KR100340230B1 - a process for preparing cleanser soap - Google Patents

a process for preparing cleanser soap Download PDF

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Publication number
KR100340230B1
KR100340230B1 KR1019990012654A KR19990012654A KR100340230B1 KR 100340230 B1 KR100340230 B1 KR 100340230B1 KR 1019990012654 A KR1019990012654 A KR 1019990012654A KR 19990012654 A KR19990012654 A KR 19990012654A KR 100340230 B1 KR100340230 B1 KR 100340230B1
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South Korea
Prior art keywords
weight
parts
detergent
las
charcoal
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KR1019990012654A
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Korean (ko)
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KR19990046650A (en
Inventor
이수응
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(주)한국자원재활유지
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Priority to KR1019990012654A priority Critical patent/KR100340230B1/en
Publication of KR19990046650A publication Critical patent/KR19990046650A/en
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Publication of KR100340230B1 publication Critical patent/KR100340230B1/en

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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/10—Mixing; Kneading
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/143—Sulfonic acid esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions
    • C11D11/0094—Process for making liquid detergent compositions, e.g. slurries, pastes or gels
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/14—Shaping
    • C11D13/16—Shaping in moulds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/005—Synthetic soaps

Abstract

PURPOSE: A preparation method of a charcoal-containing detergent used for kitchen is provided, to minimize the skin stimulation and to enhance the washability by including the finely ground charcoal powders into the detergent. CONSTITUTION: The preparation method of the soap used for kitchen detergent comprises a grinding process of finely grinding the charcoal obtained by burning a firewood; first blending process of charging 8.5 parts by weight of the charcoal powders ground finely by the grinding process, 20 parts by weight of water, 30 parts by weight of a neutral detergent, 270 parts by weight of a sodium silicate, 30 parts by weight of DDPA(Sodium Tritolyl Phosphate), and 270 parts by weight of sodium sulfate into a stirrer to blend it for about 20-30 minutes; second blending process of further adding 400 parts by weight of LAS to the blend obtained after completing the first blending process and reworking the stirrer for about 5-10 minutes to mix LAS to the blend homogeneously, followed by charging the blend-completed liquid detergent into a container and hardening it to obtain a solid detergent.

Description

세제용 비누 제조방법 {a process for preparing cleanser soap}Detergent soap manufacturing method {a process for preparing cleanser soap}

본 발명은 숯이 함유된 주방용 세제의 제조방법에 관한 것으로, 특히 미세하게 분쇄시킨 숯 가루를 주방용 세제에 함유시킴으로서 피부에 대한 자극성을 최소화 시킴과 아울러, 세척력이 향상될수 있도록 한 숯이 함유된 주방용 세제의 제조방법에 관한 것이다.The present invention relates to a method for producing a dishwashing detergent containing charcoal, in particular, by containing a finely ground charcoal powder in the dishwashing detergent to minimize the irritation to the skin, as well as the cooking power containing the charcoal to improve cleaning It relates to a method for producing a detergent.

일반적으로 주방용 세제는 각종의 음식물을 담아주는 그릇이나 음식을 조리시 사용되는 조리용구 등에 묻어있는 음식물찌꺼기및 기름때 등을 세척시켜 줄때 사용되는 것으로서, 흔히 유효성분, 가용화제및 첨가제 등이 혼합된 수용액으로 구성되어 있는 것이다.In general, dishwashing detergents are used to wash food residues and oil stains, etc., which are embedded in bowls containing various foods or cooking utensils used to cook foods, and are often aqueous solutions mixed with active ingredients, solubilizers and additives. It is composed of.

상기와 같은 주방용 세제는 세척력에 따라 소비자의 구입에 많은 영향을 주게 되는 것으로서, 세척력을 높여주기 위해서는 첨가되는 첨가제의 량이 상대적으로 많은 함량을 보유하게 됨에 따라 세척력을 향상시킬 수 는 있으나 식기를 세척시 세제가 직접적으로 닿게 되는 손의 피부에 자극을 주게 되는 단점이 있음은 물론, 환경오염을 유발시키는 단점이 있는 것이다.The above dish detergent has a lot of influence on the purchase of the consumer according to the washing power, and in order to increase the washing power, the washing power can be improved as the amount of the additive added is relatively high. There is a disadvantage in that the detergent is directly irritated to the skin of the hand to be touched, there is a disadvantage that causes environmental pollution.

즉, 적은 량의 세제를 가지고도 식기에 묻어있는 음식물 찌꺼기나 기름때 등의 세척력을 높여주기 위해서는 높은 농도를 갖고 있는 첨가제를 사용하게 되므로서, 세척력이 좋게 되는 반면에, 상대적으로 피부에는 심한 자극을 주게되는 단점이 있는 것이고, 반대로 피부에 자극을 최소한으로 줄여주기 위해서는 사용되는 첨가제의 농도를 줄여 주게 되는데, 이때에는 세척력이 상대적으로 떨어지게 되는 단점이 있는 것이다.In other words, even with a small amount of detergent, high concentrations of additives are used to enhance the cleaning power of food residues and grease, etc. In order to reduce the irritation to the skin to a minimum, it is to reduce the concentration of the additive used, which is a disadvantage that the washing power is relatively reduced.

그리고, 세척력이 좋은 세제는 적은량이 사용되지만 농도가 그만큼 높아 사용이 완료되어 버려진 물을 여과시켜 줄때 그만큼 많은 량의 물이 필요하게 되는 것이고, 반대로 세척력이 떨어지는 세제는 세척력을 높여주기 위해 사용자가 많은량의 세제를 사용함에 따라 세제의 낭비를 초래함은 물론, 사용된 물의 여과시 사용되는 물의 량은 전자와 마찬 가지로 많은 량의 물이 소요되어야 하므로서, 환경오염을 유발시키게 되는 단점이 있었던 것이다.And, detergents that have good cleaning power are used in small amounts, but the concentration is so high that when the use is completed, the amount of water that is needed is filtered. On the contrary, detergents that have low cleaning power have many users to increase cleaning power. In addition to the waste of detergent, the amount of water used for filtration of the used water, as well as the amount of water used in the same amount as the former, had a disadvantage that causes environmental pollution. .

따라서, 본 발명은 식기 등에 묻어있는 음식물찌꺼기나 기름때 등의 오염물질을 세척시 사용되는 세제에 미세하게 분쇄된 숯 가루를 첨가시켜 준 세제를 사용함으로서, 최소한의 세제를 사용한 상태에서 세척은 우수함과 아울러, 피부의 자극을 최소한으로 줄여주어 피부의 손상을 방지할수 있도록 하는것을 기술적인 과제로 한다.Therefore, the present invention uses a detergent that adds finely ground charcoal powder to a detergent used to wash contaminants such as food scraps or oil stains on the tableware, etc. In addition, the technical problem is to reduce the irritation of the skin to the minimum to prevent damage to the skin.

이하, 본 발명을 상세히 설명하면 다음과 같다.본 발명은 주방용 세제의 제조에 있어서, 장작으로 태워서 만들어진 숯을 분쇄기를 통해 미세하게 분쇄시켜 주는 분쇄공정과; 상기 분쇄공정을 통해 미세하게 분쇄된 숯가루 8.5중량부와 물 20중량부, 중성세제 30중량부, 규산소다 270중량부, DDPA(Sodium Tritoly Phosphate) 30중량부, 망초(Sodium Sulfate) 270중량부를 교반기내에 혼합되도록 투입시켜 20 - 30분 정도의 시간에 걸쳐 혼합이 이루어지도록 하는 1차 배합공정과; 상기 1차배합 공정이 완료된 배합물에 라스(LAS) 400중량부의 량을 별도로 투입시켜 준 상태에서 5 - 10분 정도의 시간에 걸쳐 교반기를 재차 가동시켜 배합물에 라스가 고르게 혼합이 이루어지도록 한 다음 배합이 완료된 액체의 세제를 용기에 충진시켜 준 상태에서 경화시켜 주므로서 고형의 세제가 완성되도록 한 것을 특징으로 하는 세제용 비누의 제조방법이다.이하, 본 발명의 제조공정을 더욱 상세히 설명하면 다음과 같다.Hereinafter, the present invention will be described in detail. The present invention includes a grinding step of finely grinding a charcoal made by burning firewood through a grinder; 8.5 parts by weight of finely ground charcoal powder and 20 parts by weight of water, 30 parts by weight of neutral detergent, 270 parts by weight of sodium silicate, 30 parts by weight of DDPA (Sodium Tritoly Phosphate), 270 parts by weight of sodium sulfate A primary blending step of mixing the mixture into a stirrer and mixing the mixture over a time period of about 20 to 30 minutes; In a state in which 400 parts by weight of las (LAS) was separately added to the compound in which the primary compounding process was completed, the stirrer was restarted over a period of about 5 to 10 minutes so that las was uniformly mixed in the compound. This is a method for producing a soap for detergent, characterized in that the solid detergent is completed by curing the liquid detergent in the state filled in the container. Hereinafter, the manufacturing process of the present invention will be described in more detail. same.

제1공정(분쇄공정)First process (grinding process)

본 발명의 제 1공정은 장작으로 태워서 만들어진 숯을 분쇄기에 의해 미세하게 분쇄시켜 주는 단계이다.The first process of the present invention is a step of finely pulverizing the charcoal produced by burning with firewood.

이때, 분쇄되는 숯가루는 밀가루 정도의 메쉬가 되도록 곱게 분쇄가 이루어지게 되는 것으로서, 세제를 사용도중 알갱이의 숯가루에 의한 식기및 피부에 손상을 주지 않기 위함이다.At this time, the pulverized charcoal is to be finely pulverized so as to be a mesh of the wheat flour, so as not to damage the tableware and the skin caused by the charcoal of the granules during the use of the detergent.

제2공정(1차배합공정)2nd process (1st compounding process)

본 발명의 제 2공정은 물 2Kg, 중성세제 3Kg, 규산소다 27Kg, DDPA(Sodium Tritoly Phosphate) 3Kg, 망초(Sodium Sulfate) 27Kg과 상기 제1공정을 통해 미세하게 분쇄된 숯가루 850g을 교반기내에 혼합되도록 투입시켜 준 상태에서 20 - 30분 정도의 시간에 걸쳐 교반기를 가동시켜 혼합되어 있는 재료가 고루게 배합이 이루어지도록 한다.In the second process of the present invention, 2Kg of water, 3Kg of neutral detergent, 27Kg of sodium silicate, 3Kg of DDPA (Sodium Tritoly Phosphate), 27Kg of sodium sulfate and 850g of finely ground charcoal powder through the first process are mixed in a stirrer. Run the stirrer over a period of 20-30 minutes in the state of injecting to make sure that the mixed materials are evenly combined.

이때, 중성세제라 함은 식기를 세척시 음식물찌꺼기나 기름때 등이 효율적으로 제거될수 있는 계면활성 물질 즉, 음이온, 비이온, 양이온 계면활성제와 이들 계면활성제의 혼합물을 의미하는 것이다.In this case, the term "neutral detergent" refers to a surface-active substance that can efficiently remove food waste or oil when washing dishes, that is, an anion, nonionic, cationic surfactant, and a mixture of these surfactants.

제 3 공정(2차배합공정)Third Process (Secondary Blending Process)

본 발명의 제 3공정은 상기 제2공정을 거치면서 고루게 혼합된 혼합물내에 라스(LAS) 40Kg의 량을 제차 투입시켜 준 상태에서 5 - 10분 정도의 시간에 걸쳐 교반기를 가동시켜 1차로 혼합된 혼합물에 라스가 고르게 혼합이 이루어지도록 한 다음 상기와 같이 혼합이 완료된 혼합물의 일정한 크기 즉, 가정이나 업소에서 사용하기 정당한 크기를 갖는 용기에 충진시켜 준 상태에서 경화시켜 주므로서 고형세제가 완성되는 것이다.In the third process of the present invention, the stirrer is first mixed by operating the stirrer over a time of about 5-10 minutes in a state in which 40 kg of las (LAS) is added to the mixture evenly mixed through the second process. The lass are mixed evenly in the prepared mixture, and then the solid detergent is completed by curing in a state of filling the container having a certain size, that is, a size justified for use in a home or a business, as described above. will be.

상기와 같이 완성된 고형의 세제는 용기에 담겨져 있는 상태에서 판매 및 사용 하고자 하는 장소에 위치하고 있다가 사용자가 식기를 세척시 사용되는 행주등은 고형세제에 문질러 행주에 세제가 묻어나도록 한 상태에서 식기를 문질러 주도록 하여 상기 식기에 묻어있는 음식물찌꺼기나 기름때 등을 제거시켜 주면 되는 것이다.The solid detergent finished as described above is located in a place where it is to be sold and used in a state where it is contained in a container, and the dish towels used when the user washes the dishes are rubbed with a solid detergent so that the detergent is put on the dishcloth. Rub to remove food scraps and oil stains on the tableware.

본 발명의 다른 구현예로서는 제 2 공정을 거치면서 혼합된 혼합물에 라스(LAS) 40Kg을 첨가시켜 5 - 10분 정도 교반기를 이용하여 교반이 이루어지도록 한 상태에서 경화시키지 않고 바로 액체 상태의 세제를 용기에 담아 준 상태에서 사용할 수 도 있다.In another embodiment of the present invention, a liquid detergent is added directly to the mixed mixture during the second process, and the liquid detergent is immediately stored without curing in a state where stirring is performed by using a stirrer for about 5-10 minutes. Can also be used in the state given.

이상에서와 같이 본 발명은 분쇄기를 이용하여 밀가루 정도의 메쉬를 갖도록 분쇄된 숯가루를 세제를 형성할수 있도록 하는 각종의 혼합물과 함께 혼합되도록 한 상태로 하여 세제를 조성하므로서, 세제에 함유되어 있는 숯에 의해 세척력이 향상되어 적은 량의 세제를 사용함에 따라 세제의 사용에 의한 환경오염을 최소한으로 줄여줄수 있게되는 효과가 있고, 또한 세제의 자극성이 상대적으로 낮아져 피부에 자극을 주지 않게 되는 등의 효과가 있는 것이다.As described above, in the present invention, the charcoal contained in the detergent is formed by mixing the charcoal powder pulverized to have a mesh of flour with various mixtures so as to form a detergent. The cleaning power is improved by using a small amount of detergent, which can reduce the environmental pollution caused by the use of the detergent to a minimum, and the irritation of the detergent is relatively low, so that it does not irritate the skin. There is.

Claims (2)

주방용 세제의 제조에 있어서, 장작으로 태워서 만들어진 숯을 분쇄기를 통해 미세하게 분쇄시켜 주는 분쇄공정과; 상기 분쇄공정을 통해 미세하게 분쇄된 숯가루 8.5중량부와 물 20중량부, 중성세제 30중량부, 규산소다 270중량부, DDPA(Sodium Tritoly Phosphate) 30중량부, 망초(Sodium Sulfate) 270중량부를 교반기내에 혼합되도록 투입시켜 20 - 30분 정도의 시간에 걸쳐 혼합이 이루어지도록 하는 1차 배합공정과; 상기 1차배합 공정이 완료된 배합물에 라스(LAS) 400중량부의 량을 별도로 투입시켜 준 상태에서 5 - 10분 정도의 시간에 걸쳐 교반기를 재차 가동시켜 배합물에 라스가 고르게 혼합이 이루어지도록 한 다음 배합이 완료된 액체의 세제를 용기에 충진시켜 준 상태에서 경화시켜 주므로서 고형의 세제가 완성되도록 한 것을 특징으로 하는 세제용 비누의 제조방법.In the manufacture of kitchen detergent, the grinding step of finely grinding the charcoal burned with firewood through a grinder; 8.5 parts by weight of finely ground charcoal powder and 20 parts by weight of water, 30 parts by weight of neutral detergent, 270 parts by weight of sodium silicate, 30 parts by weight of DDPA (Sodium Tritoly Phosphate), 270 parts by weight of sodium sulfate A primary blending step of mixing the mixture into a stirrer and mixing the mixture over a time period of about 20 to 30 minutes; In a state in which 400 parts by weight of las (LAS) was separately added to the compound in which the primary compounding process was completed, the stirrer was restarted over a period of about 5 to 10 minutes so that las was uniformly mixed in the compound. Method for producing a soap for detergent, characterized in that the solid detergent is completed by curing in a state in which the detergent of the completed liquid is filled in the container. 제 1 항에 있어서, 상기 제 3공정은 공정을 거치면서 혼합된 배합물을 경화시키지 않고 액체의 세제로 사용할수 있도록 한 것을 특징으로 하는 세제용 비누의 제조방법.The method of claim 1, wherein the third step is a method of producing a soap for detergents, characterized in that it can be used as a liquid detergent without curing the blended mixture through the process.
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KR20010045676A (en) * 1999-11-05 2001-06-05 문정순 Manufacturing method of cleanser
KR20020064471A (en) * 2001-02-01 2002-08-09 황성하 Manufacturing method of pine charcoal and novel use thereof as an anticancer agent

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KR840002897A (en) * 1982-04-21 1984-07-21 배기철 Manufacturing method of byeongje
KR920009963A (en) * 1990-11-21 1992-06-26 로버어트 시이 설리반 Concentrated liquid dishwashing detergent composition containing alkyl benzene sulfonate and magnesium
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