JPS6327409A - Multilayer type cosmetic - Google Patents

Multilayer type cosmetic

Info

Publication number
JPS6327409A
JPS6327409A JP16955186A JP16955186A JPS6327409A JP S6327409 A JPS6327409 A JP S6327409A JP 16955186 A JP16955186 A JP 16955186A JP 16955186 A JP16955186 A JP 16955186A JP S6327409 A JPS6327409 A JP S6327409A
Authority
JP
Japan
Prior art keywords
water
alkyl phenyl
layer
phenyl ether
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP16955186A
Other languages
Japanese (ja)
Inventor
Shinji Tobe
信治 戸辺
Fuminori Harusawa
春沢 文則
Miyuki Kawachi
河内 みゆき
Keiichi Uehara
計一 植原
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shiseido Co Ltd
Original Assignee
Shiseido Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shiseido Co Ltd filed Critical Shiseido Co Ltd
Priority to JP16955186A priority Critical patent/JPS6327409A/en
Publication of JPS6327409A publication Critical patent/JPS6327409A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/03Liquid compositions with two or more distinct layers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/39Derivatives containing from 2 to 10 oxyalkylene groups
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/002Aftershave preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

PURPOSE:A multi-layer type cosmetic that contains, as essential components, a surface active agent of polyglycerol alkyl phenyl ether type, water-soluble salts, an oily substance which is liquid at room temperature and water, thus having both clear oil and aqueous layers without unclear surfactant layer on the boundary between the two layers. CONSTITUTION:The objective multi-layer type cosmetic contains, as essential components, (A) 0.05-3wt% of a polyglycerol alkyl phenyl ether of formula I or II (n is 3-20), (B) 0.05-2wt% of salts soluble in water such as NaCl, MgSO4 or sodium succinate, (C) 1-50wt% of an oily substance which is liquid at room temperature such as fluid paraffin, squalane or olive oil and water. The resultant cosmetic rapidly separates into individual layers, when it is left to stand to form both clear oil and water phases without formation of unclear phase of the surfactant on the boundary of these phases, while it readily forms complete emulsion state by slight shaking, when it is applied, to give smooth feeling.

Description

【発明の詳細な説明】 [産業上の利用分野] 本発明は、ポリグリセリンアルキルフェニルエーテル型
の界面活性剤を含有することにより形成される新規な多
層型化粧料に関し、更に詳しくは油層及び水層が透明、
且つ両層の界面に活性剤層が存在せずくっきりと二層に
分離するという外観、及び使用時に軽く振盪することに
より容易に混合して乳化状となって、まろやかな使用感
触が得られるという特徴を有する多層型化粧料に関する
Detailed Description of the Invention [Industrial Field of Application] The present invention relates to a novel multilayer cosmetic composition formed by containing a polyglycerin alkyl phenyl ether type surfactant, and more specifically, to a multilayer cosmetic composition containing a polyglycerin alkyl phenyl ether type surfactant. The layer is transparent,
In addition, there is no active agent layer at the interface between the two layers, and the product appears to be clearly separated into two layers, and when used, it can be easily mixed into an emulsified state by shaking lightly, giving it a mellow feel when used. The present invention relates to a multilayer cosmetic having characteristics.

[従来の技術] 従来よりポリオキシエチレンソルビトール脂肪酸エステ
ル、ポリオキシエチレンソルビタン脂肪酸エステル、ポ
リエチレングリコール脂肪酸エステル、ポリオキシエチ
レンオレイルアルコールエーテル、ポリオキシエチレン
硬化ヒマシ油、ポリオキシエチレン脂肪酸アミド、ソル
ビタン脂肪酸エステル等を用いた二層型、三層型等の多
層型化粧料は広く知られているが、使用時や運搬時の振
盪、振動により混合すると分離に長時間を要し、又分離
後も油層、水層のいずれか或は両層が完全に透明になら
なかったり、油層・水層の界面に不明瞭な界面活性剤層
が現れたりして外観状好ましくないという欠点を有して
いた。
[Prior art] Conventionally, polyoxyethylene sorbitol fatty acid ester, polyoxyethylene sorbitan fatty acid ester, polyethylene glycol fatty acid ester, polyoxyethylene oleyl alcohol ether, polyoxyethylene hydrogenated castor oil, polyoxyethylene fatty acid amide, sorbitan fatty acid ester, etc. Multi-layer cosmetics such as two-layer and three-layer types using The problem is that one or both of the water layers may not become completely transparent, or an unclear surfactant layer may appear at the interface between the oil layer and the water layer, resulting in an unfavorable appearance.

[発明が解決しようとする問題点] 本発明者等は、このような状況に鑑み様々な界面活性剤
について鋭意検討した結果、ポリグリセリンアルキルフ
ェニルエーテル型の界面活性剤を用いれば従来の多層型
化粧料の欠点を解消し、振盪時の混合、乳化が良好で、
静置時の分離が速で、且つ油層、水層が透明で両層の界
面に不明瞭な界面活性剤層が現れないということを見出
し本発明を完成するに至った。
[Problems to be Solved by the Invention] In view of the above circumstances, the present inventors have conducted extensive studies on various surfactants, and have found that if a polyglycerin alkyl phenyl ether type surfactant is used, the conventional multilayer type surfactant can be used. Eliminates the drawbacks of cosmetics, provides good mixing and emulsification during shaking,
The present invention was completed based on the discovery that separation is quick when left still, the oil and water layers are transparent, and no unclear surfactant layer appears at the interface between the two layers.

[問題点を解決するための手段] 即ち、本発明は (イ)ポリグリセリンアルキルフェニルエーテル型化合
物から選ばれる一種又は二種以上(ロ)水溶性塩 (ハ)常温で液状の油性物質 及び (ニ)水 を必須成分として含有することを特徴とする多層型化粧
料である。
[Means for Solving the Problems] That is, the present invention provides (a) one or more types selected from polyglycerin alkyl phenyl ether type compounds, (b) a water-soluble salt, (c) an oily substance that is liquid at room temperature, and (c) an oily substance that is liquid at room temperature. d) It is a multilayer cosmetic characterized by containing water as an essential ingredient.

以下、本発明について詳述する。The present invention will be explained in detail below.

本発明で用いるポリグリセリンアルキルフェニルエーテ
ル型化合物は、グリセリンの平均重合度(n)が2以上
のポリグリセリンのアルキルフェニルエールであり、下
記一般式(1)又は(2)或はそれらの混合物で表され
る。これらのうちから一種又は二種以上が任意に選択さ
れて用いられる。
The polyglycerin alkyl phenyl ether type compound used in the present invention is an alkyl phenyl ether of polyglycerin having an average degree of polymerization (n) of 2 or more, and is represented by the following general formula (1) or (2) or a mixture thereof. expressed. One or more of these may be arbitrarily selected and used.

式(1) %式% 式(2) H ■ RC6H40[CH2CHCH20] n8式(1)及
び(2)中、Rは炭素数2〜24の直鎖又は分岐鎖の飽
和又は不飽和のアルキル基であり、例えばエチル、プロ
ピル、ブチル、ヘプチル、ヘキシル、オクチル、ノニル
、デシル、ウンデシル、ドデシル、トリデシル、テトラ
デシル、ペンタデシル、ヘキサデシル、ヘプタデシル、
オクタデシル、ノナデシル、エイコシル、2−へキシル
デシル、2−へブチルウンデシル、オレイル、2−オク
チルドデシル等が挙げられる。好ましくは炭素数が4〜
18のアルキル基である。
Formula (1) % Formula % Formula (2) H ■ RC6H40[CH2CHCH20] n8 In formulas (1) and (2), R is a linear or branched saturated or unsaturated alkyl group having 2 to 24 carbon atoms. Examples include ethyl, propyl, butyl, heptyl, hexyl, octyl, nonyl, decyl, undecyl, dodecyl, tridecyl, tetradecyl, pentadecyl, hexadecyl, heptadecyl,
Examples include octadecyl, nonadecyl, eicosyl, 2-hexyldecyl, 2-hebutylundecyl, oleyl, 2-octyldodecyl, and the like. Preferably the number of carbon atoms is 4 or more
18 alkyl groups.

又上記式(1)及び(2)中のnは、平均付加モル数で
2〜60、好ましくは3〜20の数である。
Further, n in the above formulas (1) and (2) is a number of 2 to 60, preferably 3 to 20, in terms of the average number of added moles.

本発明のポリグリセリンアルキルフェニルエーテル型化
合物は、一般的にはアルキルフェノールにグリシドール
を付加重合させて合成される。
The polyglycerol alkyl phenyl ether type compound of the present invention is generally synthesized by addition polymerizing glycidol to alkylphenol.

ポリグリセリンアルキルフェニルエール型化合物の配合
量は、0.01〜5重量%(以下%と略す)、好ましく
は0.05〜3%である。
The blending amount of the polyglycerol alkyl phenyl ale type compound is 0.01 to 5% by weight (hereinafter abbreviated as %), preferably 0.05 to 3%.

水溶性塩類としては無機塩、有機酸塩を用いることがで
き、塩化ナトリウム、塩化カリウム、硫酸ナトリウム、
硫酸マグネシウム、炭酸ナトリウム、炭酸カルシウム、
亜硫酸ナトリウム、クエン酸ナトリウム、リンゴ酸ナト
リウム、コハク酸ナトリウム、酒石酸ナトリウム、乳酸
ナトリウム、ピロリドンカルボン酸ナトリウム、リン酸
二水素ナトリウム等が好ましく、これらの一種又は二種
以上を用いることが出きる。
Inorganic salts and organic acid salts can be used as water-soluble salts, including sodium chloride, potassium chloride, sodium sulfate,
Magnesium sulfate, sodium carbonate, calcium carbonate,
Sodium sulfite, sodium citrate, sodium malate, sodium succinate, sodium tartrate, sodium lactate, sodium pyrrolidone carboxylate, sodium dihydrogen phosphate, etc. are preferred, and one or more of these can be used.

水溶性塩類の配合量は0.01〜4%で好ましくは0゜
05〜2%である。
The amount of water-soluble salts added is 0.01 to 4%, preferably 0.05 to 2%.

常温で液状の油性物質としては、炭化水素類、脂肪酸類
、エステル類、油脂類等があり、流動パラフィン、スク
ワラン、イソステアリン酸、グリセリルトリオクタノエ
ート、イソプロピルミリステート、ホホバ油、ヒマシ油
、オリーブ油、サフラワー油、ミンク油、シリコーン油
、ビタミンE誘導体等が好ましく、これらの一種又は二
種以上を用いることができる。
Oily substances that are liquid at room temperature include hydrocarbons, fatty acids, esters, fats and oils, and include liquid paraffin, squalane, isostearic acid, glyceryl trioctanoate, isopropyl myristate, jojoba oil, castor oil, and olive oil. , safflower oil, mink oil, silicone oil, vitamin E derivatives, etc. are preferred, and one or more of these can be used.

常温で液状の油性物質の配合量は1〜50χで、その配
合量は目的とする使用性等によって決定される。
The amount of the oily substance that is liquid at room temperature ranges from 1 to 50x, and the amount is determined depending on the intended usability.

本発明の多層型化粧料には、必要に応じて本発明の効果
を損なわない範囲で通常化粧品に用いられる油溶性、水
溶性及びその他の物質を配合することができる。例えば
エタノール、イソプロピルアルコール等の低級アルコー
ル、保湿剤、増粘剤、防腐剤、金属イオン封鎖剤、酸化
防止剤、紫外線吸収剤、生薬、薬剤、顔料、分散剤、色
素、香料等が挙げられる。
The multilayer cosmetic composition of the present invention may contain oil-soluble, water-soluble, and other substances commonly used in cosmetics, if necessary, within a range that does not impair the effects of the present invention. Examples include lower alcohols such as ethanol and isopropyl alcohol, humectants, thickeners, preservatives, sequestering agents, antioxidants, ultraviolet absorbers, herbal medicines, drugs, pigments, dispersants, pigments, and fragrances.

本発明の多層型化粧料は、スキンローション、アフター
シェーブローション、カーマインローション、ボデーロ
ーション等のスキンケア製品、ヘアリンス、ヘアリキッ
ド、スカルプロージョン等のヘア製品、フレグランス製
品等幅広い応用が可能である。
The multilayer cosmetic of the present invention can be widely applied to skin care products such as skin lotion, aftershave lotion, carmine lotion, and body lotion, hair products such as hair rinse, hair liquid, and scalp lotion, and fragrance products.

[実施例コ 次に本発明の実施例及び比較例を示し、本発明の効果を
より具体的に説明する。これらは本発明を何ら限定する
ものではない。
[Example] Next, Examples and Comparative Examples of the present invention will be shown to explain the effects of the present invention more specifically. These do not limit the present invention in any way.

実施例1 第−表の記号はそれぞれ次の内容を表す。Example 1 The symbols in Table 1 represent the following contents.

上  層:○・・・透明 X・・・白濁界  面二〇・
・・存在せず ×・・・存在する(活性剤層) 下  層:○・・・透明 △・・・やや白濁混合後の分
離の速き:O・・・速い ×・・・遅い第  1  表 実施例2 スキンローション (1)ポリグリセリン(6) ノニルフェニルエーテル 0.6% (2)ポリグリセリン(10) ノニルフェニルエーテル 0.4 (3)スクワラン        15(4)香料  
         0.1(5)エタノール     
   15(6)防腐剤          081(
7)グリセリン        5 (8)乳酸ナトリウム      1 (9)色素          適量 (10)精製水         62.8実施例3 
アフターシェーブローション(1)ポリグリセリン(8
) ノニルフェニルエーテル 2% (2〕ポリグリセリン(5) ノニルフェニルエーテル 0.5 (3)流動パラフィン      5 (4)グリセリル トリオクタノエート    2 (5)香料           0.2(6)l−メ
ントール      0.3(7)エタノール    
   20 (8)ヘチマ抽出液       0.5(9)プロピ
レングリコール   5 (10)リン酸二水素ナトリウム 0.5(11)精製
水         64.01実施例4 カーマイン
ローション (1)ポリグリセリン(10) ノニルフェニルエーテル  1 (2)イソプロピルミリステート 2 (3)p−ジメチルアミノ 安息香酸オクチル    1 (4)香料           0.1(5)エタノ
ール        10(6N、3− ブチレングリコール 10 (7)炭酸ナトリウム      1.5(8)酸化チ
タン        5 (9)酸化鉄         適量 (10)エデト酢酸三ナトリウム 0.2(11)精製
水         69.2実施例4 スカルブロー
ジョン (1)ポリグリセリン(8) トチ゛シルフェニルエーテル4 (2)シリコーン油       3 (3)ビタミンE誘導体     0.5(4)香料 
          0.1(5)l−メントール  
    0.1(6)エタノール        30
(7)ジプロピレングリコール   7(8)ピロリド
ンカルボン酸 ナトリウム 1
Upper layer: ○...Transparent X...White cloudy interface Surface 20.
...Not present ×...Present (activator layer) Lower layer: ○...Transparent △...Slightly cloudy Separation speed after mixing: O...Fast ×...Slow 1st Table Example 2 Skin lotion (1) Polyglycerin (6) Nonylphenyl ether 0.6% (2) Polyglycerin (10) Nonylphenyl ether 0.4 (3) Squalane 15 (4) Fragrance
0.1(5) Ethanol
15(6) Preservative 081(
7) Glycerin 5 (8) Sodium lactate 1 (9) Pigment appropriate amount (10) Purified water 62.8 Example 3
Aftershave lotion (1) Polyglycerin (8
) Nonylphenyl ether 2% (2] Polyglycerin (5) Nonylphenyl ether 0.5 (3) Liquid paraffin 5 (4) Glyceryl trioctanoate 2 (5) Fragrance 0.2 (6) L-menthol 0. 3(7) Ethanol
20 (8) Loofah extract 0.5 (9) Propylene glycol 5 (10) Sodium dihydrogen phosphate 0.5 (11) Purified water 64.01 Example 4 Carmine lotion (1) Polyglycerin (10) Nonylphenyl Ether 1 (2) Isopropyl myristate 2 (3) Octyl p-dimethylaminobenzoate 1 (4) Fragrance 0.1 (5) Ethanol 10 (6N, 3-butylene glycol 10) (7) Sodium carbonate 1.5 (8) ) Titanium oxide 5 (9) Iron oxide appropriate amount (10) Trisodium edetacetate 0.2 (11) Purified water 69.2 Example 4 Scarbrosion (1) Polyglycerin (8) Polystylphenyl ether 4 (2 ) Silicone oil 3 (3) Vitamin E derivative 0.5 (4) Fragrance
0.1(5) l-menthol
0.1(6) Ethanol 30
(7) Dipropylene glycol 7 (8) Sodium pyrrolidone carboxylate 1

Claims (1)

【特許請求の範囲】 (イ)ポリグリセリンアルキルフェニルエーテル型化合
物から選ばれる一種又は二種以上 (ロ)水溶性塩類 (ハ)常温で液状の油性物質 及び (ニ)水 を必須成分として含有することを特徴とする多層型化粧
料。
[Scope of Claims] (1) Contains one or more selected from polyglycerol alkyl phenyl ether type compounds (2) water-soluble salts (3) oily substances that are liquid at room temperature and (2) water as essential components. A multi-layer cosmetic that is characterized by:
JP16955186A 1986-07-18 1986-07-18 Multilayer type cosmetic Pending JPS6327409A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP16955186A JPS6327409A (en) 1986-07-18 1986-07-18 Multilayer type cosmetic

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP16955186A JPS6327409A (en) 1986-07-18 1986-07-18 Multilayer type cosmetic

Publications (1)

Publication Number Publication Date
JPS6327409A true JPS6327409A (en) 1988-02-05

Family

ID=15888569

Family Applications (1)

Application Number Title Priority Date Filing Date
JP16955186A Pending JPS6327409A (en) 1986-07-18 1986-07-18 Multilayer type cosmetic

Country Status (1)

Country Link
JP (1) JPS6327409A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0370856A2 (en) * 1988-11-09 1990-05-30 L'oreal Eye make-up remover with two distinct phases
JPH10182420A (en) * 1996-12-27 1998-07-07 Kose Corp Two-layer bath preparation
EP1475077A2 (en) * 2003-05-09 2004-11-10 Henkel Kommanditgesellschaft auf Aktien Double phase liquid antitranspirant compositions
JP2010024177A (en) * 2008-07-18 2010-02-04 Nippon Menaade Keshohin Kk Makeup remover
JP2018027917A (en) * 2016-08-18 2018-02-22 森永製菓株式会社 METHOD OF STABILIZING GLUCOSE p-COUMARIC ACID GLYCOSIDE, AND METHOD OF PRODUCING GLUCOSE p-COUMARIC ACID GLYCOSIDE SOLUTION USING THE SAME

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55139312A (en) * 1979-04-12 1980-10-31 Kanebo Ltd Two-layer cleansing lotion
JPS58177910A (en) * 1982-04-12 1983-10-18 Shiseido Co Ltd Three-layered type liquid skin cosmetic
JPS606609A (en) * 1983-05-31 1985-01-14 ロレアル Oral cavity product
JPS6018594A (en) * 1983-04-15 1985-01-30 ロレアル Detergent and foaming composition
JPS61145138A (en) * 1984-12-17 1986-07-02 ロレアル Polyglyceroled nonionic surfactant, manufacture and cosmeticcomposition

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55139312A (en) * 1979-04-12 1980-10-31 Kanebo Ltd Two-layer cleansing lotion
JPS58177910A (en) * 1982-04-12 1983-10-18 Shiseido Co Ltd Three-layered type liquid skin cosmetic
JPS6018594A (en) * 1983-04-15 1985-01-30 ロレアル Detergent and foaming composition
JPS606609A (en) * 1983-05-31 1985-01-14 ロレアル Oral cavity product
JPS61145138A (en) * 1984-12-17 1986-07-02 ロレアル Polyglyceroled nonionic surfactant, manufacture and cosmeticcomposition

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0370856A2 (en) * 1988-11-09 1990-05-30 L'oreal Eye make-up remover with two distinct phases
JPH10182420A (en) * 1996-12-27 1998-07-07 Kose Corp Two-layer bath preparation
EP1475077A2 (en) * 2003-05-09 2004-11-10 Henkel Kommanditgesellschaft auf Aktien Double phase liquid antitranspirant compositions
EP1475077A3 (en) * 2003-05-09 2005-01-26 Henkel Kommanditgesellschaft auf Aktien Double phase liquid antitranspirant compositions
JP2010024177A (en) * 2008-07-18 2010-02-04 Nippon Menaade Keshohin Kk Makeup remover
JP2018027917A (en) * 2016-08-18 2018-02-22 森永製菓株式会社 METHOD OF STABILIZING GLUCOSE p-COUMARIC ACID GLYCOSIDE, AND METHOD OF PRODUCING GLUCOSE p-COUMARIC ACID GLYCOSIDE SOLUTION USING THE SAME

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