 2008-04-17
CN101766979B (zh) 2012-12-26
MX2007002565A (es) 2007-04-24
EP1791800A2 (en) 2007-06-06
CN101023046B (zh) 2019-01-18
BRPI0514800B1 (pt) 2015-11-24
KR101363824B1 (ko) 2014-02-17
PT1791800T (pt) 2018-02-02

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