JPS62239352A - Production of photomagnetic recording medium - Google Patents

Production of photomagnetic recording medium

Info

Publication number
JPS62239352A
JPS62239352A JP8172186A JP8172186A JPS62239352A JP S62239352 A JPS62239352 A JP S62239352A JP 8172186 A JP8172186 A JP 8172186A JP 8172186 A JP8172186 A JP 8172186A JP S62239352 A JPS62239352 A JP S62239352A
Authority
JP
Japan
Prior art keywords
film
target
sputtering
thin film
substrate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP8172186A
Other languages
Japanese (ja)
Inventor
Seiji Yumoto
誠司 湯本
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NEC Corp
Original Assignee
NEC Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NEC Corp filed Critical NEC Corp
Priority to JP8172186A priority Critical patent/JPS62239352A/en
Publication of JPS62239352A publication Critical patent/JPS62239352A/en
Pending legal-status Critical Current

Links

Abstract

PURPOSE:To form a film having an excellent magnetic characteristic by providing a target having a strong gettering action or a vaporization source in a film forming device, carrying out sputtering or vapor deposition to form the desired thin film, and decreasing the oxygen partial pressure during the formation of the film. CONSTITUTION:A substrate is set on a counter electrode 8, a vacuum vessel 1 is evacuated, and a sputtering gas is introduced from a gas inlet hole 3 so that the pressure is controlled to 10<-3>-10<-4>Torr. A substrate shutter 7 is closed, and a target 4 is sputtered. Then the vacuum vessel 1 is again evacuated to about 10<-7>Torr, a sputtering gas is introduced, the substrate shutter 7 is opened, and the desired thin film is formed. The effect can be enhanced by repeating the sputtering with the target 4. As a result, a magneto-optical recording medi um having a low content of oxygen in the film and exhibiting a sharp Kerr rotational angle formation hysteresis loop is formed.

Description

【発明の詳細な説明】 (産業上の利用分野) 本発明は、例えば、書換え可能な光磁気デスクなどに用
いられ、磁気カー回転効果、あるいはファラデー効果な
どの磁気光学効果を用いて読みだすことのできる光磁気
記録媒体の製法に係わる。
[Detailed Description of the Invention] (Industrial Application Field) The present invention is used, for example, in a rewritable magneto-optical desk, and reads data using a magneto-optic effect such as the magnetic Kerr rotation effect or the Faraday effect. It is concerned with the manufacturing method of magneto-optical recording media that can be used.

(従来の技術) 近年、レーザーを用いた高密度記録法として、?、+u
   JlムL FTZZ lk−& l  プ1コb
L4tI−に−+−巳☆IF−4,衾り二μ ツヤとに
よりビットを書込み、磁気光学効果を利用して読みだす
という光磁気記録が研究開発されている。その記録媒体
として、量産に適し且つ読み出しノイズの少ないGdT
bFe、DyFe、GdCo、GdFe。
(Conventional technology) In recent years, as a high-density recording method using a laser, ? ,+u
Jlmu L FTZZ lk-&l pu1cob
Magneto-optical recording is being researched and developed in which bits are written in L4tI- by -+-sniff☆IF-4, 2μ gloss and read out using the magneto-optic effect. As a recording medium, GdT is suitable for mass production and has low read noise.
bFe, DyFe, GdCo, GdFe.

TbDyFe、TbFeCoなどの希土類−遷移金属か
らなる非晶質薄膜が注目されている。
Amorphous thin films made of rare earth-transition metals such as TbDyFe and TbFeCo are attracting attention.

(発明が解決しようとする問題点) GdTbFeをはじめとして、一般にこれら薄膜は、耐
蝕性におとり、湿気を有する雰囲気中では、腐食されて
磁気特性の劣化、外観の劣化を生じるという欠点をもつ
(Problems to be Solved by the Invention) These thin films, including GdTbFe, generally have poor corrosion resistance, but have the disadvantage that they corrode in a humid atmosphere, resulting in deterioration of magnetic properties and appearance.

膜形成後の記録媒体の劣化を防ぐ為に、従来から記録媒
体上に光学的に透明なSiO,5i02.Si3N4な
どの保護膜が設けられている。しかしながら、膜形成時
において取りこまれた酸素による特性の劣化は、従来技
術では十分に対処されていない。
In order to prevent deterioration of the recording medium after film formation, optically transparent SiO, 5i02. A protective film such as Si3N4 is provided. However, deterioration of properties due to oxygen introduced during film formation has not been adequately addressed in the prior art.

本発明の目的は、磁気特性の優れた記録媒体の製法を提
供することにある。
An object of the present invention is to provide a method for manufacturing a recording medium with excellent magnetic properties.

(発明が解決しようとする手段) 本発明は、製膜装置内にゲッター作用の強いターゲット
、又は蒸発源を設け、前記ターゲット、又は蒸発源によ
りスパッター又は蒸着を行なった後、目的の薄膜を形成
することにより、膜形成時の酸素分圧を下げ、磁気特性
の良い膜形成が可能であることを特徴としている。
(Means to be Solved by the Invention) The present invention provides a target with a strong getter action or an evaporation source in a film forming apparatus, and after sputtering or vapor deposition is performed using the target or evaporation source, a desired thin film is formed. By doing so, it is possible to lower the oxygen partial pressure during film formation and form a film with good magnetic properties.

(作用) 本発明は、製膜装置内にゲッター作用の強いターゲット
、又は蒸発源を設け、前記ターゲット、又は蒸発源によ
りスパッター又は蒸着を行なった後、目的の薄膜を形成
することにより、膜形成時の酸素分圧を下げ、磁気特性
の良い膜形成が可能であることを特徴としている。この
方法により膜中の酸素量が少ない薄膜が形成され、磁気
特性が良く、しかも、弁傘の長い光磁気記録媒体が得ら
れる。
(Function) The present invention provides a target with a strong getter effect or an evaporation source in a film forming apparatus, and after performing sputtering or evaporation using the target or evaporation source, a desired thin film is formed. It is characterized by the ability to lower the oxygen partial pressure at the time and form a film with good magnetic properties. By this method, a thin film with a small amount of oxygen in the film is formed, and a magneto-optical recording medium with good magnetic properties and a long umbrella can be obtained.

(実施例−1) 第1図は、スパッター法により本発明を実施するための
一例を示す図である。第1図中1は真空容器、2は真空
ポンプへの排気孔、3はスパッターのだめのガス導入孔
、4はゲッター作用の強いターゲット(例えば、Ti、
Si、Fe、Tb等)、5は目的の膜形成するためのタ
ーゲット、6は電力導入端子、7は基板シャッター、8
は接地された対向電極であり、基板ホルダーを兼ねてい
る。
(Example-1) FIG. 1 is a diagram showing an example of implementing the present invention by a sputtering method. In Fig. 1, 1 is a vacuum container, 2 is an exhaust hole to the vacuum pump, 3 is a gas inlet hole for sputtering, and 4 is a target with a strong getter action (for example, Ti,
(Si, Fe, Tb, etc.), 5 is a target for forming the desired film, 6 is a power introduction terminal, 7 is a substrate shutter, 8
is a grounded counter electrode, which also serves as a substrate holder.

第1図に基づき、本発明の薄膜の製造方法の一例を説明
する。基板ホルダーを兼ねた対向71!tffis上に
基板を設置した後、真空容51を10 ”Torr程度
まで排気する。しかるのち、ガス導入孔3よりスパッタ
ーガスを10−3〜10 ’Torrの範囲になるよう
に導入する。基板シャッター7を閉じた状態で、ターゲ
ット4を1000程度スパッターする。この膜厚は、タ
ーゲット4の材質により、数100人から数1000人
の厚みでつける。この後、真空容器1を再び1O−7T
orr程度まで排気し、スパッターガスを導入して、基
板シャッター7を開き、目的の薄膜を形成する。
An example of the method for manufacturing a thin film of the present invention will be explained based on FIG. Opposing 71 that also serves as a board holder! After placing the substrate on the tffis, the vacuum volume 51 is evacuated to about 10' Torr. Then, sputtering gas is introduced from the gas introduction hole 3 to a pressure in the range of 10-3 to 10' Torr.Substrate shutter 7 is closed, the target 4 is sputtered to a thickness of about 1000 mm.The film thickness is from several 100 to several 1000 mm depending on the material of the target 4.After this, the vacuum vessel 1 is sputtered again at 10-7T.
The gas is evacuated to a level of 10.0 m, sputtering gas is introduced, and the substrate shutter 7 is opened to form a desired thin film.

上記の薄膜製造方法において、ターゲット4によるスパ
ッターを、何度か繰り返すことにより、効果を大きくす
ることができる。また、ターゲット1により形成された
薄膜が、基板に積層されても、特性に影響しない場合に
は、基板シャッター7を開いたままターゲット4をスパ
ッターしてもよい。この場合には、膜形成後の保護膜を
兼ねることができる。
In the above thin film manufacturing method, the effect can be increased by repeating sputtering using the target 4 several times. Further, even if the thin film formed by the target 1 is laminated on the substrate, if the characteristics are not affected, the target 4 may be sputtered with the substrate shutter 7 open. In this case, it can also serve as a protective film after film formation.

この製法により、膜中の酸素量が少なく、角形成のよい
カー回転ヒステリシスループを示す光磁気記録媒体を形
成することができる。第3図(a)、(b)に、膜形成
時に取りこまれた酸素量による、カー回転ヒステリシス
ループの違いを示す。第3図(a)は、取りこまれた酸
素量の多い場合であり、第3図(b)は、取りこまれた
酸素量の少ない場合である。
By this manufacturing method, it is possible to form a magneto-optical recording medium that has a small amount of oxygen in the film and exhibits a well-formed Kerr rotation hysteresis loop. FIGS. 3(a) and 3(b) show the difference in the Kerr rotation hysteresis loop depending on the amount of oxygen taken in during film formation. FIG. 3(a) shows a case where the amount of oxygen taken in is large, and FIG. 3(b) shows a case where the amount of oxygen taken in is small.

(実施例−2) 第2図は、蒸着法により本発明を実施するための一例を
示す図である。実施方法は、実施例−1同様であり、蒸
発源9により蒸着を行った後、蒸発源10により目的の
薄膜を形成する。
(Example-2) FIG. 2 is a diagram showing an example of implementing the present invention by a vapor deposition method. The implementation method is the same as in Example-1, and after vapor deposition is performed using the evaporation source 9, the desired thin film is formed using the evaporation source 10.

(発明の効果) 本発明によれば、形成された膜中の酸素を極力少なくす
ることができ、それにより特性が良く弄命の長い光磁気
記録媒体を得ることができる。
(Effects of the Invention) According to the present invention, the amount of oxygen in the formed film can be reduced as much as possible, thereby making it possible to obtain a magneto-optical recording medium with good characteristics and a long lifespan.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は、スパッター法により本発明を実施するための
装置の説明図、第2図は、蒸着法により本発明を実施す
るための装置の説明図、第3図(a)、(b)は、取り
こまれた酸素量の違いによるカー回転ヒステリシスルー
プの違いを示す図、 1・・・真空容器、2・・・真空ポンプへの排気孔、3
・・・ガス導入孔、4・・・ゲッター作用の強いターゲ
ット、50.。 目的の薄膜を形成するためのターゲット、6・・・電力
導入端子、7・・・基板シャッター、8・・・対向電極
、又は、基板ホルダー、9・・・ゲッター作用の強い蒸
発源、10・・・目的の薄膜を形成するための蒸発源。 □−1\ 代、・二′、、〜゛士1“Δム、′、1目。 \。 亭   1   図
Fig. 1 is an explanatory diagram of an apparatus for carrying out the present invention by sputtering method, Fig. 2 is an explanatory diagram of an apparatus for carrying out the invention by vapor deposition method, and Figs. 3(a) and (b). The figure shows the difference in the Kerr rotation hysteresis loop due to the difference in the amount of oxygen taken in. 1... Vacuum vessel, 2... Exhaust hole to the vacuum pump, 3
... Gas introduction hole, 4... Target with strong getter action, 50. . Target for forming the desired thin film, 6... Power introduction terminal, 7... Substrate shutter, 8... Counter electrode or substrate holder, 9... Evaporation source with strong getter action, 10. ...Evaporation source for forming the desired thin film. □−1\ 代、・2′、、〜゛士1「Δm、′、1st. \。 Tei 1 Figure

Claims (1)

【特許請求の範囲】[Claims] 製膜装置中に、ゲッター作用の大きなターゲット、又は
蒸発源を設け、前記ターゲット、又は蒸発源によりスパ
ッター又は蒸着を行なった後、目的の薄膜を形成するこ
とを特徴とする光磁気記録媒体の製造方法。
Production of a magneto-optical recording medium characterized in that a target or evaporation source with a large getter action is provided in a film forming apparatus, and after sputtering or evaporation is performed by the target or evaporation source, a desired thin film is formed. Method.
JP8172186A 1986-04-08 1986-04-08 Production of photomagnetic recording medium Pending JPS62239352A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP8172186A JPS62239352A (en) 1986-04-08 1986-04-08 Production of photomagnetic recording medium

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP8172186A JPS62239352A (en) 1986-04-08 1986-04-08 Production of photomagnetic recording medium

Publications (1)

Publication Number Publication Date
JPS62239352A true JPS62239352A (en) 1987-10-20

Family

ID=13754278

Family Applications (1)

Application Number Title Priority Date Filing Date
JP8172186A Pending JPS62239352A (en) 1986-04-08 1986-04-08 Production of photomagnetic recording medium

Country Status (1)

Country Link
JP (1) JPS62239352A (en)

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