JPS6296325A - ゾルゲル法によるガラスの製造法 - Google Patents
ゾルゲル法によるガラスの製造法Info
- Publication number
- JPS6296325A JPS6296325A JP23318885A JP23318885A JPS6296325A JP S6296325 A JPS6296325 A JP S6296325A JP 23318885 A JP23318885 A JP 23318885A JP 23318885 A JP23318885 A JP 23318885A JP S6296325 A JPS6296325 A JP S6296325A
- Authority
- JP
- Japan
- Prior art keywords
- solution
- sol
- bubbles
- glass
- reduced pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011521 glass Substances 0.000 title claims abstract description 17
- 238000003980 solgel method Methods 0.000 title claims abstract description 9
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 8
- 230000007062 hydrolysis Effects 0.000 claims abstract description 6
- 229910052751 metal Inorganic materials 0.000 claims description 7
- 239000002184 metal Substances 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 19
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 7
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 abstract description 5
- 239000002253 acid Substances 0.000 abstract description 4
- 239000003513 alkali Substances 0.000 abstract description 4
- 230000003301 hydrolyzing effect Effects 0.000 abstract description 4
- 239000003054 catalyst Substances 0.000 abstract description 2
- 238000003756 stirring Methods 0.000 abstract description 2
- 239000000243 solution Substances 0.000 description 22
- 238000001879 gelation Methods 0.000 description 13
- 238000000034 method Methods 0.000 description 9
- 239000011240 wet gel Substances 0.000 description 5
- 239000000499 gel Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 239000003377 acid catalyst Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/006—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels to produce glass through wet route
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Glass Melting And Manufacturing (AREA)
- Silicon Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP23318885A JPS6296325A (ja) | 1985-10-21 | 1985-10-21 | ゾルゲル法によるガラスの製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP23318885A JPS6296325A (ja) | 1985-10-21 | 1985-10-21 | ゾルゲル法によるガラスの製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6296325A true JPS6296325A (ja) | 1987-05-02 |
| JPH0556292B2 JPH0556292B2 (enrdf_load_stackoverflow) | 1993-08-19 |
Family
ID=16951117
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP23318885A Granted JPS6296325A (ja) | 1985-10-21 | 1985-10-21 | ゾルゲル法によるガラスの製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6296325A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6465029A (en) * | 1987-09-04 | 1989-03-10 | Toshiba Ceramics Co | Production of glass |
| US6184131B1 (en) * | 1996-10-18 | 2001-02-06 | Nec Corporation | Process of forming solid thin film from layer of liquid material without void and film forming apparatus used therein |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58167436A (ja) * | 1982-03-26 | 1983-10-03 | Hitachi Ltd | 光学ガラスの製造方法 |
| JPS6186429A (ja) * | 1984-10-05 | 1986-05-01 | Sumitomo Electric Ind Ltd | ガラスの製造方法 |
-
1985
- 1985-10-21 JP JP23318885A patent/JPS6296325A/ja active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58167436A (ja) * | 1982-03-26 | 1983-10-03 | Hitachi Ltd | 光学ガラスの製造方法 |
| JPS6186429A (ja) * | 1984-10-05 | 1986-05-01 | Sumitomo Electric Ind Ltd | ガラスの製造方法 |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6465029A (en) * | 1987-09-04 | 1989-03-10 | Toshiba Ceramics Co | Production of glass |
| US6184131B1 (en) * | 1996-10-18 | 2001-02-06 | Nec Corporation | Process of forming solid thin film from layer of liquid material without void and film forming apparatus used therein |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0556292B2 (enrdf_load_stackoverflow) | 1993-08-19 |
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