JPS6152680B2 - - Google Patents
Info
- Publication number
- JPS6152680B2 JPS6152680B2 JP56028307A JP2830781A JPS6152680B2 JP S6152680 B2 JPS6152680 B2 JP S6152680B2 JP 56028307 A JP56028307 A JP 56028307A JP 2830781 A JP2830781 A JP 2830781A JP S6152680 B2 JPS6152680 B2 JP S6152680B2
- Authority
- JP
- Japan
- Prior art keywords
- glucose
- syrup
- product
- temperature
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000006188 syrup Substances 0.000 claims abstract description 100
- 235000020357 syrup Nutrition 0.000 claims abstract description 100
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 91
- 239000007787 solid Substances 0.000 claims abstract description 67
- 239000008103 glucose Substances 0.000 claims abstract description 64
- 238000000034 method Methods 0.000 claims abstract description 37
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 238000001704 evaporation Methods 0.000 claims abstract description 14
- 239000013081 microcrystal Substances 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims abstract description 9
- 238000001816 cooling Methods 0.000 claims abstract description 6
- 230000008020 evaporation Effects 0.000 claims description 10
- 238000004519 manufacturing process Methods 0.000 claims description 9
- 239000013078 crystal Substances 0.000 claims description 8
- 229920002472 Starch Polymers 0.000 claims description 6
- 239000008107 starch Substances 0.000 claims description 6
- 235000019698 starch Nutrition 0.000 claims description 6
- 239000002131 composite material Substances 0.000 claims description 4
- 230000003301 hydrolyzing effect Effects 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 230000006911 nucleation Effects 0.000 abstract description 5
- 238000010899 nucleation Methods 0.000 abstract description 5
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 93
- 229960001031 glucose Drugs 0.000 description 75
- 239000000243 solution Substances 0.000 description 29
- 238000002425 crystallisation Methods 0.000 description 23
- 230000008025 crystallization Effects 0.000 description 23
- 229920002245 Dextrose equivalent Polymers 0.000 description 20
- 239000007788 liquid Substances 0.000 description 16
- 238000009835 boiling Methods 0.000 description 14
- SPFMQWBKVUQXJV-BTVCFUMJSA-N (2r,3s,4r,5r)-2,3,4,5,6-pentahydroxyhexanal;hydrate Chemical compound O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O SPFMQWBKVUQXJV-BTVCFUMJSA-N 0.000 description 13
- WQZGKKKJIJFFOK-DVKNGEFBSA-N alpha-D-glucose Chemical compound OC[C@H]1O[C@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-DVKNGEFBSA-N 0.000 description 11
- 239000000084 colloidal system Substances 0.000 description 10
- 229960000673 dextrose monohydrate Drugs 0.000 description 10
- 238000010008 shearing Methods 0.000 description 9
- 239000008121 dextrose Substances 0.000 description 7
- 238000001694 spray drying Methods 0.000 description 7
- 239000011521 glass Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 229910001220 stainless steel Inorganic materials 0.000 description 6
- 239000010935 stainless steel Substances 0.000 description 6
- 238000007711 solidification Methods 0.000 description 5
- 230000008023 solidification Effects 0.000 description 5
- 238000002474 experimental method Methods 0.000 description 4
- 238000004898 kneading Methods 0.000 description 4
- 240000008042 Zea mays Species 0.000 description 3
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000000354 decomposition reaction Methods 0.000 description 3
- 238000004090 dissolution Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 229920001971 elastomer Polymers 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 235000000346 sugar Nutrition 0.000 description 3
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000005903 acid hydrolysis reaction Methods 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 125000000188 beta-D-glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 2
- 230000006835 compression Effects 0.000 description 2
- 238000007906 compression Methods 0.000 description 2
- 235000005822 corn Nutrition 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 230000007071 enzymatic hydrolysis Effects 0.000 description 2
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000001000 micrograph Methods 0.000 description 2
- 150000004682 monohydrates Chemical class 0.000 description 2
- 125000000449 nitro group Chemical class [O-][N+](*)=O 0.000 description 2
- 239000012047 saturated solution Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 229960004016 sucrose syrup Drugs 0.000 description 2
- 150000008163 sugars Chemical class 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 1
- 125000002353 D-glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 1
- 229920002774 Maltodextrin Polymers 0.000 description 1
- 239000005913 Maltodextrin Substances 0.000 description 1
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 description 1
- 206010027476 Metastases Diseases 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- GZCGUPFRVQAUEE-SLPGGIOYSA-N aldehydo-D-glucose Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O GZCGUPFRVQAUEE-SLPGGIOYSA-N 0.000 description 1
- 229940089206 anhydrous dextrose Drugs 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 238000005422 blasting Methods 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000008504 concentrate Nutrition 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001493 electron microscopy Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000006166 lysate Substances 0.000 description 1
- 235000009973 maize Nutrition 0.000 description 1
- 229940035034 maltodextrin Drugs 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000009401 metastasis Effects 0.000 description 1
- 230000001394 metastastic effect Effects 0.000 description 1
- 206010061289 metastatic neoplasm Diseases 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000013021 overheating Methods 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000002990 reinforced plastic Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 235000014214 soft drink Nutrition 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 229960004793 sucrose Drugs 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 230000003685 thermal hair damage Effects 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 230000005945 translocation Effects 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 238000007738 vacuum evaporation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/10—Crystallisation
Landscapes
- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Saccharide Compounds (AREA)
- Jellies, Jams, And Syrups (AREA)
- Seasonings (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB8006661 | 1980-02-27 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS56137900A JPS56137900A (en) | 1981-10-28 |
| JPS6152680B2 true JPS6152680B2 (de) | 1986-11-14 |
Family
ID=10511726
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2830781A Granted JPS56137900A (en) | 1980-02-27 | 1981-02-27 | Crystaline glucose with new configuration and production thereof |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4342603A (de) |
| EP (1) | EP0039123B1 (de) |
| JP (1) | JPS56137900A (de) |
| AT (1) | ATE9716T1 (de) |
| CA (1) | CA1171853A (de) |
| DE (1) | DE3166396D1 (de) |
| DK (1) | DK90481A (de) |
| GB (1) | GB2070015B (de) |
| GR (1) | GR74094B (de) |
| IE (1) | IE50973B1 (de) |
| ZA (1) | ZA811317B (de) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4505757A (en) * | 1982-02-16 | 1985-03-19 | Kaken Pharmaceutical Co. Ltd. | Method for a specific depolymerization of a polysaccharide having a rod-like helical conformation |
| DE3407374A1 (de) * | 1984-02-29 | 1985-08-29 | Pfeifer & Langen, 5000 Köln | Verfahren und vorrichtung zur herstellung von trockenprodukten aus zuckersirup |
| GB8406734D0 (en) * | 1984-03-15 | 1984-04-18 | Tate & Lyle Plc | Sugar process |
| JPS61103889A (ja) * | 1984-10-24 | 1986-05-22 | Hayashibara Biochem Lab Inc | 結晶エルロ−ス及びそれを含有する含蜜結晶並びにそれらの製造方法及び用途 |
| US5518551A (en) | 1993-09-10 | 1996-05-21 | Fuisz Technologies Ltd. | Spheroidal crystal sugar and method of making |
| FI952065A0 (fi) * | 1995-03-01 | 1995-04-28 | Xyrofin Oy | Foerfarande foer tillvaratagande av en kristalliserbar organisk foerening |
| FR2742164B1 (fr) * | 1995-12-11 | 1999-01-29 | Beghin Say Eridania | Sucre microcristallin : composition et methode d'obtention |
| JP3702984B2 (ja) * | 1996-07-31 | 2005-10-05 | 三井製糖株式会社 | 含蜜糖組成物 |
| FR2787811B1 (fr) * | 1998-12-24 | 2001-03-02 | Roquette Freres | Dextrose pulverulent et son procede de preparation |
| US6527868B2 (en) * | 1999-12-15 | 2003-03-04 | Roquette Freres | Dextrose in powder form and a process for the preparation thereof |
| DK1572217T3 (da) * | 2002-12-12 | 2008-12-15 | Nycomed Gmbh | Kombinationsmedikament af R,R-formoterol og ciclesonid |
| GB0315889D0 (en) * | 2003-07-08 | 2003-08-13 | Aventis Pharma Ltd | Stable pharmaceutical products |
| US8371292B2 (en) * | 2003-09-16 | 2013-02-12 | Nycomed Gmbh | Use of ciclesonide for the treatment of respiratory diseases |
| US20070134165A1 (en) * | 2004-04-20 | 2007-06-14 | Altana Pharma Ag | Use of Ciclesonide for the Treatment of Respiratory Disease in a Smoking Patient |
| FR2877186B1 (fr) * | 2004-10-29 | 2007-02-09 | Roquette Freres | Utilisation non alimentaire et non pharmaceutique d'une composition de dextrose anhydre selectionnee |
| JP5667666B2 (ja) | 2013-06-28 | 2015-02-12 | 三井製糖株式会社 | 糖結晶含有液を製造する方法 |
| EP4099846A1 (de) * | 2020-02-06 | 2022-12-14 | Cargill, Incorporated | Glukose in fester form und verfahren zur herstellung von glukose in fester form |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3236687A (en) * | 1962-07-09 | 1966-02-22 | Grain Processing Corp | Process for producing sugars from starch |
| GB1252523A (de) * | 1968-04-06 | 1971-11-03 | ||
| FR2046352A5 (en) * | 1969-04-22 | 1971-03-05 | Cpc International Inc | Anhydrous dextrose batchwise prepn |
| DE2209813A1 (de) * | 1972-03-01 | 1973-09-13 | Cpc International Inc | Verfahren zur herstellung von granulierter dextrose |
| US4059460A (en) * | 1975-11-07 | 1977-11-22 | A. E. Staley Manufacturing Company | Solid anhydrous dextrose |
| GB1567273A (en) * | 1977-07-26 | 1980-05-14 | Staley Mfg Co A E | Solid anhydrous dextrose |
-
1981
- 1981-02-23 DE DE8181300745T patent/DE3166396D1/de not_active Expired
- 1981-02-23 AT AT81300745T patent/ATE9716T1/de not_active IP Right Cessation
- 1981-02-23 EP EP81300745A patent/EP0039123B1/de not_active Expired
- 1981-02-24 US US06/237,645 patent/US4342603A/en not_active Expired - Fee Related
- 1981-02-25 CA CA000371741A patent/CA1171853A/en not_active Expired
- 1981-02-26 IE IE405/81A patent/IE50973B1/en unknown
- 1981-02-27 DK DK90481A patent/DK90481A/da not_active Application Discontinuation
- 1981-02-27 GB GB8106344A patent/GB2070015B/en not_active Expired
- 1981-02-27 JP JP2830781A patent/JPS56137900A/ja active Granted
- 1981-02-27 GR GR64256A patent/GR74094B/el unknown
- 1981-02-27 ZA ZA00811317A patent/ZA811317B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE3166396D1 (en) | 1984-11-08 |
| EP0039123A2 (de) | 1981-11-04 |
| ZA811317B (en) | 1982-03-31 |
| CA1171853A (en) | 1984-07-31 |
| GB2070015B (en) | 1983-09-01 |
| EP0039123B1 (de) | 1984-10-03 |
| ATE9716T1 (de) | 1984-10-15 |
| EP0039123A3 (en) | 1982-04-07 |
| JPS56137900A (en) | 1981-10-28 |
| IE810405L (en) | 1981-08-27 |
| GR74094B (de) | 1984-06-06 |
| US4342603A (en) | 1982-08-03 |
| GB2070015A (en) | 1981-09-03 |
| IE50973B1 (en) | 1986-08-20 |
| DK90481A (da) | 1981-08-28 |
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