KR101104958B1 - Cosmetic composition for hair - Google Patents

Abstract

The present invention relates to a cosmetic composition for hair, more specifically, the coloring power of the hair dye is improved and the colored color lasts for a long time, can increase the tensile strength of the hair, and also has no side effects and high skin safety, can be used with confidence, The present invention relates to a hair cosmetic composition that can provide excellent hair moisturizing and nourishment to hair roots and hair, and at the same time, can remove dyes inherent odor and increase hair power. To this end, the cosmetic composition for hair according to the present invention fermented / matured the pulverized product consisting of 30-40% by weight black sesame seeds, 20-30% by weight kelp, 20-30% by weight cabbage, and 15-20% by weight of soybean paste, and then concentrated under reduced pressure. Spray-dried natural powder extract is characterized in that it comprises 1-15% by weight based on the total weight of the composition.

Dyeing power, hair power, spray drying, black sesame seed, kelp, cabbage, Cheonggukjang

Description

Cosmetic composition for hair {COSMETIC COMPOSITION FOR HAIR}

The present invention relates to a cosmetic composition excellent in dyeing power and hair power, and more particularly, the coloring power of the hair dye is improved and the colored color can be maintained for a long time, and the tensile strength of the hair can be increased, and there is no side effect and the skin safety is high. The present invention relates to a hair cosmetic composition having excellent dyeing power and hair power, which can provide excellent hair hydration and nutrition to hair roots and hair, and can simultaneously remove dye stains and increase the hair power.

Generally, hair dyes (hair dyes) can be classified into temporary hair dyes, semi-permanent hair dyes, and permanent hair dyes according to the degree of durability of the dyeing effect, and according to the type of hair dyes such as powder type, spray type, mousse type, gel type, Various formulations, such as shampoo or cream type, may be provided.

Among these dyes, the temporary hair dye can erase the colored color on the hair in one hair, and the effect of the dye on the hair is not significant. The semi-permanent hair dye damages the hair as the colored color lasts for 2-4 weeks. The degree of hair loss is not so great, but there is a disadvantage that hair coloring power is inferior. In the case of permanent hair dye, the coloring power is good, but the reaction of the use of alkali and decolorization of melanin by hydrogen peroxide is accompanied by a reaction. Larger than other hair dyes. Therefore, in the manufacture of hair dyes, there is a challenge in the art to find a hair dye composition capable of maximizing the coloring effect while increasing the tensile strength of the hair without causing hair damage.

In addition, there is a conditioning agent that is used to minimize hair damage caused by the use of hair dyes, which provides a conditioning effect and prevents damage through electrical adsorption with the hair, but most of the materials used as such conditioning agents It is difficult to use a large amount of hair dye because it often interferes with hair dyeing.

On the other hand, dyes formed through hair dyeing and chemical reactions in the cortex tend to discolor or fade over time. Minimizing such discoloration or fading is also a major challenge in the art. have.

Therefore, not only the dyeing ability to the hair is improved and the colored color lasts for a long time, but also the development of a hair dye without hair damage after dyeing is urgently required.

The present invention solves the above problems and is made by the request as described above, the object of the present invention has no side effects and high skin safety can be used with confidence, as well as excellent hair moisturizing and hair nourishment to hair, hair It is to provide a hair cosmetic composition having excellent dyeing power and hair power that can be provided and at the same time remove the dye odor, increase the hair power.

Hair cosmetic composition according to the present invention for achieving the above object is fermentation / maturation of the pulverized product consisting of 30-40% by weight black sesame, 20-30% by weight kelp, 20-30% by weight cabbage and 15-20% by weight After concentration under reduced pressure and spray-dried natural powder extract is characterized in that it comprises 1-15% by weight based on the total weight of the composition.

Preferably, the natural powder extract is characterized in that the pulverized product is fermented at 20 to 25 ℃ for 15 to 20 days, and the filtrate is filtered and aged for 25 days at a constant temperature of 12 ℃.

Also preferably, the pulverized product further includes at least one natural material selected from garlic, round leek, loach, parsley, 톳, gompi, brown rice, ocher and seaweed, wherein the natural material is 100 parts by weight of the pulverized product. It is characterized by further comprising 1 to 5 parts by weight.

According to the present invention, rather than artificially solvent treatment or heat treatment to extract the effective substance of the natural substance, but through the fermentation and maturation step of the natural plant, by preventing and ripening the destruction of the efficacy of natural resources according to high temperature and heating It can solve the anti-corruption of natural materials at the same time, and can prevent the risk of skin irritation by not using any other solvent, and also obtain the fragrant natural powder extract, and by using it, enhances the dyeing power and hair power. It can increase and facilitate the improvement of dermatitis problem which is a problem when using synthetic raw materials.

Hereinafter, the present invention will be described in detail with reference to examples of the present invention. These examples are only for illustrating the present invention in more detail, it will be apparent to those skilled in the art that the scope of the present invention is not limited by these examples in accordance with the gist of the present invention. .

The cosmetic composition for hair according to the present invention has no side effects and has high skin safety, so that it can be used safely, and continuous research has been carried out to develop a composition of natural resources which can simultaneously exhibit the coloring strength enhancement and tensile strength effect of the hair according to an excellent hair dye. As a result, it was developed by confirming that the mixed extract of specific natural resources exhibits the above effects.

Hair cosmetic composition according to the present invention fermented / matured pulverized product consisting of 30-40% by weight black sesame seeds, 20-30% by weight kelp, 20-30% by weight cabbage and 15-20% by weight of chunggukjang and concentrated under reduced pressure spray drying The powdered natural extract is characterized in that it comprises 1-15% by weight based on the total weight of the composition.

Hair cosmetic composition according to the present invention fermentation of black sesame, kelp, cabbage and Cheonggukjang fermentation of glucose and fructose in the cabbage changes into alcohol, vitamin C, tocopherol, free amino acid, minerals, iodine Since it is possible to extract a significant amount of the active ingredient, etc., it is possible to obtain an excellent effect of increasing the dyeing force and the hair tension force by interaction with the active ingredient of black sesame, kelp, soybean cabbage and Cheonggukjang without using any other solvent, the present invention Uses this effect.

The natural powder extract was fermented for 15-20 days at 20 ~ 25 ℃ the black sesame seed, kelp, cabbage cabbage and Cheonggukjang, and the filtrate was filtered at 25 ℃ constant temperature for 25 days and concentrated under reduced pressure After spray drying is carried out. At this time, it is effective to carry out the vacuum concentration until the mass of the matured product is concentrated to the first 40-45% by the vacuum evaporator.

In addition, a mixer or the like is used for crushing natural resources. The fermentation is carried out at 20 to 25 ° C. for 15 to 20 days in relation to the fermentation capacity of the natural strains and enzymes in the cabbage. When the temperature is 20 ° C. or lower, the fermentation period becomes too long, and the temperature exceeds 25 ° C. This is because there is a risk that natural strains die and fermentation is stopped. In addition, if the fermentation at the temperature for 15 to 20 days, all of the sugar disappears and the fermentation is completed.

When the fermentation is complete, avoiding direct sunlight and aging for 25 days at 12 ℃ continuously without changing the temperature. This is because, when the aged extract is exposed to direct sunlight, the extract, which is easily oxidized and is called a living organic substance, changes well according to time, temperature, and light. In other words, if the temperature is too low, the aging does not work properly. If the temperature is too high, it is not suitable for aging for a long time. Therefore, in order to extract the active ingredient, the aging temperature is preferably 12 ° C. and the period is preferably 25 days. Do. Through this aging step, many active ingredients are eluted.

The aged extract is concentrated under reduced pressure until the extract mass reaches the first 40-45%, in order to shorten the process time when the spray dryer is used. Here, it is preferable to perform concentration under reduced pressure of 25-35 CmHg. This is because when the concentration is less than 25CmHg, the concentration time is long, and when the concentration exceeds 35CmHg, a large amount of active ingredient is released.

Finally, the final extract obtained by using the spray concentrated extractor (In let: 150 ~ 200 ℃, Out let: 80 ~ 100 ℃) is a natural powder extract. By using a spray dryer, it is possible to high concentration of the active ingredient to remove the alcohol components that can cause skin irritation and to have the effect of enhancing the dyeing power and increasing the hair power.

In the hair cosmetic composition according to the present invention, the pulverized product further comprises at least one natural material selected from garlic, round leek, loot, parsley, 톳, gompi, brown rice, ocher and seaweed, wherein the natural material is the pulverized product. It is characterized by further comprising 1 to 5 parts by weight based on 100 parts by weight. If the amount of these natural substances is less than 1 part by weight with respect to 100 parts by weight of black sesame seed, kelp, cabbage and cheonggukjang pulverized powder, it does not sufficiently play a role in strengthening the dyeing force. This is because the effect on is insignificant and does not have an effect as a supplemental effect.

Hereinafter, although an Example and a comparative example are given and this invention is demonstrated in detail, the technical scope of this invention is not limited to these Examples.

Example 1

Grind 40kg of black sesame, 20kg of kelp, 20kg of cabbage cabbage and 20kg of Cheonggukjang, put them in a brewing container, ferment at 23 ℃ for 20 days, filter with 200 mesh filter cloth (Chang-Gye Co., Ltd.), and continuously keep the temperature at 12 ℃. It was aged for 25 days. The dried product (41kg) was concentrated under reduced pressure using a Tokyo Rikakikai Co., Rotary vacuum evaporator until the mass of the matured product was concentrated to about 45% of the original, and then powdered using a spray dryer (model MH-8). 5.3 kg of natural extract was obtained.

[Example 2]

Grind 40 kg of black sesame, 20 kg of kelp, 20 kg of cabbage cabbage, 20 kg of Cheonggukjang and 20 kg of round leek, put them in a brewing container, ferment at 23 ° C. for 20 days, filter them with 200 mesh filter cloth, and keep the temperature unchanged. It was continuously aged at 12 ° C. for 25 days. The matured product (42.8kg) was concentrated under reduced pressure using a Tokyo Rikakikai Co., Rotary vacuum evaporator until the mass of the matured product was concentrated to about 45% of the original, and then powdered using a spray dryer (model MH-8). 5.5 kg of natural extract was obtained.

Comparative Example 1

Black sesame seed 40kg, kelp 20kg, 20kg cabbage 20kg and 15kg of chunggukjang crushed and crushed, and then extracted with 100L ethanol for 7 days and filtered using a 200 mesh filter cloth (Cheongggye Sangsa). The extract was concentrated under reduced pressure with a vacuum vacuum evaporator (Tokyo Rikakikai co, Rotary vacuum evaporator) until it was concentrated to 45% of the initial mass of the extract to obtain a viscous concentrated concentrate.

Comparative Example 2

Black sesame 40kg, kelp 20kg, cabbage 20kg, Cheonggukjang 15kg and 2kg of round leeks were crushed and pulverized after 48 hours of heat extraction with 250L of water to obtain an extract and filtered using a 200 mesh filter cloth (Cheongggye Sangsang). The extract was concentrated under reduced pressure with a vacuum vacuum evaporator (Tokyo Rikakikai co, Rotary vacuum evaporator) until it was concentrated to 45% of the initial mass of the extract to obtain a viscous concentrated concentrate.

Production Example A

Using the composition of Table 1 to prepare a hair dye composition for enhancing the dyeing power according to a conventional manufacturing method.

[Table 1]

Ingredient Name Preparation Example 1 Production Example 2 compare
Production Example 1 compare
Preparation Example 2 A p-phenylenediamine 1.0 1.0 1.0 1.0 p-aminophenol 1.8 1.8 1.8 1.8 o-aminophenol 3.8 3.8 3.8 3.8 m-aminophenol 0.15 0.15 0.15 0.15 B Sodium perborate (monohydrate) 28.0 28.0 28.0 28.0 Citric acid 5.0 5.0 5.0 5.0 Sodium Edetate 0.5 0.5 0.5 0.5 C Natural powder extract of Example 1 15 - - - Natural powder extract of Example 2 - 15 - - Decompression concentrate of Comparative Example 1 - - 15 - Decompression concentrate of Comparative Example 2 - - - 15 D Purified water TO 100.0 TO 100.0 TO 100.0 TO 100.0

[Manufacture example B]

To prepare a shampoo composition for increasing hair power according to a conventional manufacturing method using the composition of Table 2 below.

TABLE 2

fair Ingredient Name Production Example 3 Preparation Example 4 compare
Preparation Example 3 compare
Preparation Example 4 A Micolin ES-430 25.00 25.00 25.00 25.00 Micolin S-430 15.00 15.00 15.00 15.00 Micopol CDE 3.60 3.60 3.60 3.60 Glycerin 1.40 1.40 1.40 1.40 Mitain ca 3.00 3.00 3.00 3.00 KF 6011 0.30 0.30 0.30 0.30 Para-m 0.20 0.20 0.20 0.20 B Purified water 10.0 10.0 10.0 10.0 P.G 1.00 1.00 1.00 1.00 EDTA-2Na 0.20 0.20 0.20 0.20 Germall 115 0.10 0.10 0.10 0.10 IPBC-30 0.30 0.30 0.30 0.30 C incense 0.20 0.2 0.2 0.2 D Natural powder extract of Example 1 5.00 - - - Natural powder extract of Example 2 - 5.00 - - Decompression concentrate of Comparative Example 1 - - 5.00 - Decompression concentrate of Comparative Example 2 - - - 5.00 E Purified water To 100 To 100 To 100 To 100

Experimental Example 1: Hair Coloring Experiment

Preparation Example 1-2 and Comparative Preparation Example 1-2 of Preparation Example A were applied to the hair bundle having a weight of 1.5 g and a length of 180 mm using a commercially available Korean KS standard white hair for hair dye test, and left at room temperature for 25 minutes. Next, it was washed once with shampoo and dried for 3 hours or more using natural wind. Since the dyeing power and the persistence of the color can be said to be larger as the color difference increases after a certain time, the color difference (ΔE) between the hair treated and the untreated hair is measured using a spectrophotometer (Spectrophotometer CM-3500d, Minolta Co., Ltd., Japan, light source: xenon lamp, wavelength: 400-700nm, reflection angle: 8 °) and the results are shown in Table 3 below.

[Table 3] Hair Coloring Test Results

 Coloring power (ΔE) Preparation Example 1 Production Example 2 Comparative Preparation Example 1 Comparative Production Example 2 Hair Coloring Force (ΔE) 87 88 49 52

When viewing the results shown in Table 3, the color difference in the dyeing agent composition for enhancing the dyeing power of Preparation Example 1 and Preparation Example 2 containing the natural powder extract according to the present invention, it can be seen that the hair dyeing effect is high.

[Experimental Example 2: Comparative Test of Tensile Strength of Hair]

Tensile strength of hair when the shampoo containing the natural powder extract prepared in Preparation Example 3 of Preparation Example B and the shampoo containing the reduced pressure concentrate prepared in Comparative Preparation Example 3 were used. Each group was divided into two groups, each of which consisted of 10 people, and were measured by conducting a clinical trial once a day for 8 weeks. At this time, the tensile strength measurement of the hair was used a digital force gauge (DPS-5R). The measurement results are shown in Table 4.

Table 4 Hair Tensile Strength Test Results

NO Preparation Example 3 Use Group Comparative Production Example 3 Group Before use after use Before use after use One 0.108 0.130 0.109 0.110 2 0.094 0.119 0.105 0.107 3 0.092 0.120 0.100 0.109 4 0.102 0.128 0.091 0.102 5 0.094 0.121 0.092 0.104 6 0.095 0.124 0.102 0.103 7 0.088 0.127 0.101 0.106 8 0.105 0.122 0.095 0.102 9 0.100 0.121 0.099 0.104 10 0.095 0.156 0.100 0.109 Average 0.097 0.127 0.099 0.106

From the results of Table 4, the results of experiments on the tensile strength of hair (force required until the hair breaks), the group using the preparation example 3 containing the natural powder extract according to the present invention hair compared to the group using the comparative preparation example 1 It can be seen that the tensile strength of increased by about 20%.

In the present specification, only a few examples of various manufacturing and analysis experiments performed by the present inventors are described, but the technical idea of the present invention is not limited thereto, and may be variously modified and implemented by those skilled in the art. .

Claims (3)

delete As a cosmetic composition for hair, The pulverized product consisting of 30-40% by weight black sesame seed, 20-30% by weight kelp, 20-30% by weight cabbage and 15-20% by weight of soybean paste was fermented at 20-25 ° C. for 15-20 days, which was then 200 mesh. The filtrate filtered with filter cloth was aged for 25 days continuously at a constant temperature of 12 ° C., and the dried and spray dried natural powder extract was concentrated to 1% to 15% by weight of the composition until reduced to 45% of its original mass. It comprises%, cosmetic composition for hair. 3. The method of claim 2, The pulverized product further includes at least one natural material selected from garlic, round leek, wood starfish, parsley, 톳, gompi, brown rice, ocher and seaweed, wherein the natural material is 1 to 5 weight parts based on 100 parts by weight of the pulverized product. The cosmetic composition for hair, characterized in that it further comprises a part.