JPS6217325B2 - - Google Patents

Info

Publication number

JPS6217325B2

JPS6217325B2 JP13031480A JP13031480A JPS6217325B2 JP S6217325 B2 JPS6217325 B2 JP S6217325B2 JP 13031480 A JP13031480 A JP 13031480A JP 13031480 A JP13031480 A JP 13031480A JP S6217325 B2 JPS6217325 B2 JP S6217325B2

Authority

JP

Japan

Prior art keywords

paste

transparent conductive

conductive film

acetope

dimethyltin

Prior art date

1980-09-19

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Links

• Espacenet
• Global Dossier
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• ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 12
• 229910052738 indium Inorganic materials 0.000 claims description 12
• APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 claims description 9
• 239000002904 solvent Substances 0.000 claims description 9
• QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 claims description 6
• 239000003795 chemical substances by application Substances 0.000 claims description 6
• 229940007550 benzyl acetate Drugs 0.000 claims description 3
• 150000001875 compounds Chemical class 0.000 claims description 3
• 229920002678 cellulose Polymers 0.000 claims description 2
• 239000001913 cellulose Substances 0.000 claims description 2
• PWEVMPIIOJUPRI-UHFFFAOYSA-N dimethyltin Chemical compound C[Sn]C PWEVMPIIOJUPRI-UHFFFAOYSA-N 0.000 description 14
• 229910052718 tin Inorganic materials 0.000 description 11
• YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 description 8
• WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 8
• CUJRVFIICFDLGR-UHFFFAOYSA-N acetylacetonate Chemical compound CC(=O)[CH-]C(C)=O CUJRVFIICFDLGR-UHFFFAOYSA-N 0.000 description 6
• 238000000034 method Methods 0.000 description 6
• 238000007650 screen-printing Methods 0.000 description 6
• 238000009835 boiling Methods 0.000 description 5
• 238000010304 firing Methods 0.000 description 5
• NIQCNGHVCWTJSM-UHFFFAOYSA-N Dimethyl phthalate Chemical compound COC(=O)C1=CC=CC=C1C(=O)OC NIQCNGHVCWTJSM-UHFFFAOYSA-N 0.000 description 4
• 229910006404 SnO 2 Inorganic materials 0.000 description 4
• UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 description 4
• 239000012975 dibutyltin dilaurate Substances 0.000 description 4
• 150000003606 tin compounds Chemical class 0.000 description 4
• WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 3
• 239000011521 glass Substances 0.000 description 3
• -1 indium organic acids Chemical class 0.000 description 3
• 238000004519 manufacturing process Methods 0.000 description 3
• 229910044991 metal oxide Inorganic materials 0.000 description 3
• 150000004706 metal oxides Chemical class 0.000 description 3
• 239000000126 substance Substances 0.000 description 3
• OJVAMHKKJGICOG-UHFFFAOYSA-N 2,5-hexanedione Chemical compound CC(=O)CCC(C)=O OJVAMHKKJGICOG-UHFFFAOYSA-N 0.000 description 2
• 239000000020 Nitrocellulose Substances 0.000 description 2
• 238000000576 coating method Methods 0.000 description 2
• DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 2
• FLKPEMZONWLCSK-UHFFFAOYSA-N diethyl phthalate Chemical compound CCOC(=O)C1=CC=CC=C1C(=O)OCC FLKPEMZONWLCSK-UHFFFAOYSA-N 0.000 description 2
• FBSAITBEAPNWJG-UHFFFAOYSA-N dimethyl phthalate Natural products CC(=O)OC1=CC=CC=C1OC(C)=O FBSAITBEAPNWJG-UHFFFAOYSA-N 0.000 description 2
• 229960001826 dimethylphthalate Drugs 0.000 description 2
• 238000001035 drying Methods 0.000 description 2
• 230000000694 effects Effects 0.000 description 2
• 150000002471 indium Chemical class 0.000 description 2
• 150000002472 indium compounds Chemical class 0.000 description 2
• HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 description 2
• QPJVMBTYPHYUOC-UHFFFAOYSA-N methyl benzoate Chemical compound COC(=O)C1=CC=CC=C1 QPJVMBTYPHYUOC-UHFFFAOYSA-N 0.000 description 2
• 229920001220 nitrocellulos Polymers 0.000 description 2
• 235000005985 organic acids Nutrition 0.000 description 2
• 238000001259 photo etching Methods 0.000 description 2
• 239000007921 spray Substances 0.000 description 2
• 239000000758 substrate Substances 0.000 description 2
• 238000001771 vacuum deposition Methods 0.000 description 2
• FPZWZCWUIYYYBU-UHFFFAOYSA-N 2-(2-ethoxyethoxy)ethyl acetate Chemical compound CCOCCOCCOC(C)=O FPZWZCWUIYYYBU-UHFFFAOYSA-N 0.000 description 1
• SBASXUCJHJRPEV-UHFFFAOYSA-N 2-(2-methoxyethoxy)ethanol Chemical compound COCCOCCO SBASXUCJHJRPEV-UHFFFAOYSA-N 0.000 description 1
• YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 description 1
• 239000001856 Ethyl cellulose Substances 0.000 description 1
• ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 1
• CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
• SMEGJBVQLJJKKX-HOTMZDKISA-N [(2R,3S,4S,5R,6R)-5-acetyloxy-3,4,6-trihydroxyoxan-2-yl]methyl acetate Chemical compound CC(=O)OC[C@@H]1[C@H]([C@@H]([C@H]([C@@H](O1)O)OC(=O)C)O)O SMEGJBVQLJJKKX-HOTMZDKISA-N 0.000 description 1
• FJWGYAHXMCUOOM-QHOUIDNNSA-N [(2s,3r,4s,5r,6r)-2-[(2r,3r,4s,5r,6s)-4,5-dinitrooxy-2-(nitrooxymethyl)-6-[(2r,3r,4s,5r,6s)-4,5,6-trinitrooxy-2-(nitrooxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-3,5-dinitrooxy-6-(nitrooxymethyl)oxan-4-yl] nitrate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O)O[C@H]1[C@@H]([C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@@H](CO[N+]([O-])=O)O1)O[N+]([O-])=O)CO[N+](=O)[O-])[C@@H]1[C@@H](CO[N+]([O-])=O)O[C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O FJWGYAHXMCUOOM-QHOUIDNNSA-N 0.000 description 1
• 229940081735 acetylcellulose Drugs 0.000 description 1
• 150000001298 alcohols Chemical class 0.000 description 1
• 235000019445 benzyl alcohol Nutrition 0.000 description 1
• 229910052793 cadmium Inorganic materials 0.000 description 1
• 238000001354 calcination Methods 0.000 description 1
• 229920002301 cellulose acetate Polymers 0.000 description 1
• 239000000919 ceramic Substances 0.000 description 1
• 239000011248 coating agent Substances 0.000 description 1
• 150000002148 esters Chemical class 0.000 description 1
• 238000005530 etching Methods 0.000 description 1
• XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 description 1
• 229920001249 ethyl cellulose Polymers 0.000 description 1
• 235000019325 ethyl cellulose Nutrition 0.000 description 1
• 238000001704 evaporation Methods 0.000 description 1
• 238000002474 experimental method Methods 0.000 description 1
• 239000005357 flat glass Substances 0.000 description 1
• 238000001879 gelation Methods 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• 150000002576 ketones Chemical class 0.000 description 1
• 239000007788 liquid Substances 0.000 description 1
• 239000004973 liquid crystal related substance Substances 0.000 description 1
• 238000002844 melting Methods 0.000 description 1
• 230000008018 melting Effects 0.000 description 1
• 239000002184 metal Substances 0.000 description 1
• 229910052751 metal Inorganic materials 0.000 description 1
• 229940095102 methyl benzoate Drugs 0.000 description 1
• 238000002156 mixing Methods 0.000 description 1
• 239000000203 mixture Substances 0.000 description 1
• WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 description 1
• 230000001737 promoting effect Effects 0.000 description 1
• 230000009257 reactivity Effects 0.000 description 1
• 239000004065 semiconductor Substances 0.000 description 1
• 239000002699 waste material Substances 0.000 description 1