JPS62210053A - 光学異性体分離用充填剤 - Google Patents

光学異性体分離用充填剤

Info

Publication number
JPS62210053A
JPS62210053A JP61051062A JP5106286A JPS62210053A JP S62210053 A JPS62210053 A JP S62210053A JP 61051062 A JP61051062 A JP 61051062A JP 5106286 A JP5106286 A JP 5106286A JP S62210053 A JPS62210053 A JP S62210053A
Authority
JP
Japan
Prior art keywords
packing material
column
compd
crown
optically active
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP61051062A
Other languages
English (en)
Japanese (ja)
Other versions
JPH0357816B2 (enExample
Inventor
Toshio Shinpo
外志夫 新保
Koichiro Nishimura
浩一郎 西村
Tomohiko Yamaguchi
智彦 山口
Masaaki Sugiura
正昭 杉浦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
National Institute of Advanced Industrial Science and Technology AIST
Original Assignee
Agency of Industrial Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Agency of Industrial Science and Technology filed Critical Agency of Industrial Science and Technology
Priority to JP61051062A priority Critical patent/JPS62210053A/ja
Priority to US07/022,039 priority patent/US4842935A/en
Priority to DE19873707291 priority patent/DE3707291A1/de
Publication of JPS62210053A publication Critical patent/JPS62210053A/ja
Publication of JPH0357816B2 publication Critical patent/JPH0357816B2/ja
Granted legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/29—Chiral phases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004—Sorbent size or size distribution, e.g. particle size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3092—Packing of a container, e.g. packing a cartridge or column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204—Inorganic carriers, supports or substrates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3242—Layers with a functional group, e.g. an affinity material, a ligand, a reactant or a complexing group
    • B01J20/3244—Non-macromolecular compounds
    • B01J20/3246—Non-macromolecular compounds having a well defined chemical structure
    • B01J20/3248—Non-macromolecular compounds having a well defined chemical structure the functional group or the linking, spacer or anchoring group as a whole comprising at least one type of heteroatom selected from a nitrogen, oxygen or sulfur, these atoms not being part of the carrier as such
    • B01J20/3253—Non-macromolecular compounds having a well defined chemical structure the functional group or the linking, spacer or anchoring group as a whole comprising at least one type of heteroatom selected from a nitrogen, oxygen or sulfur, these atoms not being part of the carrier as such comprising a cyclic structure not containing any of the heteroatoms nitrogen, oxygen or sulfur, e.g. aromatic structures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3242—Layers with a functional group, e.g. an affinity material, a ligand, a reactant or a complexing group
    • B01J20/3244—Non-macromolecular compounds
    • B01J20/3246—Non-macromolecular compounds having a well defined chemical structure
    • B01J20/3248—Non-macromolecular compounds having a well defined chemical structure the functional group or the linking, spacer or anchoring group as a whole comprising at least one type of heteroatom selected from a nitrogen, oxygen or sulfur, these atoms not being part of the carrier as such
    • B01J20/3255—Non-macromolecular compounds having a well defined chemical structure the functional group or the linking, spacer or anchoring group as a whole comprising at least one type of heteroatom selected from a nitrogen, oxygen or sulfur, these atoms not being part of the carrier as such comprising a cyclic structure containing at least one of the heteroatoms nitrogen, oxygen or sulfur, e.g. heterocyclic or heteroaromatic structures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/54—Sorbents specially adapted for analytical or investigative chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/58—Use in a single column
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00—Chemistry: molecular biology and microbiology
    • Y10S435/803—Physical recovery methods, e.g. chromatography, grinding
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
    • Y10T428/2991—Coated
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
    • Y10T428/2991—Coated
    • Y10T428/2993—Silicic or refractory material containing [e.g., tungsten oxide, glass, cement, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
    • Y10T428/2991—Coated
    • Y10T428/2998—Coated including synthetic resin or polymer

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
JP61051062A 1986-03-07 1986-03-07 光学異性体分離用充填剤 Granted JPS62210053A (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP61051062A JPS62210053A (ja) 1986-03-07 1986-03-07 光学異性体分離用充填剤
US07/022,039 US4842935A (en) 1986-03-07 1987-03-05 Filler for separating optical isomer
DE19873707291 DE3707291A1 (de) 1986-03-07 1987-03-06 Fuellstoff zum abtrennen von optischen isomeren

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP61051062A JPS62210053A (ja) 1986-03-07 1986-03-07 光学異性体分離用充填剤

Publications (2)

Publication Number Publication Date
JPS62210053A true JPS62210053A (ja) 1987-09-16
JPH0357816B2 JPH0357816B2 (enExample) 1991-09-03

Family

ID=12876315

Family Applications (1)

Application Number Title Priority Date Filing Date
JP61051062A Granted JPS62210053A (ja) 1986-03-07 1986-03-07 光学異性体分離用充填剤

Country Status (2)

Country Link
US (1) US4842935A (enExample)
JP (1) JPS62210053A (enExample)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0269472A (ja) * 1988-09-05 1990-03-08 Agency Of Ind Science & Technol 新規なクラウンエーテル化合物及び分離剤
JPH02290898A (ja) * 1989-04-28 1990-11-30 Daicel Chem Ind Ltd 立体異性体の分離法
KR100364255B1 (ko) * 2000-09-08 2002-12-12 현명호 생리활성 라세미 일차 아미노 화합물의 광학분할을 위한ｌｃ용 크라운 에테르 키랄고정상 및 이들로 충진된키랄칼럼
WO2012050124A1 (ja) * 2010-10-13 2012-04-19 株式会社ダイセル クロマトグラフィー用分離剤
JP2013023483A (ja) * 2011-07-22 2013-02-04 Toyoji Shimada クラウンエーテル様環状構造及びビナフチル基を有する新規化合物及びその製造方法
WO2014126028A1 (ja) 2013-02-12 2014-08-21 国立大学法人 金沢大学 光学活性ポリ（ジフェニルアセチレン）化合物及びその製造方法、並びにその光学異性体分離剤としての用途
WO2023008546A1 (ja) * 2021-07-29 2023-02-02 株式会社ダイセル 液体クロマトグラフィーによるアミンの分離方法

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2925753B2 (ja) * 1990-02-23 1999-07-28 ダイセル化学工業株式会社 光学異性体の分離方法
US5110474A (en) * 1990-04-09 1992-05-05 Arch Development Corporation Method for liquid chromatographic extraction of strontium from acid solutions
US5498752A (en) * 1991-08-22 1996-03-12 Daicel Chemical Industries, Ltd. Process for recovering optical isomers and solvent, process for using solvent by circulation and process for reusing optical isomers in optical resolution
JP3010816B2 (ja) * 1991-08-22 2000-02-21 ダイセル化学工業株式会社 光学分割における光学異性体と溶媒との回収方法、溶媒の循環使用方法、および光学異性体の再利用方法
DE4217203C2 (de) * 1992-05-23 1995-09-21 Degussa Verfahren zum Abtrennen von Aminosäuren aus wäßrigen Lösungen
US5968364A (en) * 1993-03-16 1999-10-19 Henkel Corporation Process for the removal of toxic cyanide and heavy metal species from alkaline solutions
US5651883A (en) * 1995-06-06 1997-07-29 Argonne National Laboratory/University Of Chicago Development Corp. Method for the chromatographic separation of cations from aqueous samples
CN1099593C (zh) * 1995-12-21 2003-01-22 大赛璐化学工业株式会社 高效液体色谱用填充剂
US5865994A (en) * 1997-03-13 1999-02-02 Dionex Corporation Bifunctional crown ether-based cation-exchange stationary phase for liquid chromatography
KR100622436B1 (ko) * 1999-12-18 2006-09-11 삼성토탈 주식회사 노보렌 이성질체의 분리방법
US20190126241A1 (en) * 2017-09-26 2019-05-02 Waters Technologies Corporation High purity chromatographic materials comprising an ionizable modifier for retention of acidic analytes

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4474963A (en) * 1980-11-03 1984-10-02 W. R. Grace & Co. Crown ether compositions with sidearms affording enhanced cation binding
US4640943A (en) * 1983-09-22 1987-02-03 Ajinomoto Co., Inc. Surface modifier for inorganic substances

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0269472A (ja) * 1988-09-05 1990-03-08 Agency Of Ind Science & Technol 新規なクラウンエーテル化合物及び分離剤
JPH02290898A (ja) * 1989-04-28 1990-11-30 Daicel Chem Ind Ltd 立体異性体の分離法
KR100364255B1 (ko) * 2000-09-08 2002-12-12 현명호 생리활성 라세미 일차 아미노 화합물의 광학분할을 위한ｌｃ용 크라운 에테르 키랄고정상 및 이들로 충진된키랄칼럼
WO2012050124A1 (ja) * 2010-10-13 2012-04-19 株式会社ダイセル クロマトグラフィー用分離剤
US9145430B2 (en) 2010-10-13 2015-09-29 Daicel Corporation Separating agent for chromatography
JP2013023483A (ja) * 2011-07-22 2013-02-04 Toyoji Shimada クラウンエーテル様環状構造及びビナフチル基を有する新規化合物及びその製造方法
WO2014126028A1 (ja) 2013-02-12 2014-08-21 国立大学法人 金沢大学 光学活性ポリ（ジフェニルアセチレン）化合物及びその製造方法、並びにその光学異性体分離剤としての用途
WO2023008546A1 (ja) * 2021-07-29 2023-02-02 株式会社ダイセル 液体クロマトグラフィーによるアミンの分離方法

Also Published As

Publication number Publication date
US4842935A (en) 1989-06-27
JPH0357816B2 (enExample) 1991-09-03

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Legal Events

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EXPY Cancellation because of completion of term