KR100361904B1 - Method for manufacturing cleaning material of drinking water - Google Patents

Method for manufacturing cleaning material of drinking water Download PDF

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KR100361904B1
KR100361904B1 KR1019990036755A KR19990036755A KR100361904B1 KR 100361904 B1 KR100361904 B1 KR 100361904B1 KR 1019990036755 A KR1019990036755 A KR 1019990036755A KR 19990036755 A KR19990036755 A KR 19990036755A KR 100361904 B1 KR100361904 B1 KR 100361904B1
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water
zeolite
mesh
gemstone
elvan
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KR1019990036755A
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KR20010020066A (en
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이영환
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이영환
성인식
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/32Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016Particle form
    • B01J20/28019Spherical, ellipsoidal or cylindrical
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/3021Milling, crushing or grinding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/3078Thermal treatment, e.g. calcining or pyrolizing

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  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Physical Water Treatments (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Water Treatment By Sorption (AREA)

Abstract

본 발명은 음료수 정수제의 제조방법에 관한 것으로, 통상 원적외선을 방사하는 세라믹, 맥반석, 제올라이트, 옥석, 견운모는 325메쉬로, 황토는 200∼325메쉬, 참숫은 150∼200메쉬로 분쇄하는 분쇄단계와, 분쇄된 각 소재를 선별한 후 1000℃ 정도로 소성하여 급냉하는 건조단계와, 분쇄된 황토, 맥반석, 제올라이트, 옥석, 견운모 등에 함유된 철분을 고강의 자석으로 제거하는 이물제거단계와, 황토 20%, 맥반석 30%, 제올라이트 15%, 옥석 15%, 견운모 15%, 참숫 5% 등의 비율로 혼합하되, 상기 각 소재들의 접착성을 위하여 60% 설탕 수용액을 첨가하여 회전하는 원통에 넣어 10∼20mm 크기의 구체로 제조한 후 자연건조하며, 구체의 표면에 5% 키토산 수용액을 분무하여 코팅하는 소성단계로 이루어지는 것을 특징으로 한다.The present invention relates to a method for producing a beverage purifier, ceramic, elvan, zeolite, gemstone, mica, which emits far-infrared rays, pulverized to 325 mesh, loess to 200 to 325 mesh, and true water to 150 to 200 mesh. And, after crushing each material pulverized and dried to about 1000 ℃ quenching and drying step, foreign matter removal step of removing iron contained in the crushed ocher, ganban stone, zeolite, gemstone, mica, etc. with a high strength magnet, and ocher 20 %, Elvan 30%, zeolite 15%, jadeite 15%, biotite 15%, true 5%, etc., each of the materials for the adhesion of 60% sugar solution is added to the rotating cylinder 10 ~ It is made of a sphere of 20mm size and then dried naturally, characterized in that the firing step of coating by spraying 5% chitosan aqueous solution on the surface of the sphere.

Description

음료수 정수제의 제조방법{Method for manufacturing cleaning material of drinking water}Method for manufacturing cleaning material of drinking water

본 발명은 사람이 살아가는데 없어서는 아니되는 물을 산성에서 알칼리성으로 변화시킴과 아울러 우리 입맛에 맞는 물 또는 지장수를 만들기 위한 음료수 정수제의 제조방법에 관한 것이다.The present invention relates to a method for preparing a beverage purifier for changing water from acidic to alkaline, which is essential for human life, and for making water or jijangsu suitable for our taste.

최근 인간의 편의성 때문에 만들어진 화학제품들이 늘어남에 따라 공해가 증가되며, 최근 증가되는 다이옥신 및 농약등 각기 화학약품의 성분들이 땅속으로 스며들어 감에 따라 국토의 수질을 오염시키게 된다.Pollution increases as the number of chemical products made due to the convenience of humans increases recently, and as the constituents of each chemical, such as dioxins and pesticides, penetrate into the ground, they pollute the water quality of the land.

종래의 기술은 옛부터 전해온 용기(흙.황토)를 사용하여 제작된 것들과 맥반석을 10mm 크기로 분쇄하여 용기에 담궈두는 방식과, 생황토를 물에 풀어 침전후 지장수로 만드는 방식을 써왔으며 옛 선인들은 용기그릇을 1350℃로 소성하여 토기그릇으로 사용한 바 있으나 원적외선 효과 및 수질정화 효과는 기대할 수 없으며, 협소한 공간에 많은 부피를 차지하는 등의 불편함이 수반되었다.Conventional technologies have been used to cultivate those made using containers (soil, ocher), which have been transmitted since ancient times, and to crush elbows in 10 mm size and to immerse them in containers, and to dissolve the raw ocher in water and settle it into Jizo water. The predecessors fired the vessel bowl at 1350 ℃ and used it as an earthenware vessel, but the far-infrared effect and the water purification effect could not be expected, and it was accompanied by inconvenience such as occupying a large volume in a narrow space.

수질 또한 여러 항목에 대한 검사 결과 기준치에 못 미치는 현상을 보이며 미관상 및 사용에 불편함이 있었다.The quality of water also showed a phenomenon that it failed to meet the standard value, and it was unsatisfactory in appearance and use.

본 발명은 이러한 문제점을 해결하기 위한 것으로, 산성의 물을 알칼리성으로 전환시킬 수 있도록 함으로써 상당량의 수분을 섭취하지 않고는 살 수 없는 인체에 오염되지 않은 맑은 물을 공급할 수 있도록 한 음료수 정수제의 제조방법을 제공하는데 그 목적이 있다.상기 목적을 달성하기 위한 본 발명은, 세라믹, 맥반석, 제올라이트, 옥석, 견운모는 325메쉬로, 황토는 200∼325메쉬, 참숫은 150∼200메쉬로 분쇄하는 분쇄단계와, 분쇄된 각 소재를 선별한 후 1000℃ 정도로 소성하여 급냉하는 건조단계와, 분쇄된 황토, 맥반석, 제올라이트, 옥석, 견운모 등에 함유된 철분을 고강의 자석으로 제거하는 이물제거단계와, 황토 20%, 맥반석 30%, 제올라이트 15%, 옥석 15%, 견운모 15%, 참숫 5% 등의 비율로 혼합하되, 상기 각 소재들의 접착성을 위하여 60% 설탕 수용액을 첨가하여 회전하는 원통에 넣어 10∼20mm 크기의 구체로 제조한 후 자연건조하며, 구체의 표면에 5% 키토산 수용액을 분무하여 코팅하는 소성단계로 이루어지는 것을 특징으로 한다.The present invention has been made to solve this problem, by making the conversion of acidic water to alkaline to prepare a drinking water purifier that can supply clean water uncontaminated to the human body can not live without a significant amount of water In order to achieve the above object, the present invention provides a ceramic, elvan, zeolite, gemstone, and mica in 325 mesh, loess in 200-325 mesh, and true water in 150-200 mesh. And a step of drying each of the pulverized materials by sintering and quenching by quenching at about 1000 ° C., and removing foreign substances by removing the iron contained in the crushed ocher, elvan, zeolite, gemstone, and mica with a high-strength magnet. 20%, elvan 30%, zeolite 15%, jadeite 15%, biotite 15%, 5% of true water, etc., but 60% sugar aqueous solution for the adhesion of each material It is added to the rotating cylinder to make a sphere of 10 ~ 20mm size and then dried naturally, characterized in that the firing step of coating by spraying 5% chitosan aqueous solution on the surface of the sphere.

이하, 본 발명에 의한 음료수 정수제의 제조방법을 상세히 설명하면 다음과 같다.본 발명에 의한 정수제의 제조방법은 분쇄단계와, 건조단계와, 재분쇄단계, 이물제거단계와, 소성단계 및 키토산 분무단계로 이루어진다.상기 분쇄단계에서는 통상 원적외선을 방사하는 세라믹, 맥반석, 제올라이트, 옥석, 견운모를 5∼10mm 크기로 분쇄한다.상기 건조단계에서는 분쇄된 각 소재를 선별한 후 1000℃로 소성하여 냉수로 급냉한다.상기 재분쇄단계에서는 분쇄된 원적외선 방사물질을 325메쉬로 잘게 분쇄하고, 황토는 생황토를 유지하기 위하여 200℃로 건조한 후 200∼325메쉬로 분쇄하며, 별도로 150∼200메쉬로 분쇄된 참숫을 준비한다.상기 이물제거단계에서는 분쇄된 황토, 맥반석, 제올라이트, 옥석, 견운모 등에 함유된 철분을 고강의 전자 자석으로 제거한다.상기 소성단계에서는 황토 20%, 맥반석 30%, 제올라이트 15%, 옥석 15%, 견운모 15%, 참숫 5% 등의 비율로 혼합하되, 상기 각 소재들의 접착성을 위하여 60% 설탕 수용액을 첨가하여 회전하는 원통에 넣어 10∼20mm 크기의 구체로 제조한 후 자연건조한다.이와 같이 소성된 구체의 표면에 5% 키토산 수용액을 분무하여 코팅한 후 플라스틱 용기 또는 부직포로 포장함으로써 정수제의 제조가 완료된다.실험예)본 발명의 물질을 통상 먹는 물에 담구어서 약 1~3시간이 경과한 후 수질검사를 하였다. 그 결과, pH7.2에서 8.5로 변하며 12시간 경과 후에는 최대 8.9까지 상승하였다. 알칼리수 시약은 B.T.B로 하였으며 색상은 청색으로 변하였다(산성은 노란색으로 변함). 칼슘, 마그네슘 시약은 E.T.B.로 하였으며 색상은 분홍색으로 변하였다(칼슘, 마그네슘이 없는 물은 청색으로 변함). 본 발명의 물질을 넣었더니 12시간 경과 후 미네랄 물로 변하였다.상술한 바와 같이 제조된 정수제는 여러 시약 및 실험결과 92%의 다이옥신을 제거하는 효과 및 산성의 물을 알칼리성으로 전환시키는 효과를 가지는 바, 물맛을 좋게 하고 대장균을 살균하여 오감테스트의 결과 좋은 효능이 입증되었으며, 갈수록 토질이 화학약품과 대기오염 등으로 산성화되어 땅속의 수질까지도 오염됨과 동시에 날로 악화되고 있는 실정에 따라 우리나라 뿐만 아니라 전세계적으로 심각한 식수 대란 등이 초래할 소지를 미연에 방지할 수 있게 되고, 또한 점차 산성화되어 가는 식수를 알칼리성 및 지장수로 개질시킬 수 있게 됨으로써 노화방지 및 위막을 보호하고 장을 건강하게 하는데 큰 효과를 기대할 수 있게 된다.또한, 아파트 및 공동주택에 설치된 수조탱크에 저장된 물을 각 가정으로 공급하는 과정에서, 상기 수조탱크에 본 발명의 정수제를 투입하면 산성화된 물을 알칼리수로 전화시킴으로써 수조탱크에 연결된 철제파이프의 부식을 방지할 수 있게 된다.Hereinafter, a method for preparing a beverage of water purifying agent according to the present invention will be described in detail. The method for preparing a water purifying agent according to the present invention includes a grinding step, a drying step, a regrinding step, a foreign material removing step, a firing step and Chitosan spraying step. In the crushing step, the ceramic, ganban stone, zeolite, gemstone, and mica that emit far-infrared rays are usually pulverized to 5 to 10 mm. In the drying step, each pulverized material is sorted and then fired at 1000 ° C. In the regrinding step, the pulverized far-infrared radioactive material is finely pulverized to 325 mesh, and the ocher is dried to 200 ° C. and then pulverized to 200 to 325 mesh to maintain fresh ocher, and separately to 150 to 200 mesh. In the foreign material removing step, the iron contained in the crushed ocher, elvan, zeolite, gemstone, mica and the like is removed by a high-strength electronic magnet. In the firing step, the mixture is mixed in the ratio of 20% ocher, 30% elvan, 15% zeolite, 15% gemstone, 15% villus, 5% true, etc. It is put into a rotating cylinder and made into a sphere of 10 to 20 mm in size, followed by air drying. The surface of the calcined sphere is sprayed with 5% aqueous chitosan solution and coated in a plastic container or a nonwoven fabric to complete the preparation of the water purifying agent. Experimental Example) The substance of the present invention was immersed in normal drinking water, and after about 1 to 3 hours, water quality examination was performed. As a result, the pH was changed to 8.5 at pH 7.2 and rose to a maximum of 8.9 after 12 hours. The alkaline water reagent was B.T.B and the color turned blue (acid changed to yellow). The calcium and magnesium reagents were E.T.B. and the color turned pink (water without calcium and magnesium turned blue). The material of the present invention was added and turned into mineral water after 12 hours. The purified water prepared as described above had the effect of removing 92% of dioxins and of converting acidic water to alkaline after various reagents and experiments. Bar, improve the taste of water and sterilize Escherichia coli, and proved good efficacy as a result of five sense test, and the soil is acidified with chemicals and air pollution, and contaminates the water quality in the ground and deteriorates day by day. It will be able to prevent the cause of severe drinking water turmoil in the world in advance, and it will be able to reform the gradually acidified drinking water into alkaline and lichen water, which is expected to have a great effect on protecting aging, protecting the gastric membrane and making the intestines healthy. In addition, in the tank tank installed in an apartment and the apartment house In the process of supplying the water stored in each home, if the input constant of the invention in the water tank the tank it is possible for the acidified water to prevent corrosion of the steel pipe is connected to the phone by a water bath tank in alkaline water.

이상에서 설명한 바와 같이, 본 발명에 의하면 산성의 물을 알칼리성으로 전환시킬 수 있도록 함으로써 상당량의 수분을 섭취하지 않고는 살 수 없는 인체에 오염되지 않은 맑은 물을 공급할 수 있도록 하며, 위막 및 장을 보호하는 등 인체에 유익한 효과를 가져다 준다.즉, 통상 물 속에는 유기 미네랄과 무기 미네랄이 존재하는데 인간이 필요로 하는 유기 미네랄은 전체 미네랄 성분의 1% 밖에 들어 있지 않다. 물속에 함유된 미네랄의 주요 성분은 칼슘, 칼륨, 나트륨, 염소, 마그네슘외에 미량의 철, 망간, 구리, 요오드, 불소 등이다. 이 중 칼슘은 성인의 하루 필요량이 약 1g, 인은 약 0.8g, 칼륨의 경우는 2~4g, 나트륨은 2~4g, 망간은 12~20mg이다. 이 같은 미네랄을 물에서 섭취하기 위해서는 칼슘의 경우 46~57ℓ, 인은 3,3363ℓ, 칼슘은 1,000~2,000ℓ의 물을 마셔야 한다. 그러나, 인체는 하루 평균 1.5~1.8ℓ의 물을 생리적으로 요구 하기 때문에 물에서 미네랄을 섭취하기 위해 과량의 물을 마신다는 것은 현실적으로 불가능하다. 따라서, 미네랄은 음식물에서 섭취하고, 물은 깨끗이 정수된 안전한 물을 마셔야 한다는 관점에서 본 발명은 대단히 효과적인 발명인 것이다.As described above, according to the present invention, by converting the acidic water to alkaline, it is possible to supply clean water uncontaminated to the human body that can not live without ingesting a considerable amount of water, and protects the stomach and intestines It has a beneficial effect on the human body, such as organic minerals and inorganic minerals are usually present in the water, but the human body needs only 1% of the total minerals. The main components of minerals in water are calcium, potassium, sodium, chlorine, magnesium, trace iron, manganese, copper, iodine and fluorine. Among them, calcium is about 1g for adults, about 0.8g for phosphorus, about 2 ~ 4g for potassium, about 2 ~ 4g for sodium, and about 12 ~ 20mg for manganese. In order to consume such minerals in water, 46 to 57 ℓ of calcium, 3,3363 ℓ of phosphorus and 1,000 to 2,000 ℓ of calcium should be drunk. However, because the human body requires 1.5 to 1.8 liters of water a day on average, it is practically impossible to drink excess water to consume minerals from the water. Therefore, the present invention is a very effective invention from the point of view that minerals are taken from food and water should be safely purified water.

Claims (2)

세라믹, 맥반석, 제올라이트, 옥석, 견운모는 325메쉬로, 황토는 200∼325메쉬, 참숫은 150∼200메쉬로 분쇄하는 분쇄단계와,Ceramic, elvan, zeolite, gemstone, biotite to 325 mesh, loess to 200 to 325 mesh, torture and grinding to 150 to 200 mesh, 분쇄된 각 소재를 선별한 후 1000℃ 정도로 소성하여 급냉하는 건조단계와,A drying step of quenching by pulverizing about 1000 ℃ and then crushed each material, 분쇄된 황토, 맥반석, 제올라이트, 옥석, 견운모 등에 함유된 철분을 고강의 자석으로 제거하는 이물제거단계와,A foreign material removal step of removing the iron contained in the crushed ocher, elvan, zeolite, gemstone, biotite, etc. with a high-strength magnet, 황토 20%, 맥반석 30%, 제올라이트 15%, 옥석 15%, 견운모 15%, 참숫 5% 등의 비율로 혼합하되, 상기 각 소재들의 접착성을 위하여 60% 설탕 수용액을 첨가하여 회전하는 원통에 넣어 10∼20mm 크기의 구체로 제조한 후 자연건조하며, 구체의 표면에 5% 키토산 수용액을 분무하여 코팅하는 소성단계로 이루어지는 것을 특징으로 하는 음료수 정수제의 제조방법.20% ocher, 30% elvanite, 15% zeolite, 15% gemstone, 15% mica, 5%, etc. A method of producing a beverage water purifier, characterized in that the firing step of manufacturing a sphere of 10 to 20mm size and then drying naturally, spraying 5% chitosan aqueous solution on the surface of the sphere. 삭제delete
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