KR100613589B1 - Jellied for a pack - Google Patents

Abstract

The present invention relates to a method for manufacturing a nonwoven fabric pack using kappa-carrageenan and locust bean gum, and more particularly, to a nonwoven surface, a gel-forming water consisting of kappa-carrageenan and locust bean gum mixed with a moisturizing agent and a nutrient preservative. The present invention relates to a method for producing a nonwoven fabric pack using kappa-carrageenan and locust bean gum, which cut off the swollen gel and give a cosmetic effect on the face and the like.

To this end, a gelling agent dissolution process in which a mixture of kappa-carrageenan and locust bean gum is added to water and heated to dissolve so that the resulting sol has a uniform composition, and the stomaching agent is cooled to a certain temperature, followed by a moisturizing agent, a nutrient surfactant, a whitening agent, Packed material mixing process to add antioxidants, preservatives, fragrances, pigments, etc., gelling aid to mix additives involved in gel formation such as sodium hexametaphosphate, delta lactone gluconate, calcium sulfate, calcium lactate, calcium gluconate Process and gelation process Gel-forming process to pour gelling agent into flat cotton or non-woven fabric, gel cutting process, mask cutting process to cut hole and nose in the form of mask, polyethylene derephthalate coated aluminum foil and polyethylene It is a packaging process that puts in a bag of material and packs materials such as moisturizers and nutrients into the gel. By adding more active ingredients while eliminating the flaw that flows, the effect is to double the sorry effect.

Gelling agent, kappa-carrageenan, locust bean gum, pack, mask

Description

Manufacturing method of nonwoven pack using kappa-carrageenan and locust bean gum {Jellied for a pack}

The present invention relates to a method for producing a nonwoven tabular pack using kappa-carrageenan and locust bean gum. More specifically, a nonwoven fabric is obtained by mixing a gelling agent consisting of kappa-carrageenan and locust bean gum with a moisturizer, a nutrient preservative, and the like. It is to provide a method for producing a nonwoven fabric pack using kappa-carrageenan and locust bean gum that is poured into a mold laid with a gel and cut and gelled to give a facial effect.

In addition to the general method of putting a thin plate of vegetables or fruits on the face, the pack is a peel off type to remove the film formed on the skin after application, and a wash off type to be washed with water after drying, such as clay. There are non-woven fabrics that use non-woven fabrics soaked with cosmetics on the face, but the method of blowing thin slices of vegetables and fruits is not easy to crush, and they are flawed when they move. Peel-off and wash-off types can be removed or washed after drying. Inconvenient, the non-woven fabric that penetrates the essence or lotion in the cloth has a limit of the amount of cosmetic material absorbed in the cloth, so there is a inconvenience to flow down if you absorb a large amount.

Long-lasting gelling agents include gelatin, agar, sodium alginate, and carrageenan. Gelatin is a product of collagen, a light protein that is widely distributed in the animal world, and it is produced by thermal degeneration. Alginic acid has been used in many ways because it is a millennial from brown algae.

However, gelatin and agar do not react with calcium salts and form gels only by cooling, but are not suitable for the manufacture of packs of non-woven type because they change to a road sol state when the temperature rises.

In addition, sodium alginate and cappa-carrageenan and iota-carrageenan combine with calcium ions to form insoluble gels when metal salts such as calcium are added, but they are brittle due to their elongation and lack flexibility. If it is placed in a severe bend, it will not be cut or excited and will not adhere to the skin. Therefore, the cosmetic effect cannot be obtained. The gel produced using only gelling agents such as sodium alginate and cappa-carrageenan is unstable. (渗出) phenomenon occurs.

In general, carrageenan is widely used in processed foods such as gel food, fish cake, meat and chicken meat because of its high gel-forming ability and excellent reactivity with protein, and various patents are also applied to give gel properties suitable for use.
Japanese Patent No. 120154 (Application No. 880066241 880321, Kato et al.) Prepared a gel having excellent moisture and flavor divergence by adding potassium alginate to carrageenan.
In US Pat. No. 3,658,556 (Klein et al.), Potassium and calcium ions were added to the gelling agent of kappa and iota-carrageenan and locust bean gum to obtain even dispersion of the pulp. Two or more kinds of cations or alkylammonium were used in carrageenan or mixture of carrageenan to reduce the melting point of the gel, thus preparing a gel having excellent texture and flavor divergence.
U.S. Patent No. 4,307,124 (Moilano) prepared a composition having a fibrous texture using kappa-carrageenan, locust bean gum and potassium tartrate.
When carrageenan and locust bean gum are used as gelling agents, gels produced by gelation, softness, texture, flavor divergence, etc. are remarkably different depending on the type of carrageenan, the type and concentration of cation added, and the type and amount of buffer. Change.
In general, gels are formed as soon as metal ions are added to gelling agents such as carrageenan and locust bean gum. Sodium hyaluronate is used in addition to sodium acetate or sodium citrate as a buffer to control the reaction rate. It dissociates into ions and sodium ions in the organic phase and changes them into insoluble calcium compounds, temporarily blocking the reaction with the gelling agent, and increasing the ion concentration of the organic acid as a soluble compound over time. As it changes, it reacts with the gelling agent to produce a gel.

In the present invention, when the calcium ion is added to the kappa-carrageenan to improve the defects of the prior art as described above, the defects that are broken by bending and bending when placed on a severely curved face due to the elongation (弛 張) When placed on the face due to lack of flexibility, there is a gap between the face and the pack, so that the beauty material is not absorbed evenly on the face, and if left for a long time, the gel strength increases and moisture containing the beauty material is separated from the gel. Lowers the effect.
In order to eliminate these defects, the gel formation time is controlled by varying the amount of gelling aid added to produce gels with moderate gel strength, excellent flexibility, toughness, and safety. An object of the present invention is to provide a method for producing a nonwoven pack using locust bean gum.

The present invention provides a gel strength, flexibility and toughness suitable as a pack material by controlling the gel formation time affecting gel properties by adding a gelling agent to the gelling agent of kappa-carrageenan and locust bean gum. A gel with a back is formed and attached to the entire face without any gap when placed on the face so that the beauty material is uniformly absorbed.
To this end, the present invention is a gelling agent dissolution step of heating and dissolving a gelling agent composition of kappa-carrageenan and locust bean gum, and after cooling the gelling agent to a certain temperature, moisturizers, nutrients, activators, whitening agents, antioxidants, preservatives A gelling aid addition step of mixing a pack material mixing step of adding a scent, a fragrance, a pigment, and the like and additives involved in gel formation such as hexameta phosphate, delta lactone gluconate, calcium sulfate, calcium lactate, and calcium gluconate, Gel forming process that gels the gelling agent onto a flat or non-woven surface and gels it, a mask cutting process that cuts out holes and cuts into the shape of a mask, and vacuums them in a bag made of aluminum foil and polyethylene coated with polyethylene derephthalate. It consists of a packaging process for packaging.

Referring to the nonwoven fabric pack using kappa-carrageenan and locust bean gum of the present invention according to the manufacturing process as follows. The weight percentages below are relative to the total weight of the gelling agent.

Gel agent dissolution process

The gel agent is dissolved by heating a mixture of 0.2-0.8% kappa-carrageenan and 0.3-0.7% locust bean gum by heating 60% -85% of water to dissolve it, and then converting the sol into a normal colloid mill (wing circumferential speed). 3000 rpm) to obtain a homogeneous solution and then heated to 85 ° C.

Pack material mixing process

The uniformly dispersed sol is cooled to 65 ° C. and then placed in a sealed container with a stirrer (rotational speed 60 rpm) and mixed by adding a moisturizer, a nutrient surfactant, a whitening agent, an antioxidant, a preservative, a fragrance, and a pigment.

Moisturizers include Propylene glycol, Sorbitol, Dipropylene glycol, Butylene glycol, Sodium hyaluronate, POE methyl glucoside, Glycerine Emulsions include Squalane, Liquid paraffin, Olive oil, Castor oil, Stearic acid, Cetyl alcohol, etc. Active agents include POE (12) nonyl phenyl ether, POB (12) nonyl phenyl ether, Polysorbate 60, Potassium stearate, and other active ingredients and nutrients such as Allantoin, In addition to DL-Panthenol, and methyl parabene as a preservative, Propyl parabene, and other fragrance PH regulators, various cosmetic ingredients are added.

Gelation aid addition process

Gel modifiers include gel formers, gel inhibitors, and disintegrating agents. The gel modifiers of kappa-carrageenan and locust bean gum are insoluble in combination with calcium ions such as calcium lactate, calcium gluconate, and calcium sulfate. To delay this reaction, the gel is formed as a gelling inhibitor. Sodium salts of organic acids such as sodium citrate and sodium acetate or condensed phosphates such as sodium polyphosphate and hexameta phosphate are used. Blocks the calcium ions in the salt and turns them into insoluble calcium compounds to inhibit the reaction with the gelling agent.

In the above reaction, the amount of condensed phosphate varies depending on the amount of condensed phosphate, but the gelling agent does not form gel after several hours or several tens of hours. Add gluconate.

Gelling inhibitor

Gelling inhibitors contain colloidal precipitates by blocking calcium ions in solution to form a colloidal precipitate, and calcium ions block the reaction with the gelling agent. Sodium phosphate, polyphosphate, condensed phosphate, etc. However, in the present invention, 0.16% to 0.24% hexa metaphosphate is added.

The addition amount of the gelling inhibitor is related to the gel formation time and the gel strength. If the addition amount is large, the gel formation time is long. At this time, the gel strength is weakened, but a gel rich in flexibility and toughness is formed.

Disintegrant

As the decomposing agent, delta lactone gluconate is used as an additive which decomposes colloidal precipitate of calcium produced by the action of condensed phosphate and calcium ion into soluble salts. It decomposes in solution to form gluconic acid, which dissolves colloidal precipitates of calcium into soluble salts, which react with the gelling agent to form an insoluble gel. Delta lactone gluconate is added at 0.5% to 0.18%.

The amount of disintegrating agent does not affect the characteristics of the resulting gel, but when excessively added, an unstable gel is produced in which the bound water is exuded.

Gel former

The gel former is a soluble calcium salt which reacts with the gelling agent to form a gel. There are additives such as calcium lactate, calcium gluconate, calcium sulfate, but in the present invention, 0.10% to 0.9% of calcium sulfate is added. If the amount of the gel-forming agent is added, the gelation time is shortened and a brittle gel is formed due to the high strength of the gel.

The above additive, which is directly or indirectly involved in gelation, is added with stirring at a time difference according to the above procedure, and after dissolution is completed, bubbles generated in the sol during stirring are removed.

The gelling agent in the aqueous medium forms a gel because it has a high cohesive wave network, and the strength of the gel formed by the above treatment can be arbitrarily controlled. By adjusting the amount, it can be controlled up to 20 hours in a few minutes.

Gel molding process

The nonwoven fabric is laid on a frame surrounded by four sides, and a gelling agent mixed with a pack material and a gel-forming additive is injected and cooled.

Mask cutting process

When gelation is completed after injection, it is cut in the form of a mask with a cutter and completed by cutting holes in the eye and nose area with a cutter.

Packing process

The cut nonwoven fabric pack is shipped in a bag made of polyethylene derephthalate coated with aluminum foil and polyethylene and vacuum-packed.

An embodiment of the present invention will be described in detail as follows.

Example 1

This embodiment relates to a pack of a nonwoven fabric using kappa-carrageenan and locust bean gum to which Witch hazel extract with a convergence effect, prepared by the following formulation ratio, and a method of manufacturing the same:

Add 400 gr of kappa-carrageenan and 2.5 gr of locust bean gum to 400 g of water, and then heat-dissolve the colloidal solution with ethanol 73 gr, glycerin 5 gr, butylene glycol 2.2 gr, and phenyl siloxane 1.0. gr, Witch hazel extract 5.5gr, POE (60) hydrogenated castor oil 1.0gr, Perfume 1.0gr, preservative, methyl paraben 0.5gr, preservative, propylparaben (Propyl paraben) 0.05gr, nutrient DL-Panthenol 0.8gr, active ingredient Allantoin 0.25gr, etc. are added and mixed uniformly, sodium hexametaphosphate 1.2gr, delteractone gluconate 2.0 gr and calcium sulfate 1.0gr are added and stirred in order, and then nonwoven fabric is injected into a flat mold, gelled, and cut into a mask form. The above prescription is a non-woven pack containing a cosmetic solution that emphasizes convergence, and the gel containing cosmetic materials does not crumble due to the relativity and has excellent flexibility so that it does not break when attached to the face without any breaks. It is absorbed uniformly on the face to produce a pack with increased cosmetic effect. This pack contains moisturizing glycerin, butylene glycol, etc., and phenyl siloxane, which is a softening agent, to moisturize and soften the stratum corneum, which facilitates the next step of makeup, and also formulates witch hazel extract to supply moisture to the stratum corneum and sweat It is suitable for oily skin or acne skin because it gives a convergence effect that suppresses secretion rate and increases ethanol content (14.6%) to disinfect skin and remove oil.

Example 2

This embodiment is a kappa-added with Phenyl siloxane which gives flexibility and moisturizing effect and POE (60) hydrogenated castor oil (POE (60) hydrogenated castor oil) which disperse it produced by the following mixing ratio. A nonwoven fabric pack using carrageenan and locust bean gum, and a method for producing the same.

34g ethanol 34g, 15g glycerin, 15gr butylene glycol 15gr, 2.4gr phenyl siloxane, POE 60) Hydrogenated castor oil (POE (60) hydrogenated castor oil) 1.7gr, Perfume 1.5gr, Preservative, Methyl paraben 0.5gr, Preservative, Propyl paraben 0.1gr After mixing, add 1.1 g of sodium hexametaphosphate, 1.0 gr of delteractone gluconate, and 1.2 gr of calcium sulfate in order to stir, inject a flat surface or non-woven fabric into a flat mold, and then gel it into a mask.

This gel has no crumbs due to the stiffness and has excellent properties such as flexibility and toughness when it is placed on a severely curved face, and it adheres to the face without space. Therefore, the gel contains moisturizers such as glycerin and butylene glycol, Easily penetrates phenyl siloxane, which is highly effective in moisturizing, to soften the stratum corneum and give the face a smooth touch to facilitate the next step of makeup.
In addition, the content of ethanol (6.8%) is reduced from that of Example 1, but it can be applied to sensitive skin because it has the action of disinfecting skin and removing oil.

Example 3

This embodiment relates to a pack of a nonwoven fabric using kappa-carrageenan and locust bean gum to which citric acid, which has a weakly acidic effect produced by the following formulation ratio, is added, and a manufacturing method thereof.

Ethanol 43gr, Glycerine 7.0gr, Propylene glycol 17gr, POE (20) Cetyl Oreate (Pole (20)) in a colloidal solution obtained by heating and dissolving 3.2 gr of kappa-carrageenan and 2.8 gr of locust bean gum in 420 gr of water. POE (20) cetyl oleate 1.1gr, Perfume 1.0gr, Preservative, Methyl paraben 0.45gr, Preservative, Propyl paraben 0.05gr, Citric acid 0.05gr, Nutritional supplement, DL Add 1.0 g of DL-Panthenol, activator, 0.25 g of Allantoin, etc., and then uniformly mix, add 1.0 gr of hexamethaphosphate, 1.0 gr of delteractone gluconate, and 1.1 gr of calcium sulfate. After stirring, the nonwoven fabric is injected into a flat mold, gelled, and cut into a mask. Gel containing cosmetic ingredients as described above does not crumble due to the relativity and has excellent flexibility, so it does not break when applied to the face and adheres to the face without gaps, so that the cosmetic ingredients are absorbed evenly on the face. It is a nonwoven pack that increases its effectiveness This pack contains moisturizing glycerin and propylene glycol to moisturize and soften the stratum corneum to facilitate the next step of makeup, and also mix citric acid to neutral or mildly alkaline the skin surface due to the alkalinity of the face wash. Restores mild acid to smooth out unbalanced skin and softens skin. In addition, the content of ethanol (8.6%) is reduced than that of Example 1, but it can be applied to sensitive skin because it has an action of disinfecting skin and removing oil.

As described above, the gel containing the cosmetic material in the nonwoven pack using the kappa-carrageenan, locust bean gum and soluble calcium salt of the present invention has no crumbs due to the stretching property and has excellent flexibility when applied to the face. It is very high in utility because it increases the beauty effect by being in close contact without bending.

It has gel properties suitable for manufacturing a pack free of defects due to the deterioration of the alginic acid gel and the breakage of the gel due to bending.

In addition, in the conventional nonwoven pack, the amount of moisturizer or nutrient absorbed by a single nonwoven fabric is limited, and the gel containing the beauty material does not crumble due to the elasticity and has excellent flexibility so that it does not break when applied to the face. Cohesion increases the cosmetic effect.

Conventional gel-free, nonwoven cloth packs have drawbacks when excessively absorbing active ingredients, and the amount of cosmetic material absorbed by a single nonwoven fabric is limited, but the kappa-carrageenan and locust of the present invention are limited. Since the pack of the nonwoven fabric using the bean gum is determined by the thickness of the gel, the content of an active ingredient such as a humectant or a nutrient can be controlled by controlling the thickness of the gel.

In addition, the moisturizers and nutrients contained in the gel are held in a stable state in the gel, but when contacted with an absorbent article, the water containing the active ingredient in the gel is easily exuded, thus forming the gel. Packs using water have good gel properties and very high utility.

Claims (1)

0.2 to 0.8 wt% of kappa-carrageenan and 0.3 to 0.7 wt% of kappa-carrageenan as a gelling agent when preparing non-woven packs by mixing cosmetic materials such as moisturizers and nutrients in a gelatin solution obtained by heating and dissolving a mixture of kappa-carrageenan and locust bean gum. Using a colloidal solution and adding a gel of 0.16 to 0.24% by weight of hexa meta phosphate, 0.18 to 0.5% of delta lactone gluconate and 0.10 to 0.90% by weight of calcium compound after the gelation of the gelling agent was completed. Method for producing a pack using kappa-carrageenan and locust bean gum