JPS6121993B2 - - Google Patents
Info
- Publication number
- JPS6121993B2 JPS6121993B2 JP3382776A JP3382776A JPS6121993B2 JP S6121993 B2 JPS6121993 B2 JP S6121993B2 JP 3382776 A JP3382776 A JP 3382776A JP 3382776 A JP3382776 A JP 3382776A JP S6121993 B2 JPS6121993 B2 JP S6121993B2
- Authority
- JP
- Japan
- Prior art keywords
- melting point
- oil
- triglyceride
- fractional crystallization
- fat
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000002844 melting Methods 0.000 claims description 66
- 230000008018 melting Effects 0.000 claims description 63
- 239000003925 fat Substances 0.000 claims description 47
- 235000019197 fats Nutrition 0.000 claims description 47
- 239000003921 oil Substances 0.000 claims description 47
- 239000002904 solvent Substances 0.000 claims description 37
- 238000000034 method Methods 0.000 claims description 33
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 claims description 26
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 24
- 238000005194 fractionation Methods 0.000 claims description 22
- 150000003626 triacylglycerols Chemical class 0.000 claims description 20
- 238000001640 fractional crystallisation Methods 0.000 claims description 19
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 18
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 claims description 17
- 239000007788 liquid Substances 0.000 claims description 16
- 235000014121 butter Nutrition 0.000 claims description 15
- 244000299461 Theobroma cacao Species 0.000 claims description 11
- 235000005764 Theobroma cacao ssp. cacao Nutrition 0.000 claims description 11
- 235000005767 Theobroma cacao ssp. sphaerocarpum Nutrition 0.000 claims description 11
- 235000001046 cacaotero Nutrition 0.000 claims description 11
- 125000001931 aliphatic group Chemical group 0.000 claims description 10
- 125000004432 carbon atom Chemical group C* 0.000 claims description 6
- 239000012046 mixed solvent Substances 0.000 claims description 5
- IPCSVZSSVZVIGE-UHFFFAOYSA-N palmitic acid group Chemical group C(CCCCCCCCCCCCCCC)(=O)O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 125000005457 triglyceride group Chemical group 0.000 claims 2
- 235000021281 monounsaturated fatty acids Nutrition 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 235000019198 oils Nutrition 0.000 description 36
- 239000013078 crystal Substances 0.000 description 25
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 15
- 235000019441 ethanol Nutrition 0.000 description 13
- 239000000126 substance Substances 0.000 description 11
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 10
- 235000019879 cocoa butter substitute Nutrition 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 7
- 238000001816 cooling Methods 0.000 description 7
- 235000014593 oils and fats Nutrition 0.000 description 7
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 239000002994 raw material Substances 0.000 description 6
- 235000019482 Palm oil Nutrition 0.000 description 5
- 229940110456 cocoa butter Drugs 0.000 description 5
- 235000019868 cocoa butter Nutrition 0.000 description 5
- 239000002540 palm oil Substances 0.000 description 5
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 4
- 235000018936 Vitellaria paradoxa Nutrition 0.000 description 4
- 241001135917 Vitellaria paradoxa Species 0.000 description 4
- MWKFXSUHUHTGQN-UHFFFAOYSA-N decan-1-ol Chemical compound CCCCCCCCCCO MWKFXSUHUHTGQN-UHFFFAOYSA-N 0.000 description 4
- 239000003778 fat substitute Substances 0.000 description 4
- 235000013341 fat substitute Nutrition 0.000 description 4
- 229910052740 iodine Inorganic materials 0.000 description 4
- 239000011630 iodine Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 229940057910 shea butter Drugs 0.000 description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 238000011109 contamination Methods 0.000 description 3
- 238000004090 dissolution Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000012188 paraffin wax Substances 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000001953 recrystallisation Methods 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- 235000019484 Rapeseed oil Nutrition 0.000 description 2
- 150000001242 acetic acid derivatives Chemical class 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 235000013373 food additive Nutrition 0.000 description 2
- 239000002778 food additive Substances 0.000 description 2
- 125000005456 glyceride group Chemical group 0.000 description 2
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 description 2
- 239000005453 ketone based solvent Substances 0.000 description 2
- 150000002576 ketones Chemical class 0.000 description 2
- 150000002632 lipids Chemical class 0.000 description 2
- -1 n-hexane Chemical class 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 2
- 238000010956 selective crystallization Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000003549 soybean oil Substances 0.000 description 2
- 235000012424 soybean oil Nutrition 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 230000001052 transient effect Effects 0.000 description 2
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 1
- DPUOLQHDNGRHBS-UHFFFAOYSA-N Brassidinsaeure Natural products CCCCCCCCC=CCCCCCCCCCCCC(O)=O DPUOLQHDNGRHBS-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- URXZXNYJPAJJOQ-UHFFFAOYSA-N Erucic acid Natural products CCCCCCC=CCCCCCCCCCCCC(O)=O URXZXNYJPAJJOQ-UHFFFAOYSA-N 0.000 description 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 1
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 1
- 235000019774 Rice Bran oil Nutrition 0.000 description 1
- 235000019485 Safflower oil Nutrition 0.000 description 1
- 235000011054 acetic acid Nutrition 0.000 description 1
- 125000000218 acetic acid group Chemical class C(C)(=O)* 0.000 description 1
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- ZOJBYZNEUISWFT-UHFFFAOYSA-N allyl isothiocyanate Chemical compound C=CCN=C=S ZOJBYZNEUISWFT-UHFFFAOYSA-N 0.000 description 1
- 235000015278 beef Nutrition 0.000 description 1
- 230000036760 body temperature Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- DPUOLQHDNGRHBS-KTKRTIGZSA-N erucic acid Chemical compound CCCCCCCC\C=C/CCCCCCCCCCCC(O)=O DPUOLQHDNGRHBS-KTKRTIGZSA-N 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 125000005313 fatty acid group Chemical group 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000008172 hydrogenated vegetable oil Substances 0.000 description 1
- JMMWKPVZQRWMSS-UHFFFAOYSA-N isopropanol acetate Natural products CC(C)OC(C)=O JMMWKPVZQRWMSS-UHFFFAOYSA-N 0.000 description 1
- 229940011051 isopropyl acetate Drugs 0.000 description 1
- GWYFCOCPABKNJV-UHFFFAOYSA-N isovaleric acid Chemical compound CC(C)CC(O)=O GWYFCOCPABKNJV-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 239000008164 mustard oil Substances 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- WOFPPJOZXUTRAU-UHFFFAOYSA-N octan-4-ol Chemical compound CCCCC(O)CCC WOFPPJOZXUTRAU-UHFFFAOYSA-N 0.000 description 1
- 150000003904 phospholipids Chemical class 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 230000008707 rearrangement Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000008165 rice bran oil Substances 0.000 description 1
- 235000005713 safflower oil Nutrition 0.000 description 1
- 239000003813 safflower oil Substances 0.000 description 1
- 235000014612 sandwich biscuits Nutrition 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP3382776A JPS52117305A (en) | 1976-03-26 | 1976-03-26 | Solvent fractionation of fat and oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP3382776A JPS52117305A (en) | 1976-03-26 | 1976-03-26 | Solvent fractionation of fat and oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS52117305A JPS52117305A (en) | 1977-10-01 |
| JPS6121993B2 true JPS6121993B2 (xx) | 1986-05-29 |
Family
ID=12397311
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP3382776A Granted JPS52117305A (en) | 1976-03-26 | 1976-03-26 | Solvent fractionation of fat and oil |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS52117305A (xx) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63113998U (xx) * | 1987-01-16 | 1988-07-22 | ||
| JPH02181691A (ja) * | 1989-01-06 | 1990-07-16 | Fumio Fukushima | 携帯用下車駅通報機 |
| JP5803671B2 (ja) * | 2009-09-30 | 2015-11-04 | 不二製油株式会社 | グリセリド油脂中のクロロプロパノール類及びその形成物質、グリシドール脂肪酸エステルを低減する方法 |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2464655A1 (fr) * | 1979-09-10 | 1981-03-20 | Blohorn Sa | Procede d'obtention d'un substitut de beurre de cacao, substitut correspondant et son utilisation pour le chocolat |
-
1976
- 1976-03-26 JP JP3382776A patent/JPS52117305A/ja active Granted
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63113998U (xx) * | 1987-01-16 | 1988-07-22 | ||
| JPH02181691A (ja) * | 1989-01-06 | 1990-07-16 | Fumio Fukushima | 携帯用下車駅通報機 |
| JP5803671B2 (ja) * | 2009-09-30 | 2015-11-04 | 不二製油株式会社 | グリセリド油脂中のクロロプロパノール類及びその形成物質、グリシドール脂肪酸エステルを低減する方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS52117305A (en) | 1977-10-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0196780B1 (en) | Use of mixed acid triglycerides as a fat blooming inhibitor | |
| Rossell | Fractionation of lauric oils | |
| EP0074146B1 (en) | Wet fractionation of hardened butterfat | |
| JP4193999B2 (ja) | トリグリセリド油の分別 | |
| US3686240A (en) | Process for producing cacao butter substitute from palm oil described and claimed therein | |
| EP0081881B1 (en) | A process for the solvent fractionation of palm oil stearines and products obtained with said process | |
| US7785645B2 (en) | Process for obtaining an oil composition and the oil composition obtained therefrom | |
| US4601857A (en) | Process for fat fractionation with azeotropic solvents | |
| Young | Interchangeability of fats and oils | |
| JP3388838B2 (ja) | 製菓用油脂組成物の製造方法 | |
| JP5755472B2 (ja) | 油脂のドライ分別方法 | |
| JPS6121993B2 (xx) | ||
| JPS61242543A (ja) | ハ−ドバタ−の品質改良法 | |
| US3944585A (en) | Multi-step crystallization and blending process for making physiochemically designed fat compositions from tallow | |
| US3790608A (en) | Process for preparing edible fats by hydrogenation and fractionation of triglyceride fatty oils containing c20 and c22 fatty acids | |
| JPH0427813B2 (xx) | ||
| JP6369586B1 (ja) | 食用シアオレインおよびその製造法 | |
| JPH02150236A (ja) | ハードバター組成物 | |
| CN112970914B (zh) | 一种巧克力抑霜剂及其制备方法 | |
| JPH069465B2 (ja) | ハ−ドバタ−の製造法 | |
| JP3502158B2 (ja) | カカオ脂の分別方法及び該方法によって得られる分別脂を含有するチョコレート | |
| JP6534512B2 (ja) | ハードバターの製造方法 | |
| US4839191A (en) | Fat fractions and mixtures thereof | |
| US4880658A (en) | Obtaining a fat fraction with azeotropic solvents | |
| EP0035298B1 (en) | Process for the solvent fractionation of olive oil stearine and related products |