JPS6160843B2 - - Google Patents
Info
- Publication number
- JPS6160843B2 JPS6160843B2 JP54117088A JP11708879A JPS6160843B2 JP S6160843 B2 JPS6160843 B2 JP S6160843B2 JP 54117088 A JP54117088 A JP 54117088A JP 11708879 A JP11708879 A JP 11708879A JP S6160843 B2 JPS6160843 B2 JP S6160843B2
- Authority
- JP
- Japan
- Prior art keywords
- polymer emulsion
- polymerization
- polymer
- emulsion
- chloroprene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920000642 polymer Polymers 0.000 claims description 58
- 239000000839 emulsion Substances 0.000 claims description 53
- 239000000178 monomer Substances 0.000 claims description 28
- YACLQRRMGMJLJV-UHFFFAOYSA-N chloroprene Chemical compound ClC(=C)C=C YACLQRRMGMJLJV-UHFFFAOYSA-N 0.000 claims description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000002518 antifoaming agent Substances 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 13
- 238000010438 heat treatment Methods 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 9
- 238000007720 emulsion polymerization reaction Methods 0.000 claims description 4
- 238000006116 polymerization reaction Methods 0.000 description 31
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- 229920001971 elastomer Polymers 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- LIFLRQVHKGGNSG-UHFFFAOYSA-N 2,3-dichlorobuta-1,3-diene Chemical compound ClC(=C)C(Cl)=C LIFLRQVHKGGNSG-UHFFFAOYSA-N 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 229920002050 silicone resin Polymers 0.000 description 4
- 159000000000 sodium salts Chemical class 0.000 description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000012141 concentrate Substances 0.000 description 3
- 238000005187 foaming Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229920001296 polysiloxane Polymers 0.000 description 3
- BJEMXPVDXFSROA-UHFFFAOYSA-N 3-butylbenzene-1,2-diol Chemical group CCCCC1=CC=CC(O)=C1O BJEMXPVDXFSROA-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical compound C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000003995 emulsifying agent Substances 0.000 description 2
- 230000001804 emulsifying effect Effects 0.000 description 2
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- 238000000710 polymer precipitation Methods 0.000 description 2
- 239000002685 polymerization catalyst Substances 0.000 description 2
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000013112 stability test Methods 0.000 description 2
- DBCAQXHNJOFNGC-UHFFFAOYSA-N 4-bromo-1,1,1-trifluorobutane Chemical compound FC(F)(F)CCCBr DBCAQXHNJOFNGC-UHFFFAOYSA-N 0.000 description 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- LWZFANDGMFTDAV-BURFUSLBSA-N [(2r)-2-[(2r,3r,4s)-3,4-dihydroxyoxolan-2-yl]-2-hydroxyethyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O LWZFANDGMFTDAV-BURFUSLBSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- XYLMUPLGERFSHI-UHFFFAOYSA-N alpha-Methylstyrene Chemical compound CC(=C)C1=CC=CC=C1 XYLMUPLGERFSHI-UHFFFAOYSA-N 0.000 description 1
- 235000010407 ammonium alginate Nutrition 0.000 description 1
- 239000000728 ammonium alginate Substances 0.000 description 1
- KPGABFJTMYCRHJ-YZOKENDUSA-N ammonium alginate Chemical compound [NH4+].[NH4+].O1[C@@H](C([O-])=O)[C@@H](OC)[C@H](O)[C@H](O)[C@@H]1O[C@@H]1[C@@H](C([O-])=O)O[C@@H](O)[C@@H](O)[C@H]1O KPGABFJTMYCRHJ-YZOKENDUSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- WNAHIZMDSQCWRP-UHFFFAOYSA-N dodecane-1-thiol Chemical compound CCCCCCCCCCCCS WNAHIZMDSQCWRP-UHFFFAOYSA-N 0.000 description 1
- STVZJERGLQHEKB-UHFFFAOYSA-N ethylene glycol dimethacrylate Substances CC(=C)C(=O)OCCOC(=O)C(C)=C STVZJERGLQHEKB-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- -1 fatty acid ester Chemical class 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 229920001451 polypropylene glycol Polymers 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
Landscapes
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11708879A JPS5641212A (en) | 1979-09-12 | 1979-09-12 | Treatment of polymer emulsion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11708879A JPS5641212A (en) | 1979-09-12 | 1979-09-12 | Treatment of polymer emulsion |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5641212A JPS5641212A (en) | 1981-04-17 |
| JPS6160843B2 true JPS6160843B2 (es) | 1986-12-23 |
Family
ID=14703087
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11708879A Granted JPS5641212A (en) | 1979-09-12 | 1979-09-12 | Treatment of polymer emulsion |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5641212A (es) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2241580A1 (de) | 2009-04-17 | 2010-10-20 | LANXESS Deutschland GmbH | Verfahren zur Herstellung einer Polymer-Dispersion auf Basis von Polychloropren sowie Anlage zur Herstellung einer Polymer-Dispersion auf Basis von Polychloropren |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004035846A (ja) * | 2002-07-08 | 2004-02-05 | Asahi Kasei Chemicals Corp | 重合体ラテックスの濃縮方法 |
| DE10318107A1 (de) * | 2003-04-22 | 2004-11-11 | Bayer Materialscience Ag | Wässrige Klebstoff-Dispersionen |
| JP5484680B2 (ja) * | 2008-02-18 | 2014-05-07 | 電気化学工業株式会社 | クロロプレン系重合体組成物の製造方法 |
| JP6477012B2 (ja) * | 2015-02-26 | 2019-03-06 | 日本ゼオン株式会社 | 重合体ラテックスの製造方法 |
| WO2019017239A1 (ja) * | 2017-07-19 | 2019-01-24 | 日本ゼオン株式会社 | フォームラバーの製造方法 |
| KR102651970B1 (ko) * | 2017-07-19 | 2024-03-26 | 니폰 제온 가부시키가이샤 | 폼 러버의 제조 방법 |
| CN113950487B (zh) * | 2019-05-31 | 2023-08-15 | 株式会社力森诺科 | 精制氯丁二烯系聚合物胶乳的制造方法 |
| WO2020241251A1 (ja) * | 2019-05-31 | 2020-12-03 | 昭和電工株式会社 | クロロプレン系重合体ラテックスの製造方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS51959A (en) * | 1974-05-24 | 1976-01-07 | Aaru Kutsuku Junia Uiriamu | Shigaisenhatsuseisochi |
-
1979
- 1979-09-12 JP JP11708879A patent/JPS5641212A/ja active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS51959A (en) * | 1974-05-24 | 1976-01-07 | Aaru Kutsuku Junia Uiriamu | Shigaisenhatsuseisochi |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2241580A1 (de) | 2009-04-17 | 2010-10-20 | LANXESS Deutschland GmbH | Verfahren zur Herstellung einer Polymer-Dispersion auf Basis von Polychloropren sowie Anlage zur Herstellung einer Polymer-Dispersion auf Basis von Polychloropren |
| WO2010118958A1 (de) | 2009-04-17 | 2010-10-21 | Lanxess Deutschland Gmbh | Verfahren zur herstellung einer polymer-dispersion auf basis von polychloropren sowie anlage zur herstellung einer polymer-dispersion auf basis von polychloropren |
| JP2012524132A (ja) * | 2009-04-17 | 2012-10-11 | ランクセス・ドイチュランド・ゲーエムベーハー | ポリクロロプレンに基づくポリマー分散体を生産するプロセス、および、ポリクロロプレンに基づくポリマー分散体を生産する装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5641212A (en) | 1981-04-17 |
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