KR101241671B1 - A natural fertilizer and deodorizer composite, and a manufacturing method of the same - Google Patents

Abstract

PURPOSE: A natural composition for a plant growth and deodorization and a preparation method thereof are provided to have an improved effect on deodorization, plant growth, and soil improvement. CONSTITUTION: A preparation method of a natural composition for a plant growth and deodorization comprises a step(ST1) of pulverizing raw materials, a step(ST3) of cooling the raw materials while rotating the raw materials in a rotary drum, a step(ST4) of drying cooled raw material powder under sunlight, a step(ST6) of mixing the dried raw material powder in a designated ratio, a step(ST8) of rotating the mixture and cooling the mixture, a step(ST9) of cooling the mixture under the shade, a step(ST10) of regrinding the dried mixture in minute powder form, and a step(ST14) of mixing and stirring the powder, molasses, and water and aging the mixture. [Reference numerals] (ST1) Pulverizing raw materials; (ST10) Re-pulverizing into powder; (ST11) Packaging; (ST12) Naturally maturing; (ST13) Mixing and stirring matured powder, molasses, and water; (ST14) Maturing at room temperature; (ST15) Packaging and shipping; (ST2,S7) Heating by rotating a rotary drum at high speed; (ST3,ST8) Cooling by rotating the rotary drum at low speed; (ST4) Drying under the sunlight; (ST5) Individual packaging; (ST6) Mixing different kinds of raw materials; (ST9) Drying under the shade

Description

A natural fertilizer and deodorizer composite, and a manufacturing method of the same}

The present invention relates to a natural composition for plant growth and deodorization, and a method for manufacturing the same. Specifically, natural fertilizers, soil modifiers, and deodorants are prepared by processing, blending, treating, and ripening various natural materials easily obtainable in a natural state. It relates to a natural composition having an excellent effect as a method and a method for producing the same.

In growing crops, the soil should not be acidified, but the soil should have a variety of high-quality nutrients. Nutrients such as nitrogen, phosphate, and potassium, which are needed for plants to grow, start to be depleted due to the long use of the soil. Therefore, fertilizers such as ammonium sulfate, superphosphate, and potassium sulfate are supplied to artificially supply essential nutrients to plants.

However, the use of such various artificial fertilizers promote acidification of the soil, which eventually prevents the plants from growing properly, and has a disadvantage of weakening resistance to pathogens such as filamentous fungi.

Thus, researches and efforts to develop organic or natural fertilizers or soil improvers extracted from various natural materials are continuing.

In addition, various methods have been attempted to remove odors generated from industrial wastewater, livestock wastewater, and infrastructural facilities. The basic methods of removing odors include decomposing odor causing substances, adsorption methods, spraying microorganisms, There is a method of removing the malodor by reacting the substance causing the malodor with a third substance.

Recently, various efforts have been made to remove odors without harming humans and harming livestock by developing materials that are extracted from natural materials rather than chemical compounds as odor removing materials.

Patent No. 10-0770427 "Method of preparing a wood (juk) vinegar composition, and wood (juk) vinegar composition prepared using the same", Patent No. 10-1026368 "Deodorizing fermentation composition containing mugwort and rice bran and The manufacturing method ", Patent No. 10-1145154" Pollution-free pesticides and its manufacturing method ", Korean Patent Publication No. 10-2012-0019335" Manufacturing method of eco-friendly organic fertilizer pellets using herbal medicine ", etc. are extracted from natural materials or fermented Agrochemicals, fertilizers and deodorants using the composition are disclosed.

Patent No. 10-0770427 discloses a method for preparing a composition having a wood vinegar solution by heating any one or more selected from various kinds of trees and the like and processing it in multiple stages to have a bactericidal, deodorant and plant nutrient component.

Korean Patent No. 10-1026368 discloses a method for preparing a deodorizing fermentation composition by mixing vermiculite and carbon source with mugwort and rice bran and fermenting them.

On the other hand, Patent No. 10-1145154 discloses a pollution-free pesticide that is prepared by absorbing wood vinegar to charcoal powder after the preparation of wood vinegar and adding plum to it.

Korean Patent Laid-Open Publication No. 10-2012-0019335 discloses a method of preparing fertilizer in pellet form by mixing, crushing and fermenting rice bran and the like by using herbal medicine by-products.

In the present invention, a method of preparing a natural composition which is harmless to human body through a multi-step processing process from a natural substance which can be easily obtained in nature and has excellent plant growth, soil improvement, and deodorizing effect, and deodorant, fertilizer, and soil produced thereby It is intended to provide a modifier.

Korean Patent No. 10-0770427 "Method of preparing a wood (juk) vinegar composition and wood (juk) vinegar composition prepared using the same" Patent No. 10-1026368 "Deodorization fermentation composition containing wormwood and rice bran and a method of manufacturing the same" Patent No. 10-1145154 "Pollution-free pesticides and its manufacturing method" Korean Patent Publication No. 10-2012-0019335 "Method of manufacturing environmentally friendly organic fertilizer pellets using herbal medicine"

It is an object of the present invention to grind, rotary frictionally heat, cool and dry natural materials such as birch, oak, sycamore, chaff and brown rice, and then re-compound each of these raw material powders, rotary frictional heating, cooling, drying, secondary grinding and After maturing, the molasses and water are mixed and stirred and aged to provide a natural composition that is harmless to the human body having excellent effects on deodorization, plant growth, soil improvement, and soil restoration.

Another object of the present invention is to provide a method for producing such a natural composition for plant growth and deodorization.

In order to achieve the above object, in the present invention, a) grinding each of the raw material consisting of birch, oak, sycamore, chaff and brown rice; B) Put each of the pulverized powder into a centrifugal rotary drum, rotate it at a rotational speed of 30 to 50 RPM under a temperature atmosphere of 80 to 90 ° C, hold it for 12 to 24 hours, and then rotate at a rotational speed of 30 RPM or less. Cooling down; C) drying the cooled raw material powder under sunlight to obtain a water content of 10 to 15%; D) 100 to 250 parts by weight of oak powder, 80 to 150 parts by weight of sycamore powder, 100 to 250 parts by weight of chaff powder, 80 to 150 parts by weight of brown rice powder Blending in a proportion of 100 to 300 parts by weight of water; E) putting the compound into a centrifugal rotary drum and rotating at a rotational speed of 30 to 50 RPM under a temperature atmosphere of 80 to 90 ° C. for 12 to 24 hours, and then rotating the mixture at a rotational speed of 30 RPM or less. ; F) drying the cooled blend in a well-ventilated shade so that the moisture content is 10-15%; G) regrinding the dried blend into a fine powder; H) mixing molasses and water in the regrind powder and stirring in a stirrer and aging at room temperature; It proposes a method for producing a natural composition for plant growth and deodorization comprising a.

Here, it is preferable to further include the step of natural ripening and storing for 6 to 12 months after packaging a predetermined amount of the regrind powder between the step 4) and the step a).

Meanwhile, at least one selected from pine needles, reeds, bran, and ginkgo biloba is added to the raw material of step a), and the dry powder of the added raw material is 50 to 150 weight parts based on 100 parts by weight of the birch powder in step d). It can be combined in parts.

At this time, the mixing ratio of the regrind powder, molasses, and water in step a) may be set to 1: 3 to 10:30 to 70 by mass.

According to another aspect of the present invention, there is provided a natural composition, a natural fertilizer, a soil improver and a deodorant, which is produced by the above production method.

Since the composition of the present invention is manufactured using natural materials such as various trees or chaff, it is harmless to the human body, has no skin irritation, and has excellent deodorizing and odor removing effects. In addition, it has excellent characteristics as a soil improver and has excellent characteristics in removing and preventing pests of crops and fruit trees during organic cultivation.

1 is a process flowchart showing the manufacturing process of the present invention in order.
Figure 2 is a report of acute toxicity test results of the composition according to the present invention.
Figure 3 is a skin stimulation toxicity test report of the composition according to the present invention.
4 is a heavy metal test report of the composition according to the present invention.
5 is a water test report of the composition according to the present invention.
6 is ammonia deodorization test report of the composition according to the present invention.
7 is a trimethylamine deodorization test report of the composition according to the present invention.
Figure 8 is a result of the beet cultivation test results of the composition according to the present invention.
Figure 9 is a test result of the presence and absence of the strain and antimicrobial activity of the composition according to the invention.

Hereinafter, the technical spirit of the present invention will be described in more detail.

The present invention is a raw material primary processing step of grinding, heating, cooling, drying and packaging natural materials such as birch, oak, bran, chaff, brown rice, pine needles, reeds, sycamore, and ginkgo biloba, and each of the primary raw materials Secondary processing steps of raw materials for compounding, heating, cooling, drying, regrinding, packing and aging at a predetermined rate, and final composition for packing and shipping after mixing, stirring and aging a certain amount of molasses and water in the second processed compound. It consists of a manufacturing step.

The raw material of the present invention is made of birch, oak, sycamore, chaff and brown rice as the main ingredients, and if necessary, one or more combinations selected from natural materials such as pine needles, reeds, bran, and ginkgo biloba may be added. .

Wood materials such as birch, oak, and sycamore, which are the raw materials, may be selected from leaves, stems, and roots, or may be mixed and used in a predetermined amount.

1 is a process flowchart showing the manufacturing process of the present invention in order. As shown, the method for producing a natural composition for plant growth and deodorization of the present invention (hereinafter, simply referred to as the method for preparing the composition of the present invention) is largely a raw material grinding step (ST1), a rotating drum high speed operation heating step (ST2), and rotation Drum low speed operation cooling step (ST3), solar drying step (ST4), individual packaging step (ST5), heterogeneous raw material mixing step (ST6), rotary drum high speed operation heating step (ST7), rotary drum low speed operation cooling step (ST8) ), Shade drying step (ST9), regrinding step into powder form (ST10), packing step (ST11), natural ripening step (ST12), mixing and stirring by adding a certain amount of molasses and water to the aged powder (ST13) ), The step of aging at room temperature (ST14) and the packaging and shipping step (ST15).

In the first step of processing each raw material (ST1 to ST5), each raw material is subjected to the individual packing step (ST5) from the raw material grinding step (ST1) to each material without mixing each raw material, and individually packed for each raw material. .

In the raw material grinding step (ST1), each raw material such as birch, oak, sycamore, chaff, brown rice, etc. is powdered using a grinder.

One kind of powder raw material is put into a centrifugal rotary drum (wood cylinder), and the drum is heated while operating at a rotational speed of 30 to 50 RPM. The raw material powder injected into the rotating drum increases in temperature due to frictional heat and maintains the operation of the rotating drum for 12 to 24 hours while maintaining the temperature atmosphere inside the rotating drum at 80 to 90 ° C.

Thereafter, the raw material powder is cooled by a low speed operation (below 30 RPM) to gradually reduce the rotational speed of the rotating drum.

The cooled raw material powder is solar dried to have a water content of 15% or less.

When the solar drying is finished, the dried powder is packed in a predetermined amount unit.

These steps are performed separately for each raw material such as birch, oak, sycamore, chaff, brown rice, pine needles, reeds, bran, and ginkgo biloba.

100 to 250 parts by weight of oak powder, 100 to 250 parts by weight of sycamore powder, 80 to 150 parts by weight of rice hull powder, 100 parts by weight of birch, oak, sycamore, chaff, and brown rice individually packaged through the primary processing steps above It mix | blends at the ratio of -250 weight part, 80-150 weight part of brown rice powder, and 100-300 weight part of water (ST6).

The compound is placed in a centrifugal rotary drum and rotated at high speed at a speed of 30 to 50 RPM. At this time, the temperature inside the rotating drum to maintain 80 ~ 90 ℃ (ST7). After maintaining the temperature and rotation speed of the rotating drum for 12 to 24 hours, reduce the rotating speed of the rotating drum to less than 30 RPM rotational speed (ST8).

Next, the cooled mixture is dried in a well-ventilated shade so that the moisture content is 15% or less (ST9).

The shade-dried blend is processed into a powder form by regrinding into a finer powder form than the first processing step using a grinder (ST10).

Powder in fine powder form (regrinding powder) is packaged in a certain amount unit and then aged in a aging room for a certain period of time to mature naturally. The period of natural maturation is preferably about 6-12 months (ST11, ST12)

After the secondary processing step (ST6 ~ ST12) of the above raw materials to the regrind powder (powder form) is added by mixing a certain amount of molasses and water. The mixture is stirred in a stirrer and aged at room temperature for 12 to 48 hours.

Here, the mixing ratio between the regrind powder, molasses and water is preferably 300 to 1000 parts by weight of molasses and 3000 to 7000 parts by weight of water with respect to 100 parts by weight of the regrind powder.

The stock solution composition, which has undergone such a final composition preparation step (ST13 to ST14), is packaged in a predetermined amount unit, for example, in a 20Kg or 1 ton container and then shipped.

Example

1. Raw material preparation and primary processing

1) Grind each pine leaf, birch, reed, bran, rice husk, brown rice, oak, sycamore, and ginkgo biloba separately to prepare powder.

2) Put each raw material in powder state into the centrifugal rotating drum (wood cylinder) and operate the rotating drum at the speed of 30 ~ 50RPM, keep the temperature at 80 ~ 90 ℃ and operate for 12 ~ 24 hours.

3) After cooling the internal raw material powder while slowly reducing the speed of the rotating drum at 30 RPM.

4) The cooled raw material powder is dried in sunlight to have a moisture content of 10 ~ 15%, and then individually packed in 500kg units.

2. Secondary processing of raw materials

1) Each raw material powder prepared and packaged separately is pine needle 10-15kg, birch 10-15kg, reed 5-10kg, bran 10-15kg, brown rice 12-15kg, oak 20-25kg, sycamore 10-15kg, ginkgo leaf 5 Mix by mixing in a weight ratio of ~ 10kg, water 30kg.

2) Put the above mixture into a rotating drum and heat it for 12 to 24 hours at a temperature atmosphere of 80 ~ 90 ℃ and a rotation speed of 30 ~ 50 RPM.

3) Then, slowly reduce the rotational speed of the rotating drum below 30 RPM and cool the compound.

4) Dry the cooled formulation to 10-15% moisture content in a well-ventilated shade.

5) Shade dried blends are regrind into finer powder than the first processing step.

6) The regrind powder is packaged in 5kg unit and naturally aged in the aging room for 12 months.

3. Preparation of Final Composition

1) Mix 100 to 300 kg of molasses and 2 tons of water to 30 kg of natural aged regrind powder and stir in a stirrer and age at room temperature for 24 hours.

2) The aged mixed composition is packaged in 20 kg or 1 ton containers.

The composition of the present invention prepared through such a process was found to be excellent in the ability to decompose and remove ammonia and trimethylamine, which is a natural material, has no acute toxicity, is harmless to the human body, and causes various sludges and odors.

Therefore, the composition of the present invention can be used for purifying and decomposing sludge in various septic tanks, sewers and wastewater treatment plants, or for septic tank sludge, water tank contamination, and soil heavy metal fermentation. In addition, it has an excellent effect on the removal of odors in sewers and various barns. When applied to organic cultivation of plants, it is possible to prevent and remove pests of crops or fruit trees and to improve the growth of plants.

When the composition of the present invention is sprayed on soils such as orchards, paddy fields, and fields for plant growth, soil restoration, and soil improvement, water may be diluted and used by adding about 100 times to 1 liter of the composition stock solution of the present invention (before seeding). ).

For example, in the case of cultivation of Altari radish, it was confirmed that the fertilization of foliar fertilization by diluting 1000 times by adding water to the composition stock solution of the present invention improves the growth of Altari radish.

After seeding, the leaves of 5 leaves were sprouted after diluting by 500 to 1000 times by adding water to the composition stock solution of the present invention and then cultivating the foliar three times at 7-day intervals.

To remove odors in sewers, barns, rivers, and agricultural waterways, 50-fold water is added to the composition stock solution of the present invention, and diluted. 20 liters of the composition stock solution of the present invention is applied to 20 m2 of septic tank to prevent odor. great.

Figure 2 is a report of acute toxicity test results of the composition according to the invention, Figure 3 is a report of skin irritation toxicity test results of the composition according to the present invention. As shown in the results it can be confirmed that the composition of the present invention is a natural composition harmless to the human body without acute toxicity or skin irritation toxicity.

Figure 4 is a test report of heavy metals of the composition according to the present invention, Figure 5 is a test report of water quality of the composition according to the present invention, the composition (product name: OK53) of the present invention contains almost no heavy metals, the concern of water pollution It can be seen that there is no.

Figure 6 is a test report of ammonia deodorization of the composition according to the invention, Figure 7 is a trimethylamine deodorization test report of the composition according to the present invention. According to this, it can be seen that the deodorizing and malodor removing ability of the composition according to the present invention is excellent.

Figure 8 is a notification of the result of the cultivation of the radish cultivation test of the composition according to the present invention, it can be seen that the growth and yield of Altari radish increased when foliar treatment by diluting the composition stock solution of the present invention 1000 times.

9 is a test result of the presence of strain and antimicrobial activity of the composition according to the present invention can be seen in the composition of the present invention (OK53) a lot of useful bacteria lactic acid and yeast, excellent antibacterial activity against pathogens such as E. coli and Salmonella It can be seen that there is an effect of antibiotic replacement when used in livestock farms.

According to the composition of the present invention, it is possible to prevent and remove odors of sewers, septic tanks, factory wastewater and barns, and to prevent and remove plant pests and to improve plant growth when the plants are sprayed or treated in soil. . In addition, since the composition of the present invention is a natural composition harmless to the human body, it will need to be actively applied in various industrial waste disposal companies, livestock farms, fruit trees and crop growing farms.

Claims (8)

A) grinding each of the raw materials consisting of birch, oak, sycamore, chaff and brown rice;
B) Put each of the pulverized powder into a centrifugal rotary drum, rotate it at a rotational speed of 30 to 50 RPM under a temperature atmosphere of 80 to 90 ° C, hold it for 12 to 24 hours, and then rotate at a rotational speed of 30 RPM or less. Cooling down;
C) drying the cooled raw material powder under sunlight to obtain a water content of 15% or less;
D) 100 to 250 parts by weight of oak powder, 80 to 150 parts by weight of sycamore powder, 100 to 250 parts by weight of chaff powder, 80 to 150 parts by weight of brown rice powder Blending in a proportion of 100 to 300 parts by weight of water;
E) putting the compound into a centrifugal rotary drum and rotating at a rotational speed of 30 to 50 RPM under a temperature atmosphere of 80 to 90 ° C. for 12 to 24 hours, and then rotating the mixture at a rotational speed of 30 RPM or less. ;
F) drying the cooled blend in a well-ventilated shade so that the moisture content is less than 15%;
G) regrinding the dried blend into a fine powder;
H) mixing molasses and water in the regrind powder and stirring in a stirrer and aging at room temperature;
Method for producing a natural composition for plant growth and deodorization comprising a. The method of claim 1,
After the step of step 4) and the step a) after repacking the powder by a predetermined amount for 6 to 12 months of storage and for natural aging of the plant growth and deodorizing a natural composition further comprising the step of storing Manufacturing method. The method of claim 2,
At least one selected from pine needles, reeds, bran, and ginkgo biloba is added to the raw material of step a), and the dry powder of the added raw material is added in an amount of 50 to 150 parts by weight based on 100 parts by weight of the birch powder in step d). Method for producing a natural composition for plant growth and deodorization, characterized in that. 4. The method according to any one of claims 1 to 3,
Mixing ratio between the regrind powder, molasses, and water in the step a) is based on the mass 1: 1: 3 ~ 10: 30 ~ 70 method for producing a natural composition for plant growth and deodorization. A natural composition, which is prepared by the method of any one of claims 1 to 3. A natural fertilizer, characterized in that it is produced by the method of any one of claims 1 to 3. A natural soil modifier, characterized in that it is produced by any one of the manufacturing method of claim 1. A natural deodorant, characterized in that produced by any one of claims 1 to 3.

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