KR100771709B1 - 무수 포름산 생성에서의 소포제로서의 추출제의 이용 - Google Patents

무수 포름산 생성에서의 소포제로서의 추출제의 이용 Download PDF

Info

Publication number
KR100771709B1
KR100771709B1 KR1020027009418A KR20027009418A KR100771709B1 KR 100771709 B1 KR100771709 B1 KR 100771709B1 KR 1020027009418 A KR1020027009418 A KR 1020027009418A KR 20027009418 A KR20027009418 A KR 20027009418A KR 100771709 B1 KR100771709 B1 KR 100771709B1
Authority
KR
South Korea
Prior art keywords
extractant
distillation
formic acid
distillation apparatus
stream
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1020027009418A
Other languages
English (en)
Korean (ko)
Other versions
KR20020070350A (ko
Inventor
하인즈 아우어
베른트 베슬링
한스 함머
한스 하쎄
프리드리히 자우어
막시밀리안 비카리
게르하르트 바그너
틸 아드리안
Original Assignee
바스프 악티엔게젤샤프트
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 바스프 악티엔게젤샤프트 filed Critical 바스프 악티엔게젤샤프트
Publication of KR20020070350A publication Critical patent/KR20020070350A/ko
Application granted granted Critical
Publication of KR100771709B1 publication Critical patent/KR100771709B1/ko
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/09Preparation of carboxylic acids or their salts, halides or anhydrides from carboxylic acid esters or lactones
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
  • Medicinal Preparation (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
KR1020027009418A 2000-01-24 2001-01-24 무수 포름산 생성에서의 소포제로서의 추출제의 이용 Expired - Fee Related KR100771709B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10002793.8 2000-01-24
DE10002793A DE10002793A1 (de) 2000-01-24 2000-01-24 Verwendung eines Extraktionsmittels bei der Herstellung von wasserfreier Ameisensäure

Publications (2)

Publication Number Publication Date
KR20020070350A KR20020070350A (ko) 2002-09-05
KR100771709B1 true KR100771709B1 (ko) 2007-10-30

Family

ID=7628464

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020027009418A Expired - Fee Related KR100771709B1 (ko) 2000-01-24 2001-01-24 무수 포름산 생성에서의 소포제로서의 추출제의 이용

Country Status (12)

Country Link
US (1) US6838579B2 (enExample)
EP (1) EP1250307B1 (enExample)
JP (1) JP4746242B2 (enExample)
KR (1) KR100771709B1 (enExample)
CN (1) CN1271033C (enExample)
AT (1) ATE396167T1 (enExample)
AU (1) AU2001228487A1 (enExample)
BR (1) BR0107822B1 (enExample)
DE (2) DE10002793A1 (enExample)
MY (1) MY136296A (enExample)
NO (1) NO327829B1 (enExample)
WO (1) WO2001055071A1 (enExample)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR0215793B1 (pt) * 2002-06-26 2012-11-27 métodos para reduzir acúmulo de resìduos em unidade de lavagem usada em processo de craqueamento de hidrocarbonetos.
US7906012B2 (en) * 2002-07-16 2011-03-15 Dorf Ketal Chemicals India Pvt. Ltd. Method for reducing foam in a primary fractionator
DE102011075777A1 (de) * 2011-05-13 2012-11-15 Evonik Degussa Gmbh Verfahren zur Herstellung von Isophoron in Gegenwart mindestens eines Entschäumers in der Abwasserkolonne im Aufarbeitungsteil
CN109234530B (zh) * 2018-09-11 2023-12-08 福建紫金选矿药剂有限公司 一种高性能萃取稀释剂
CN115353450A (zh) * 2022-09-26 2022-11-18 河北康壮环保科技股份有限公司 一种稀甲酸浓缩的工艺

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0017866A1 (de) * 1979-04-11 1980-10-29 BASF Aktiengesellschaft Verfahren zur Gewinnung von wasserfreier oder weitgehend wasserfreier Ameisensäure
EP0156309A2 (de) * 1984-03-28 1985-10-02 BASF Aktiengesellschaft Verfahren zur Gewinnung von wasserfreier oder weitgehend wasserfreier Ameisensäure durch Hydrolyse von Methylformiat

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2545658C2 (de) * 1975-10-11 1985-12-19 Basf Ag, 6700 Ludwigshafen Verfahren zur Gewinnung von Carbonsäuren aus ihren wäßrigen Lösungen
DE3319651A1 (de) * 1983-05-31 1984-12-06 Basf Ag, 6700 Ludwigshafen Verfahren zur destillativen gewinnung von ameisensaeure

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0017866A1 (de) * 1979-04-11 1980-10-29 BASF Aktiengesellschaft Verfahren zur Gewinnung von wasserfreier oder weitgehend wasserfreier Ameisensäure
EP0156309A2 (de) * 1984-03-28 1985-10-02 BASF Aktiengesellschaft Verfahren zur Gewinnung von wasserfreier oder weitgehend wasserfreier Ameisensäure durch Hydrolyse von Methylformiat

Also Published As

Publication number Publication date
JP2003520834A (ja) 2003-07-08
MY136296A (en) 2008-09-30
KR20020070350A (ko) 2002-09-05
EP1250307B1 (de) 2008-05-21
CN1395553A (zh) 2003-02-05
DE10002793A1 (de) 2001-07-26
BR0107822A (pt) 2002-10-29
DE50113988D1 (de) 2008-07-03
NO327829B1 (no) 2009-10-05
NO20023513L (no) 2002-08-26
NO20023513D0 (no) 2002-07-23
ATE396167T1 (de) 2008-06-15
WO2001055071A1 (de) 2001-08-02
US6838579B2 (en) 2005-01-04
CN1271033C (zh) 2006-08-23
EP1250307A1 (de) 2002-10-23
US20030009057A1 (en) 2003-01-09
AU2001228487A1 (en) 2001-08-07
JP4746242B2 (ja) 2011-08-10
BR0107822B1 (pt) 2011-07-12

Similar Documents

Publication Publication Date Title
KR100772748B1 (ko) 무수 포름산을 생성시키는 방법
KR100772760B1 (ko) 무수 포름산의 생성 방법에서의 폐수 처리
US4349416A (en) Process and device for the separation of mixtures which form an azeotrope
US6713649B1 (en) Method for production of formic acid
US4076594A (en) Purification of formic acid by extractive distillation
FI84259C (fi) Foerfarande foer framstaellning av vattenfri eller naestan vattenfri myrsyra genom hydrolys av metylformiat.
KR100591625B1 (ko) 포름 알데히드 함유 혼합물의 처리
JP7449877B2 (ja) 軽質アクリレートを精製するための方法
KR100830758B1 (ko) 폐가스 흐름의 세정 방법
US5292917A (en) Process for purifying dimethyl carbonate
KR100771709B1 (ko) 무수 포름산 생성에서의 소포제로서의 추출제의 이용
WO2013030162A1 (en) Process of formic acid production by hydrolysis of methyl formate
JPH0832667B2 (ja) 炭酸ジメチルの精製法
JP4483156B2 (ja) ガンマブチロラクトンの精製方法
GB778966A (en) Recovery of hydrogen peroxide by fractional distillation of the products of the oxidation of alcohols
KR840000571B1 (ko) 정제 아세토니트릴의 회수방법
JPH10139720A (ja) メタクリル酸およびその誘導品の製造法

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
AMND Amendment
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

AMND Amendment
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E601 Decision to refuse application
PE0601 Decision on rejection of patent

St.27 status event code: N-2-6-B10-B15-exm-PE0601

AMND Amendment
J201 Request for trial against refusal decision
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PJ0201 Trial against decision of rejection

St.27 status event code: A-3-3-V10-V11-apl-PJ0201

PB0901 Examination by re-examination before a trial

St.27 status event code: A-6-3-E10-E12-rex-PB0901

B701 Decision to grant
PB0701 Decision of registration after re-examination before a trial

St.27 status event code: A-3-4-F10-F13-rex-PB0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

PN2301 Change of applicant

St.27 status event code: A-5-5-R10-R13-asn-PN2301

St.27 status event code: A-5-5-R10-R11-asn-PN2301

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

FPAY Annual fee payment

Payment date: 20121009

Year of fee payment: 6

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

FPAY Annual fee payment

Payment date: 20131002

Year of fee payment: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

FPAY Annual fee payment

Payment date: 20141002

Year of fee payment: 8

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8

FPAY Annual fee payment

Payment date: 20151020

Year of fee payment: 9

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 9

FPAY Annual fee payment

Payment date: 20161014

Year of fee payment: 10

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 10

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

LAPS Lapse due to unpaid annual fee
PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20171025

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20171025

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000