KR100636466B1 - 오르토-치환된 아릴금속 화합물을 제조하고 이 화합물을 친전자성 시약과 반응시키는 방법 - Google Patents

오르토-치환된 아릴금속 화합물을 제조하고 이 화합물을 친전자성 시약과 반응시키는 방법 Download PDF

Info

Publication number
KR100636466B1
KR100636466B1 KR1019990058665A KR19990058665A KR100636466B1 KR 100636466 B1 KR100636466 B1 KR 100636466B1 KR 1019990058665 A KR1019990058665 A KR 1019990058665A KR 19990058665 A KR19990058665 A KR 19990058665A KR 100636466 B1 KR100636466 B1 KR 100636466B1
Authority
KR
South Korea
Prior art keywords
formula
compounds
alkyl
group
carbon atoms
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1019990058665A
Other languages
English (en)
Korean (ko)
Other versions
KR20000062207A (ko
Inventor
스티아스니한스-크리스티안
라이펜래트볼커
Original Assignee
메르크 파텐트 게엠베하
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 메르크 파텐트 게엠베하 filed Critical 메르크 파텐트 게엠베하
Publication of KR20000062207A publication Critical patent/KR20000062207A/ko
Application granted granted Critical
Publication of KR100636466B1 publication Critical patent/KR100636466B1/ko
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F1/00—Compounds containing elements of Groups 1 or 11 of the Periodic Table
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F1/00—Compounds containing elements of Groups 1 or 11 of the Periodic Table
    • C07F1/02—Lithium compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1019990058665A 1998-12-19 1999-12-17 오르토-치환된 아릴금속 화합물을 제조하고 이 화합물을 친전자성 시약과 반응시키는 방법 Expired - Fee Related KR100636466B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19858855A DE19858855A1 (de) 1998-12-19 1998-12-19 Verfahren zur Herstellung von ortho-substituierten Arylmetallverbindungen und deren Umsetzung mit Elektrophilen
DE19858855.0 1998-12-19

Publications (2)

Publication Number Publication Date
KR20000062207A KR20000062207A (ko) 2000-10-25
KR100636466B1 true KR100636466B1 (ko) 2006-10-18

Family

ID=7891832

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019990058665A Expired - Fee Related KR100636466B1 (ko) 1998-12-19 1999-12-17 오르토-치환된 아릴금속 화합물을 제조하고 이 화합물을 친전자성 시약과 반응시키는 방법

Country Status (6)

Country Link
US (1) US6420584B1 (enExample)
EP (1) EP1010702B1 (enExample)
JP (1) JP4481407B2 (enExample)
KR (1) KR100636466B1 (enExample)
AT (1) ATE272064T1 (enExample)
DE (2) DE19858855A1 (enExample)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19858856A1 (de) * 1998-12-19 2000-06-21 Merck Patent Gmbh Verfahren zur Herstellung von Arylmetallverbindungen und deren Umsetzung mit Elektrophilen
DE10139664A1 (de) * 2001-08-11 2003-02-20 Clariant Gmbh Verfahren zur Herstellung von Aryl- und Alkyl-Bor-Verbindungen in Mikroreaktoren
DE10140857A1 (de) * 2001-08-21 2003-03-06 Clariant Gmbh Verfahren zur Herstellung von Aryl- und Alkyl-Bor-Verbindungen in Mikroreaktoren
DE10150610A1 (de) * 2001-10-12 2003-04-30 Clariant Gmbh Verfahren zur metallorganischen Herstellung organischer Zwischenprodukte über Amidbasen
GB0515926D0 (en) * 2005-08-03 2005-09-07 Merck Sharp & Dohme Chemical process
DE102005054090A1 (de) * 2005-11-12 2007-05-16 Bayer Technology Services Gmbh Verfahren zur kontinuierlichen Herstellung von Difluorbenzol-Derivaten mit hohen Standzeiten
JP5056118B2 (ja) * 2006-03-31 2012-10-24 Ｄｉｃ株式会社 ジフルオロベンゼン誘導体の製造方法
CN1966482B (zh) * 2006-11-20 2010-05-12 烟台万润精细化工股份有限公司 一类含环己基侧向邻二氟苯类液晶化合物的制备方法
JP5584444B2 (ja) * 2008-09-12 2014-09-03 Ａｇｃセイミケミカル株式会社 １，２−ジシクロヘキシルテトラフルオロエチレン骨格を有する化合物およびその製造方法
DE102019008481A1 (de) * 2018-12-21 2020-06-25 Merck Patent Gmbh Kontinuierliches Verfahren zur Funktionalisierung von fluorierten Benzolverbindungen im Strömungsrohr
CN111018892A (zh) * 2020-01-03 2020-04-17 烟台盛华液晶材料有限公司 一种芳烃氟邻位金属化的制备方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5087764A (en) 1988-03-10 1992-02-11 Merck Patent Gesellschaft mit beschrankter Hafung Process for the preparation of 2,3-difluorobenzenes
US5262556A (en) 1992-01-20 1993-11-16 Merck Patent Gesellschaft Mit Beschrankter Haftung Process for the reaction of halogenated aromatics with electrophiles

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1989002425A1 (en) 1987-09-09 1989-03-23 MERCK Patent Gesellschaft mit beschränkter Haftung Fluorinated oligophenyls and their use in liquid crystal materials
US5162577A (en) * 1990-02-13 1992-11-10 Hoffmann-La Roche Inc. Process for lithiation of 1,3-bis(trifluoromethyl)benzene
DE4219281C1 (de) * 1992-06-12 1993-12-23 Merck Patent Gmbh Verfahren zur Herstellung von substituiertem Trifluormethoxybenzol
US5626798A (en) * 1996-01-05 1997-05-06 Fmc Corporation Aryllithium products and processes
US5663398A (en) * 1996-05-17 1997-09-02 Fmc Corporation Processes for preparing functionalized alkyllithium compounds
DE19725192C1 (de) * 1997-06-14 1999-01-28 Metallgesellschaft Ag Verfahren zur Herstellung von Organoalkalimetallverbindungen
DE19858856A1 (de) * 1998-12-19 2000-06-21 Merck Patent Gmbh Verfahren zur Herstellung von Arylmetallverbindungen und deren Umsetzung mit Elektrophilen
TWI287547B (en) * 2000-06-14 2007-10-01 Dow Agrosciences Llc Process for the selective deprotonation and functionalization of 3-substituted benzotrifluorides

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5087764A (en) 1988-03-10 1992-02-11 Merck Patent Gesellschaft mit beschrankter Hafung Process for the preparation of 2,3-difluorobenzenes
US5262556A (en) 1992-01-20 1993-11-16 Merck Patent Gesellschaft Mit Beschrankter Haftung Process for the reaction of halogenated aromatics with electrophiles

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
J. Org. Chem. 1988, 53, 1367-1371 *
J. Org. Chem. 1994, 59, 2616-2619

Also Published As

Publication number Publication date
EP1010702A2 (de) 2000-06-21
DE19858855A1 (de) 2000-06-21
EP1010702A3 (de) 2002-04-10
ATE272064T1 (de) 2004-08-15
US6420584B1 (en) 2002-07-16
JP4481407B2 (ja) 2010-06-16
DE59910061D1 (de) 2004-09-02
JP2000239282A (ja) 2000-09-05
EP1010702B1 (de) 2004-07-28
KR20000062207A (ko) 2000-10-25

Similar Documents

Publication Publication Date Title
KR100594811B1 (ko) 아릴금속 화합물을 제조하고 제조된 화합물을 친전자성 시약과 반응시키는 방법
KR100636466B1 (ko) 오르토-치환된 아릴금속 화합물을 제조하고 이 화합물을 친전자성 시약과 반응시키는 방법
US5087764A (en) Process for the preparation of 2,3-difluorobenzenes
JP2007314546A (ja) 五フッ化硫黄化合物とその製法および利用
US5262556A (en) Process for the reaction of halogenated aromatics with electrophiles
US5493032A (en) Process for the preparation of substituted difluorobenzo-1,3-dioxoles
US5194628A (en) Process for the preparation of substituted difluorobenzo-1,3-dioxoles
CA1338936C (en) Process for the preparation of substituted difluorobenzo-1,3-dioxoles
EP1660463B1 (en) A process for the preparation of phenyltetrazole derivatives
Brauer et al. The effect of trifluoromethyl substitution on the B N bond in trifluoromethyl-dimethylaminoboranes, CF3 (R) BNMe2: crystal and molecular structure of CF3 (Et)(NCCH2) B· NHMe2
Choi et al. A novel α, ω silyl dianionic salt. The synthesis and characterization of remotely connected benzannulated silole monoanions
DE4234585C1 (de) Fluorierte Trifluormethoxybenzole
DE4219281C1 (de) Verfahren zur Herstellung von substituiertem Trifluormethoxybenzol
TWI833451B (zh) 異噁唑衍生物的製備方法及其中間體
JPH02202863A (ja) ２―フルオロベンゾニトリルの誘導体の製造方法
Beckmann et al. A supramolecular hydrogen‐bonded complex between 1, 3, 5‐tris (diisobutylhydroxysilyl) benzene and trans‐bis (4‐pyridyl) ethylene
US20220251115A1 (en) Methods for preparing catlayst precursor materials
JP2004525894A (ja) ビス（アルキルチオ）カルベニウム塩
JPH0692339B2 (ja) オルトー脂肪族オキシフェノール誘導体の製造方法
Yagupolskii et al. Trifluoromethylsulfonylmethanides functionalized by a CN group
Brauer et al. Fluorine effects in organoboranes; formation of cyanoalkyl-bis (trifluoromethyl)-organoborates
Uemura et al. Regioselectivity of nucleophilic additions to (arene) chromium complexes: conformational effects of Cr (CO) 3 moieties and the nature of carbanions
JPH0269486A (ja) ハロシランの製造方法
JP2020079225A (ja) 芳香族チオノカルボン酸エステルの製造方法

Legal Events

Date Code Title Description
PA0109 Patent application

St.27 status event code: A-0-1-A10-A12-nap-PA0109

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

D13-X000 Search requested

St.27 status event code: A-1-2-D10-D13-srh-X000

D14-X000 Search report completed

St.27 status event code: A-1-2-D10-D14-srh-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U11-oth-PR1002

Fee payment year number: 1

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

FPAY Annual fee payment

Payment date: 20120919

Year of fee payment: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

FPAY Annual fee payment

Payment date: 20130924

Year of fee payment: 8

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8

FPAY Annual fee payment

Payment date: 20140923

Year of fee payment: 9

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 9

FPAY Annual fee payment

Payment date: 20150917

Year of fee payment: 10

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 10

FPAY Annual fee payment

Payment date: 20160921

Year of fee payment: 11

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 11

FPAY Annual fee payment

Payment date: 20170920

Year of fee payment: 12

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 12

FPAY Annual fee payment

Payment date: 20181004

Year of fee payment: 13

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 13

PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20191013

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20191013

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000