KR19990046650A - a cleanser soap devise - Google Patents
a cleanser soap devise Download PDFInfo
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- KR19990046650A KR19990046650A KR1019990012654A KR19990012654A KR19990046650A KR 19990046650 A KR19990046650 A KR 19990046650A KR 1019990012654 A KR1019990012654 A KR 1019990012654A KR 19990012654 A KR19990012654 A KR 19990012654A KR 19990046650 A KR19990046650 A KR 19990046650A
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- South Korea
- Prior art keywords
- detergent
- las
- completed
- compound
- stirrer
- Prior art date
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- 239000000344 soap Substances 0.000 title claims 2
- 239000003599 detergent Substances 0.000 claims abstract description 30
- 238000000034 method Methods 0.000 claims abstract description 18
- 239000003610 charcoal Substances 0.000 claims abstract description 16
- 238000002156 mixing Methods 0.000 claims abstract description 8
- 239000000843 powder Substances 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 claims abstract description 5
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 4
- 238000000227 grinding Methods 0.000 claims abstract description 4
- 230000007935 neutral effect Effects 0.000 claims abstract description 4
- 239000013042 solid detergent Substances 0.000 claims abstract description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 3
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 3
- 239000004115 Sodium Silicate Substances 0.000 claims abstract description 3
- 229910052681 coesite Inorganic materials 0.000 claims abstract description 3
- 229910052906 cristobalite Inorganic materials 0.000 claims abstract description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims abstract description 3
- 239000010452 phosphate Substances 0.000 claims abstract description 3
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 3
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 3
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 3
- 239000011734 sodium Substances 0.000 claims abstract description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 claims abstract description 3
- 235000011152 sodium sulphate Nutrition 0.000 claims abstract description 3
- 229910052682 stishovite Inorganic materials 0.000 claims abstract description 3
- 229910052905 tridymite Inorganic materials 0.000 claims abstract description 3
- 150000001875 compounds Chemical class 0.000 claims abstract 5
- 239000000203 mixture Substances 0.000 claims description 8
- 238000009472 formulation Methods 0.000 claims 1
- 238000010298 pulverizing process Methods 0.000 claims 1
- 238000005406 washing Methods 0.000 abstract description 6
- 230000007794 irritation Effects 0.000 abstract description 4
- 238000004140 cleaning Methods 0.000 description 5
- 239000010794 food waste Substances 0.000 description 5
- 239000000654 additive Substances 0.000 description 4
- 238000004851 dishwashing Methods 0.000 description 3
- 238000003912 environmental pollution Methods 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 2
- 235000013312 flour Nutrition 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 241000209140 Triticum Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/10—Mixing; Kneading
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/143—Sulfonic acid esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0094—Process for making liquid detergent compositions, e.g. slurries, pastes or gels
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/14—Shaping
- C11D13/16—Shaping in moulds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
본 발명은 미세하게 분쇄시킨 숯 가루를 세제에 함유시킴으로서 피부에 대한 자극성을 최소화 시킴과 아울러, 세척력이 향상될수 있도록 한 숯이 함유된 주방용 세제 제조방법에 관한 것으로, 이는 장작으로 태워서 만들어진 숯을 분쇄기를 통해 미세하게 분쇄시켜 주는 분쇄공정과; 상기 분쇄공정을 통해 미세하게 분쇄된 숯가루 850gr과 물 2Kg, 중성세제 3Kg, 규산소다(SiO2 Co3) 27Kg, DDPA(Sodium Tritoly Phosphate) 3Kg, 망초(Sodium Sulfate) 27Kg을 교반기내에 혼합되도록 투입시켜 20 - 30분 정도의 시간에 걸쳐 혼합이 이루어지도록 하는 1차 배합공정과; 상기 1차배합 공정이 완료된 배합물에 라스(LAS) 40Kg의 량을 별도로 투입시켜 준 상태에서 5 - 10분 정도의 시간에 걸쳐 교반기를 재차 가동시켜 배합물에 라스가 고르게 혼합이 이루어지도록 한 다음 배합이 완료된 액체의 세제를 용기에 충진시켜 준 상태에서 경화시켜 주므로서 고형의 세제가 완성되도록 한 것을 특징으로 한다.The present invention relates to a method for preparing a kitchen detergent containing charcoal to minimize the irritation to the skin by including finely crushed charcoal powder in the detergent and to improve the washing power, which is a pulverized charcoal made by burning firewood. Grinding process for finely grinding through; The finely pulverized charcoal powder 850gr and water 2Kg, neutral detergent 3Kg, sodium silicate (SiO2 Co3) 27Kg, DDPA (Sodium Tritoly Phosphate) 3Kg, sodium sulfate (27Kg) to be mixed in the stirrer 20 A primary blending process for mixing over a time period of about 30 minutes; In a state in which 40 kg of las (LAS) was separately added to the compound in which the primary blending process was completed, the stirrer was restarted over a period of about 5 to 10 minutes so that las was uniformly mixed in the compound. It is characterized in that the solid detergent is completed by curing the detergent of the completed liquid in the state filled in the container.
Description
본 발명은 숯이 함유된 주방용 세제 제조방법에 관한 것으로, 특히 미세하게 분쇄시킨 숯 가루를 세제에 함유시킴으로서 피부에 대한 자극성을 최소화 시킴과 아울러, 세척력이 향상될수 있도록 한 숯이 함유된 주방용 세제 제조방법에 관한 것이다.The present invention relates to a method of manufacturing a detergent containing charcoal, and to preparing a detergent containing charcoal to minimize the irritation to the skin and to improve the washing power by incorporating the finely ground charcoal powder into the detergent. It is about a method.
일반적으로 주방용 세제는 각종의 음식물을 담아주는 그릇이나 음식을 조리시 사용되는 조리용구 등에 묻어있는 음식물찌꺼기및 기름때 등을 세척시켜 줄때 사용되는 것으로서, 흔히 유효성분, 가용화제및 첨가제 등이 혼합된 수용액으로 구성되어 있는 것이다.In general, dishwashing detergents are used to wash food residues and oil stains, etc., which are embedded in bowls containing various foods or cooking utensils used to cook foods, and are often aqueous solutions mixed with active ingredients, solubilizers and additives. It is composed of.
상기와 같은 주방용 세제는 세척력에 따라 소비자의 구입에 많은 영향을 주게 되는 것으로서, 세척력을 높여주기 위해서는 첨가되는 첨가제의 량이 상대적으로 많은 함량을 보유하게 됨에 따라 서척력을 향상될수는 있으나 식기를 세척시 세제가 직접적으로 닿게되는 손의 피부에 자극을 주게되는 단점이 있음은 물론, 환경오염을 유발시키는 단점이 있는 것이다.The above dish detergent has a lot of influences on the purchase of consumers according to the washing power, and in order to increase the washing power, the washing power may be improved as the amount of the additive added is relatively high, but when washing dishes There is a disadvantage in that the detergent is directly irritated to the skin of the hand to be touched, there is a disadvantage that causes environmental pollution.
즉, 적은 량의 세제를 가지고도 식기에 묻어있는 음식물찌꺼기나 기름때 등의 세척력을 높여주기 위해서는 높은 농도를 갖고있는 첨가제를 사용하게 되므로서, 세척력이 좋게 되는 반면에, 상대적으로 피부에는 심한 자극을 주게되는 단점이 있는 것이고, 반대로 피부에 자극을 최고한으로 줄여주기 위해서는 사용되는 첨가제의 농도를 줄여주게 되는데, 이때에는 세척력이 상대적으로 떨어지게 되는 단점이 있는 것이다.In other words, even with a small amount of detergent, the additives with high concentration are used to enhance the cleaning power of food scraps and oil stains on the tableware. In order to reduce the irritation to the skin to the maximum, the concentration of the additive to be used is reduced, at which time the washing power is relatively poor.
그리고, 세척력이 좋은 세제는 적은량이 사용되지만 농도가 그만큼 높아 사용이 완료되어 버려진 물을 여과시켜 줄때 그만큼 많은 량의 물이 필요하게 되는 것이고, 반대로 세척력이 떨어지는 세제는 세척력을 높여주기 위해 사용자가 많은량의 세제를 사용함에 따라 세제의 낭비를 초래함은 물론, 사용된 물의 여과시 사용되는 물의 량은 전자와 마찬 가지로 많은 량의 물이 소요되어야 하므로서, 환경오염을 유발시키게 되는 단점이 있었던 것이다.And, detergents that have good cleaning power are used in small amounts, but the concentration is so high that when the use is completed, the amount of water that is needed is filtered. On the contrary, detergents that have low cleaning power have many users to increase cleaning power. In addition to the waste of detergent, the amount of water used for filtration of the used water, as well as the amount of water used in the same amount as the former, had a disadvantage that causes environmental pollution. .
따라서, 본 발명은 식기 등에 묻어있는 음식물찌꺼기나 기름때 등의 오염물질을 세척시 사용되는 세제에 미세하게 분쇄된 숯 가루를 첨가시켜 준 세제를 사용함으로서, 최소한의 세제를 사용한 상태에서 세척은 우수함과 아울러, 피부의 자극을 최소한으로 줄여주어 피부의 손상을 방지할수 있도록 하는데 그 목적이 있는 것이다.Therefore, the present invention uses a detergent that adds finely ground charcoal powder to a detergent used to wash contaminants such as food scraps or oil stains on the tableware, etc. In addition, the purpose is to reduce the irritation of the skin to a minimum to prevent damage to the skin.
이하, 본 발명의 제조공정을 설명하면 다음과 같다.Hereinafter, the manufacturing process of the present invention will be described.
제1공정(분쇄공정)First process (grinding process)
장작으로 태워서 만들어진 숯을 분쇄기에 의해 미세하게 분쇄시켜 준다.The charcoal made by burning firewood is finely ground by a grinder.
이때, 분쇄되는 숯가루는 밀가루 정도의 메쉬가 되도록 곱게 분쇄가 이루어지게 되는 것으로서, 세제를 사용도중 알갱이의 숯가루에 의한 식기및 피부에 손상을 주지 않기 위함이다.At this time, the pulverized charcoal is to be finely pulverized so as to be a mesh of the wheat flour, so as not to damage the tableware and the skin caused by the charcoal of the granules during the use of the detergent.
제2공정(1차배합공정)2nd process (1st compounding process)
물 2Kg, 중성세제 3Kg, 규산소다(SiO2 Co3) 27Kg, DDPA(Sodium Tritoly Phosphate) 3Kg, 망초(Sodium Sulfate) 27Kg과 상기 제1공정을 통해 미세하게 분쇄된 숯가루 850g을 교반기내에 혼합되도록 투입시켜 준 상태에서 20 - 30분 정도의 시간에 걸쳐 교반기를 가동시켜 혼합되어 있는 재료가 고루게 배합이 이루어지도록 한다.2Kg of water, 3Kg of neutral detergent, 27Kg of sodium silicate (SiO2 Co3), 3Kg of DDPA (Sodium Tritoly Phosphate), 27Kg of sodium sulphate and 850g of finely ground charcoal powder through the first process are mixed to be mixed in a stirrer. Run the stirrer over a period of 20-30 minutes in a quasi-state to ensure that the ingredients are mixed evenly.
이때, 중성세제라 함은 식기를 세척시 음식물찌꺼기나 기름때 등이 효율적으로 제거될수 있는 계면활성 물질 즉, 음이온, 비이온, 양이온 계면활성제와 이들 계면활성제의 혼합물을 의미하는 것이다.In this case, the term "neutral detergent" refers to a surface-active substance that can efficiently remove food waste or oil when washing dishes, that is, an anion, nonionic, cationic surfactant, and a mixture of these surfactants.
제 3 공정(2차배합공정)Third Process (Secondary Blending Process)
상기 제2공정을 거치면서 고루게 혼합된 혼합물내에 라스(LAS) 40Kg의 량을 제차 투입시켜 준 상태에서 5 - 10분 정도의 시간에 걸쳐 교반기를 가동시켜 1차로 혼합된 혼합물에 라스가 고르게 혼합이 이루어지도록 한 다음 상기와 같이 혼합이 완료된 혼합물의 일정한 크기 즉, 가정이나 업소에서 사용하기 정당한 크기를 갖는 용기에 충진시켜 준 상태에서 경화시켜 주므로서 고형세제가 완성되는 것이다.After the second process, the las is uniformly mixed with the first mixed mixture by operating a stirrer over a time of about 5-10 minutes while the amount of 40 kg of las is added to the mixed mixture evenly. After this is done, the solid detergent is completed by curing in a state in which a mixture of the mixture is completed as described above, that is, filled in a container having a size that is justified for use in a home or a business.
상기와 같이 완성된 고형의 세제는 용기에 담겨져 있는 상태에서 판매및 사용 하고자 하는 장소에 위치하고 있다가 사용자가 식기를 세척시 사용되는 행주등은 고형세제에 문질러 행주에 세제가 묻어나도록 한 상태에서 식기를 문질러 주도록 하여 상기 식기에 묻어있는 음식물찌꺼기나 기름때 등을 제거시켜 주면 되는 것이다.The solid detergent finished as described above is located in a place where it is intended to be sold and used in a state in which the dishwasher is used. Rub to remove food scraps and oil stains on the tableware.
본 발명의 다른 실시예로서는 제 2 공정을 거치면서 혼합된 혼합물에 라스(LAS) 40Kg을 첨가시켜 5 - 10분 정도 교반기를 이용하여 교반이 이루어지도록 한 상태에서 경화시키지 않고 바로 액체 상태의 세제를 용기에 담아 준 상태에서 사용할수도 있는 것이다.According to another embodiment of the present invention, a liquid detergent is added directly to the mixed mixture through the second process, and the liquid detergent is immediately stored without curing in a state where stirring is performed by using a stirrer for about 5-10 minutes. It can also be used in the state given.
이상에서와 같이 본 발명은 분쇄기를 이용하여 밀가루 정도의 메쉬를 갖도록 분쇄된 숯가루를 세제를 형성할수 있도록 하는 각종의 혼합물과 함께 혼합되도록 한 상태로 하여 세제를 조성하므로서, 세제에 함유되어 있는 숯에 의해 세척력이 향상되어 적은 량의 세제를 사용함에 따라 세제의 사용에 의한 환경오염을 최소한으로 줄여줄수 있게되는 효과가 있고, 또한 세제의 독성이 상대적으로 낮아져 피부에 자극을 주지 않게 되는 등의 효과가 있는 것이다.As described above, in the present invention, the charcoal contained in the detergent is formed by mixing the charcoal powder pulverized to have a mesh of flour with various mixtures so as to form a detergent. The cleaning power is improved by using a small amount of detergent, which can reduce the environmental pollution caused by the use of the detergent to a minimum, and the toxicity of the detergent is relatively low, so that it does not irritate the skin. There is.
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| Application Number | Priority Date | Filing Date | Title |
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| KR1019990012654A KR100340230B1 (en) | 1999-04-10 | 1999-04-10 | a process for preparing cleanser soap |
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| KR1019990012654A KR100340230B1 (en) | 1999-04-10 | 1999-04-10 | a process for preparing cleanser soap |
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| KR19990046650A true KR19990046650A (en) | 1999-07-05 |
| KR100340230B1 KR100340230B1 (en) | 2002-06-12 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20000061940A (en) * | 1999-03-27 | 2000-10-25 | 이창진 | Aaaaa |
| KR20010045676A (en) * | 1999-11-05 | 2001-06-05 | 문정순 | Manufacturing method of cleanser |
| WO2002061019A1 (en) * | 2001-02-01 | 2002-08-08 | Seng-Ha Hoang | Manufacturing method of pine charcoal and novel use thereof as an anticancer agent |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR840002897A (en) * | 1982-04-21 | 1984-07-21 | 배기철 | Manufacturing method of byeongje |
| NZ240394A (en) * | 1990-11-21 | 1994-01-26 | Colgate Palmolive Co | Liquid detergent comprising alkylbenzene sulphonate, a magnesium salt and |
| KR0156660B1 (en) * | 1995-12-19 | 1998-12-15 | 이능희 | Cosmetic soap composition containing powdered active carbon |
| KR100206523B1 (en) * | 1996-08-21 | 1999-07-01 | 이흥렬 | The method for removing arochemicals and heavy metals from the surface of fruit |
| KR19980067230A (en) * | 1997-01-31 | 1998-10-15 | 이병모 | Composition and preparation method of laundry detergent for emulsifying |
| JP2981451B2 (en) * | 1997-06-06 | 1999-11-22 | 花王株式会社 | Concentrated liquid detergent composition for kitchen |
| KR19990015362A (en) * | 1997-08-01 | 1999-03-05 | 김선자 | Compositions of fats and oils for cleaning clothes |
| JPH11140492A (en) * | 1997-11-11 | 1999-05-25 | Ishihara Kk | Charcoal from bamboo |
| KR19980087670A (en) * | 1998-09-08 | 1998-12-05 | 박영태 | Skin cleaning and anti-inflammatory preparation method using powdered activated carbon |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20000061940A (en) * | 1999-03-27 | 2000-10-25 | 이창진 | Aaaaa |
| KR20010045676A (en) * | 1999-11-05 | 2001-06-05 | 문정순 | Manufacturing method of cleanser |
| WO2002061019A1 (en) * | 2001-02-01 | 2002-08-08 | Seng-Ha Hoang | Manufacturing method of pine charcoal and novel use thereof as an anticancer agent |
| KR20020064471A (en) * | 2001-02-01 | 2002-08-09 | 황성하 | Manufacturing method of pine charcoal and novel use thereof as an anticancer agent |
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| KR100340230B1 (en) | 2002-06-12 |
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